ES472171A1 - Procedimiento para la obtencion de silicatos insolubles en agua - Google Patents
Procedimiento para la obtencion de silicatos insolubles en aguaInfo
- Publication number
- ES472171A1 ES472171A1 ES472171A ES472171A ES472171A1 ES 472171 A1 ES472171 A1 ES 472171A1 ES 472171 A ES472171 A ES 472171A ES 472171 A ES472171 A ES 472171A ES 472171 A1 ES472171 A1 ES 472171A1
- Authority
- ES
- Spain
- Prior art keywords
- water
- silicate compound
- temperature
- suspension
- al2o3
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000002245 particle Substances 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- 238000001228 spectrum Methods 0.000 title abstract 2
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 title 1
- -1 alkali metal aluminate Chemical class 0.000 abstract 7
- 239000000725 suspension Substances 0.000 abstract 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 4
- 229910052593 corundum Inorganic materials 0.000 abstract 4
- 229910001845 yogo sapphire Inorganic materials 0.000 abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- 102000005701 Calcium-Binding Proteins Human genes 0.000 abstract 2
- 108010045403 Calcium-Binding Proteins Proteins 0.000 abstract 2
- 238000013019 agitation Methods 0.000 abstract 2
- 229910052783 alkali metal Inorganic materials 0.000 abstract 2
- 229910052681 coesite Inorganic materials 0.000 abstract 2
- 229910052906 cristobalite Inorganic materials 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000000377 silicon dioxide Substances 0.000 abstract 2
- 235000012239 silicon dioxide Nutrition 0.000 abstract 2
- 229910052682 stishovite Inorganic materials 0.000 abstract 2
- 229910052905 tridymite Inorganic materials 0.000 abstract 2
- 239000013543 active substance Substances 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 229910052910 alkali metal silicate Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 229910000323 aluminium silicate Inorganic materials 0.000 abstract 1
- 239000003599 detergent Substances 0.000 abstract 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 1
- 230000009969 flowable effect Effects 0.000 abstract 1
- 238000009472 formulation Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000376 reactant Substances 0.000 abstract 1
- 238000010998 test method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/26—Aluminium-containing silicates, i.e. silico-aluminates
- C01B33/28—Base exchange silicates, e.g. zeolites
- C01B33/2807—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures
- C01B33/2815—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures of type A (UNION CARBIDE trade name; corresponds to GRACE's types Z-12 or Z-12L)
- C01B33/2823—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures of type A (UNION CARBIDE trade name; corresponds to GRACE's types Z-12 or Z-12L) from aqueous solutions of an alkali metal aluminate and an alkali metal silicate excluding any other source of alumina or silica
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/128—Aluminium silicates, e.g. zeolites
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S423/00—Chemistry of inorganic compounds
- Y10S423/24—LTA, e.g. A, alpha, ZK-4, ZK-21, ZK-22
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Materials Engineering (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Detergent Compositions (AREA)
Abstract
Procedimiento para la obtención de silicatos insolubles en agua, de partícula fina, capacitados para el intercambio de cationes y para la ulterior elaboración a agentes de lavado y de limpieza, de fórmula general (Na20)0,8 - 1,3 . (A1203) . (Si0s) 1,75 - 2,0 por mezcla de aluminato alcalino disuelto en agua con silicato de sodio disuelto en agua en presencia de álcali en exceso, caracterizado porque las soluciones acuosas, cuya composición total calculada corresponde con respecto a su contenido en Al203 y su contenido en Si02 a la fórmula arriba indicada y especialmente a la composición del producto deseado, pero que en total presenta 3,2-4, 4 moles de Na20 por mol de Al203 y 70 - 85 moles de agua por mol de Al203 de la fórmula, se mezcla rápidamente bajo agitación presentándose la solución de silicato sódico y después dejando la suspensión obtenida durante breve tiempo bajo agitación a esta temperatura antes de efectuar a temperatura más elevada la etapa de cristalización.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19772734296 DE2734296A1 (de) | 1977-07-29 | 1977-07-29 | Verfahren zur herstellung von feinteiligen, zum kationenaustausch befaehigten wasserunloeslichen silikaten |
Publications (1)
Publication Number | Publication Date |
---|---|
ES472171A1 true ES472171A1 (es) | 1979-02-16 |
Family
ID=6015178
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES472171A Expired ES472171A1 (es) | 1977-07-29 | 1978-07-28 | Procedimiento para la obtencion de silicatos insolubles en agua |
Country Status (14)
Country | Link |
---|---|
US (1) | US4271135A (es) |
JP (1) | JPS6049133B2 (es) |
AT (1) | AT366013B (es) |
BE (1) | BE869348A (es) |
BR (1) | BR7804876A (es) |
CA (1) | CA1117733A (es) |
CH (1) | CH637352A5 (es) |
DE (1) | DE2734296A1 (es) |
ES (1) | ES472171A1 (es) |
FR (1) | FR2398697A1 (es) |
GB (1) | GB2002335B (es) |
IT (1) | IT1097166B (es) |
NL (1) | NL7807197A (es) |
SE (1) | SE437977B (es) |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5710392Y2 (es) * | 1977-07-04 | 1982-02-27 | ||
US4576986A (en) * | 1978-01-31 | 1986-03-18 | J. M. Huber Corporation | Rubber compositions containing small particle size zeolites and mixtures |
US4888378A (en) * | 1978-12-20 | 1989-12-19 | J. M. Huber Corporation | Plastic compositions containing small particle size zeolites and mixtures |
US4612342A (en) * | 1978-12-20 | 1986-09-16 | J. M. Huber Corporation | Rubber compositions containing small particle size zeolites |
DE3007080A1 (de) * | 1980-02-26 | 1981-09-10 | Degussa Ag, 6000 Frankfurt | Verfahren zur herstellung von kristallinem zeolithpulver des typs a |
DE3007087A1 (de) * | 1980-02-26 | 1981-09-10 | Degussa Ag, 6000 Frankfurt | Verfahren zur herstellung von zeolith a |
DE3007123A1 (de) * | 1980-02-26 | 1981-09-10 | Degussa Ag, 6000 Frankfurt | Verfahren zur herstellung von zeolith a |
DE3007044A1 (de) * | 1980-02-26 | 1981-09-10 | Degussa Ag, 6000 Frankfurt | Verfahren zur herstellung von kristallinem zeolith a |
FR2528722A1 (fr) * | 1982-06-18 | 1983-12-23 | Rhone Poulenc Chim Base | Zeolite comme auxiliaire de detergence |
US4540559A (en) * | 1983-08-22 | 1985-09-10 | Rhone-Poulenc Specialites Chimiques | Preparation of type Y zeolites |
DE3444311A1 (de) * | 1984-12-05 | 1986-06-05 | Degussa Ag, 6000 Frankfurt | Waessrige stabile suspension wasserunloeslicher, zum binden von calciumionen befaehigter silikate und deren verwendung zur herstellung von wasch- und reinigungsmitteln |
DE3806932A1 (de) * | 1988-03-03 | 1989-09-14 | Vaw Ver Aluminium Werke Ag | Verfahren zur modifizierung eines zeoliths |
US5443812A (en) * | 1989-04-24 | 1995-08-22 | Kanebo Ltd. | Stabilized synthetic zeolite and a process for the preparation thereof |
JPH0318146U (es) * | 1990-04-11 | 1991-02-22 | ||
DE4309656A1 (de) * | 1993-03-25 | 1994-09-29 | Henkel Kgaa | Verfahren zur Herstellung von feinstteiligen zeolithischen Alkalimetallaluminiumsilicaten |
FR2750973B1 (fr) * | 1996-07-12 | 1998-10-30 | Ceca Sa | Utilisation d'un reacteur agite par un systeme du type vis d'archimede pour la synthese de faujasite lsx |
US6413492B1 (en) * | 2000-03-23 | 2002-07-02 | Engelhard Corporation | Method of forming high aluminum aluminosilicate zeolites |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2882243A (en) * | 1953-12-24 | 1959-04-14 | Union Carbide Corp | Molecular sieve adsorbents |
US3058805A (en) * | 1958-10-03 | 1962-10-16 | Bayer Ag | Process for the production of sodium zeolite a |
FR1240756A (fr) * | 1958-10-03 | 1960-09-09 | Bayer Ag | Procédé de préparation de zéolite sodique synthétique |
FR1536947A (fr) * | 1967-03-01 | 1968-09-02 | Mines Domaniales De Potasse | Zéolites synthétiques et leur procédé de fabrication |
AR208392A1 (es) * | 1973-05-07 | 1976-12-27 | Henkel & Cie Gmbh | Composicion para lavar blanquear o limpiar materiales resistentes especialmente textiles adicional a la patente no 201687 adicional a la no 253286 |
US3985669A (en) * | 1974-06-17 | 1976-10-12 | The Procter & Gamble Company | Detergent compositions |
US4041135A (en) * | 1975-07-25 | 1977-08-09 | J. M. Huber Corporation | Production of high capacity inorganic crystalline base exchange materials |
US4102977A (en) * | 1975-11-18 | 1978-07-25 | Mizusawa Kagaku Kogyo Kabushiki Kaisha | Process for the preparation of alkali aluminosilicate detergent builder |
AT356628B (de) * | 1976-02-06 | 1980-05-12 | Henkel Kgaa | Verfahren zur herstellung waesseriger, zur weiterverarbeitung zu wasch- und reinigungs- mitteln geeigneter suspensionen von fein- teiligen, zum kationenaustausch befaehigten, noch gebundenes wasser enthaltenden wasser- unloeslichen silikaten |
DE2651445A1 (de) * | 1976-11-11 | 1978-05-18 | Degussa | Kristallines zeolithpulver des typs a ii |
-
1977
- 1977-07-29 DE DE19772734296 patent/DE2734296A1/de active Granted
-
1978
- 1978-07-03 SE SE7807490A patent/SE437977B/sv not_active IP Right Cessation
- 1978-07-03 NL NL7807197A patent/NL7807197A/xx not_active Application Discontinuation
- 1978-07-17 IT IT25781/78A patent/IT1097166B/it active
- 1978-07-25 CA CA000308064A patent/CA1117733A/en not_active Expired
- 1978-07-27 FR FR7822205A patent/FR2398697A1/fr active Granted
- 1978-07-28 ES ES472171A patent/ES472171A1/es not_active Expired
- 1978-07-28 JP JP53093084A patent/JPS6049133B2/ja not_active Expired
- 1978-07-28 GB GB7831471A patent/GB2002335B/en not_active Expired
- 1978-07-28 BE BE189563A patent/BE869348A/xx not_active IP Right Cessation
- 1978-07-28 CH CH816878A patent/CH637352A5/de not_active IP Right Cessation
- 1978-07-28 BR BR7804876A patent/BR7804876A/pt unknown
- 1978-07-28 AT AT0549678A patent/AT366013B/de not_active IP Right Cessation
-
1979
- 1979-10-04 US US06/081,824 patent/US4271135A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
AT366013B (de) | 1982-03-10 |
IT7825781A0 (it) | 1978-07-17 |
US4271135A (en) | 1981-06-02 |
FR2398697A1 (fr) | 1979-02-23 |
JPS6049133B2 (ja) | 1985-10-31 |
CA1117733A (en) | 1982-02-09 |
NL7807197A (nl) | 1979-01-31 |
BR7804876A (pt) | 1979-04-24 |
DE2734296C2 (es) | 1988-05-11 |
IT1097166B (it) | 1985-08-26 |
FR2398697B1 (es) | 1981-07-24 |
JPS5426299A (en) | 1979-02-27 |
CH637352A5 (de) | 1983-07-29 |
SE437977B (sv) | 1985-03-25 |
ATA549678A (de) | 1981-07-15 |
DE2734296A1 (de) | 1979-02-08 |
GB2002335B (en) | 1982-03-03 |
SE7807490L (sv) | 1979-01-30 |
GB2002335A (en) | 1979-02-21 |
BE869348A (fr) | 1979-01-29 |
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