ES8105739A1 - Un procedimiento para obtener derivados de triciclohexiles- tano - Google Patents
Un procedimiento para obtener derivados de triciclohexiles- tanoInfo
- Publication number
- ES8105739A1 ES8105739A1 ES492809A ES492809A ES8105739A1 ES 8105739 A1 ES8105739 A1 ES 8105739A1 ES 492809 A ES492809 A ES 492809A ES 492809 A ES492809 A ES 492809A ES 8105739 A1 ES8105739 A1 ES 8105739A1
- Authority
- ES
- Spain
- Prior art keywords
- purity
- tin hydroxide
- tricyclohexyl tin
- grignard reagent
- yield basis
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title abstract 2
- WCMMILVIRZAPLE-UHFFFAOYSA-M cyhexatin Chemical compound C1CCCCC1[Sn](C1CCCCC1)(O)C1CCCCC1 WCMMILVIRZAPLE-UHFFFAOYSA-M 0.000 title 1
- 239000007818 Grignard reagent Substances 0.000 abstract 3
- 150000004795 grignard reagents Chemical class 0.000 abstract 3
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 238000009833 condensation Methods 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- RNVJQUPAEIQUTC-UHFFFAOYSA-N tricyclohexyltin Chemical class C1CCCCC1[Sn](C1CCCCC1)C1CCCCC1 RNVJQUPAEIQUTC-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/22—Tin compounds
- C07F7/2224—Compounds having one or more tin-oxygen linkages
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/22—Tin compounds
- C07F7/2208—Compounds having tin linked only to carbon, hydrogen and/or halogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PROCEDIMIENTO PARA LA OBRENCION DE DERIVADOS DE TRICICLOHEXIL-ESTAÑO A PARTIR DE HALOGENURO DE CICLOHEXIL-MAGNESIO Y TETRAHALOGENURO DE ESTAÑO. SE HACE REACCIONAR REACTIVO DE GRIGNARD Y TETRAHALOGENURO DE ESTAÑO, EN UNA RELACION MOLAR DE 3 : 1 EN UN DISOLVENTE INERTE TAL COMO TETRAHIDROFURANO O TOLUENO. SE HIDROLIZA EL PRODUCTO Y SEPARA LA FASE ORGANICA. ESTA SE DESHIDRATA, CONCENTRA Y TRATA CON UNA CANTIDAD ADICIONAL DE REACTIVO DE GRIGNARD DE MODO QUE LA RELACION MOLAR ENTRE ESTE REACTIVO Y EL TETRAHALOGENURO DE ESTAÑO SA DE 3,5 : 1 A 3,9 : 1. SE HIDROLIZA EL PRODUCTO RESULTANTE Y SEPARA LA FASE ORGANICA. SE TRATA CON HIDROXIDO SODICO, SE DESTILA EN CORRIENTE DE VAPOR Y FILTRA.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT23893/79A IT1121958B (it) | 1979-06-27 | 1979-06-27 | Procedimento per ottenere tricicloesilstagno idrossido di elevata purezza con alte rese |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES492809A0 ES492809A0 (es) | 1981-06-01 |
| ES8105739A1 true ES8105739A1 (es) | 1981-06-01 |
Family
ID=11210697
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES492809A Expired ES8105739A1 (es) | 1979-06-27 | 1980-06-26 | Un procedimiento para obtener derivados de triciclohexiles- tano |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US4330477A (es) |
| JP (1) | JPS5639095A (es) |
| AR (1) | AR220847A1 (es) |
| AT (1) | AT379813B (es) |
| AU (1) | AU538683B2 (es) |
| BE (1) | BE883956A (es) |
| BR (1) | BR8003920A (es) |
| CA (1) | CA1136150A (es) |
| CH (1) | CH646708A5 (es) |
| DE (1) | DE3023149A1 (es) |
| DK (1) | DK280880A (es) |
| ES (1) | ES8105739A1 (es) |
| FR (1) | FR2459804B1 (es) |
| GB (1) | GB2053224B (es) |
| IL (1) | IL60297A (es) |
| IT (1) | IT1121958B (es) |
| MX (1) | MX155945A (es) |
| NL (1) | NL8003407A (es) |
| SE (1) | SE450833B (es) |
| SU (1) | SU1213987A3 (es) |
| YU (1) | YU40881B (es) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3435717A1 (de) * | 1984-09-28 | 1986-04-10 | Lentia GmbH Chem. u. pharm. Erzeugnisse - Industriebedarf, 8000 München | Verfahren zur herstellung von tricyclohexylzinnhydroxid |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3010979A (en) * | 1955-07-05 | 1961-11-28 | Metal & Thermit Corp | Chemical process and product |
| US3067226A (en) * | 1960-04-20 | 1962-12-04 | Exxon Research Engineering Co | Preparation of organotin compounds |
| GB1084076A (es) * | 1964-04-08 | 1900-01-01 | ||
| FR1434534A (fr) * | 1964-04-08 | 1966-04-08 | M & T Chemicals | Procédé de préparation de composés organiques d'étain |
| US3355470A (en) * | 1964-05-06 | 1967-11-28 | M & T Chemicals Inc | Process for preparing tri-cyclohexyltin halides |
| US3402189A (en) * | 1966-03-29 | 1968-09-17 | M & T Chemicals Inc | Process for preparing tricyclohexyl tin hydroxide |
| US3607891A (en) * | 1969-04-16 | 1971-09-21 | M & T Chemicals Inc | Process for preparing tricyclohexyltin halides |
| IL42501A (en) * | 1972-06-24 | 1976-12-31 | Oxon Italia Spa | Process for preparing tricyclohexyltin derivatives |
| IT1002391B (it) * | 1973-12-28 | 1976-05-20 | Oxon Italia Spa | Procedimento per la preparazione di tricicloesilstagno derivati |
| IT1038754B (it) * | 1975-06-06 | 1979-11-30 | Oxon Italia Spa | Procedimento continuo per la produzione di cicloesilmagnesioaloge nuri |
| US4174346A (en) * | 1976-01-30 | 1979-11-13 | Albright & Wilson Limited | Process for preparing organotin compounds |
| DD134529A1 (de) * | 1978-01-09 | 1979-03-07 | Alfred Tzschach | Verfahren zur herstellung von tricyclohexylzinnverbindungen |
-
1979
- 1979-06-27 IT IT23893/79A patent/IT1121958B/it active
-
1980
- 1980-05-20 US US06/151,594 patent/US4330477A/en not_active Expired - Lifetime
- 1980-06-11 IL IL60297A patent/IL60297A/xx unknown
- 1980-06-12 NL NL8003407A patent/NL8003407A/nl not_active Application Discontinuation
- 1980-06-17 CH CH469980A patent/CH646708A5/it not_active IP Right Cessation
- 1980-06-20 DE DE19803023149 patent/DE3023149A1/de active Granted
- 1980-06-23 FR FR8013842A patent/FR2459804B1/fr not_active Expired
- 1980-06-23 BE BE0/201136A patent/BE883956A/fr not_active IP Right Cessation
- 1980-06-24 BR BR8003920A patent/BR8003920A/pt not_active IP Right Cessation
- 1980-06-25 GB GB8020843A patent/GB2053224B/en not_active Expired
- 1980-06-26 AR AR281551A patent/AR220847A1/es active
- 1980-06-26 SE SE8004716A patent/SE450833B/sv not_active IP Right Cessation
- 1980-06-26 AT AT0335280A patent/AT379813B/de not_active IP Right Cessation
- 1980-06-26 CA CA000354891A patent/CA1136150A/en not_active Expired
- 1980-06-26 SU SU802938601A patent/SU1213987A3/ru active
- 1980-06-26 MX MX182919A patent/MX155945A/es unknown
- 1980-06-26 ES ES492809A patent/ES8105739A1/es not_active Expired
- 1980-06-27 YU YU1692/80A patent/YU40881B/xx unknown
- 1980-06-27 DK DK280880A patent/DK280880A/da not_active Application Discontinuation
- 1980-06-27 JP JP8768780A patent/JPS5639095A/ja active Granted
- 1980-06-27 AU AU59730/80A patent/AU538683B2/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| AR220847A1 (es) | 1980-11-28 |
| DE3023149C2 (es) | 1989-07-13 |
| IT1121958B (it) | 1986-04-23 |
| ES492809A0 (es) | 1981-06-01 |
| FR2459804A1 (fr) | 1981-01-16 |
| IL60297A (en) | 1984-11-30 |
| CH646708A5 (it) | 1984-12-14 |
| SE450833B (sv) | 1987-08-03 |
| JPS5639095A (en) | 1981-04-14 |
| DK280880A (da) | 1980-12-28 |
| ATA335280A (de) | 1985-07-15 |
| FR2459804B1 (fr) | 1986-06-13 |
| GB2053224B (en) | 1983-07-13 |
| JPS6352630B2 (es) | 1988-10-19 |
| IT7923893A0 (it) | 1979-06-27 |
| CA1136150A (en) | 1982-11-23 |
| BE883956A (fr) | 1980-10-16 |
| AU5973080A (en) | 1981-01-08 |
| GB2053224A (en) | 1981-02-04 |
| DE3023149A1 (de) | 1981-01-08 |
| YU169280A (en) | 1983-10-31 |
| SE8004716L (sv) | 1980-12-28 |
| AT379813B (de) | 1986-03-10 |
| SU1213987A3 (ru) | 1986-02-23 |
| AU538683B2 (en) | 1984-08-23 |
| BR8003920A (pt) | 1981-01-27 |
| US4330477A (en) | 1982-05-18 |
| MX155945A (es) | 1988-05-27 |
| YU40881B (en) | 1986-08-31 |
| NL8003407A (nl) | 1980-12-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FD1A | Patent lapsed |
Effective date: 19970401 |