ES2641533T3 - Procedimiento de ensamblaje de un supercondensador híbrido con litio - Google Patents
Procedimiento de ensamblaje de un supercondensador híbrido con litio Download PDFInfo
- Publication number
- ES2641533T3 ES2641533T3 ES12725858.0T ES12725858T ES2641533T3 ES 2641533 T3 ES2641533 T3 ES 2641533T3 ES 12725858 T ES12725858 T ES 12725858T ES 2641533 T3 ES2641533 T3 ES 2641533T3
- Authority
- ES
- Spain
- Prior art keywords
- porous carbon
- stage
- lithium
- negative electrode
- carbon material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000000034 method Methods 0.000 title claims description 45
- 229910052744 lithium Inorganic materials 0.000 title claims description 31
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 title claims description 30
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 73
- KMTRUDSVKNLOMY-UHFFFAOYSA-N Ethylene carbonate Chemical compound O=C1OCCO1 KMTRUDSVKNLOMY-UHFFFAOYSA-N 0.000 claims description 42
- 239000003792 electrolyte Substances 0.000 claims description 39
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 claims description 31
- 239000000203 mixture Substances 0.000 claims description 28
- 229910003473 lithium bis(trifluoromethanesulfonyl)imide Inorganic materials 0.000 claims description 27
- QSZMZKBZAYQGRS-UHFFFAOYSA-N lithium;bis(trifluoromethylsulfonyl)azanide Chemical compound [Li+].FC(F)(F)S(=O)(=O)[N-]S(=O)(=O)C(F)(F)F QSZMZKBZAYQGRS-UHFFFAOYSA-N 0.000 claims description 27
- 239000003575 carbonaceous material Substances 0.000 claims description 24
- 239000002904 solvent Substances 0.000 claims description 22
- 239000011244 liquid electrolyte Substances 0.000 claims description 20
- 229910003002 lithium salt Inorganic materials 0.000 claims description 20
- 159000000002 lithium salts Chemical class 0.000 claims description 20
- 239000006229 carbon black Substances 0.000 claims description 17
- 235000019241 carbon black Nutrition 0.000 claims description 17
- 239000010439 graphite Substances 0.000 claims description 17
- 229910002804 graphite Inorganic materials 0.000 claims description 17
- 229910001416 lithium ion Inorganic materials 0.000 claims description 16
- 229910001290 LiPF6 Inorganic materials 0.000 claims description 14
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 claims description 13
- 230000015572 biosynthetic process Effects 0.000 claims description 12
- 230000002045 lasting effect Effects 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 9
- 229910052799 carbon Inorganic materials 0.000 claims description 8
- RCIJMMSZBQEWKW-UHFFFAOYSA-N methyl propan-2-yl carbonate Chemical compound COC(=O)OC(C)C RCIJMMSZBQEWKW-UHFFFAOYSA-N 0.000 claims description 7
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 claims description 6
- 239000011230 binding agent Substances 0.000 claims description 6
- RUOJZAUFBMNUDX-UHFFFAOYSA-N propylene carbonate Chemical compound CC1COC(=O)O1 RUOJZAUFBMNUDX-UHFFFAOYSA-N 0.000 claims description 6
- OIFBSDVPJOWBCH-UHFFFAOYSA-N Diethyl carbonate Chemical compound CCOC(=O)OCC OIFBSDVPJOWBCH-UHFFFAOYSA-N 0.000 claims description 5
- 239000002041 carbon nanotube Substances 0.000 claims description 5
- 229910021393 carbon nanotube Inorganic materials 0.000 claims description 5
- VDVLPSWVDYJFRW-UHFFFAOYSA-N lithium;bis(fluorosulfonyl)azanide Chemical compound [Li+].FS(=O)(=O)[N-]S(F)(=O)=O VDVLPSWVDYJFRW-UHFFFAOYSA-N 0.000 claims description 5
- 229920000049 Carbon (fiber) Polymers 0.000 claims description 4
- 239000004917 carbon fiber Substances 0.000 claims description 4
- 238000011068 loading method Methods 0.000 claims description 4
- 229910010941 LiFSI Inorganic materials 0.000 claims description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 3
- 229910021401 carbide-derived carbon Inorganic materials 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 229910052760 oxygen Inorganic materials 0.000 claims description 3
- 239000001301 oxygen Substances 0.000 claims description 3
- 241000234282 Allium Species 0.000 claims description 2
- 235000002732 Allium cepa var. cepa Nutrition 0.000 claims description 2
- 125000005910 alkyl carbonate group Chemical group 0.000 claims description 2
- 239000000571 coke Substances 0.000 claims description 2
- 150000002148 esters Chemical class 0.000 claims description 2
- 150000003949 imides Chemical class 0.000 claims description 2
- 150000002596 lactones Chemical class 0.000 claims description 2
- 239000011148 porous material Substances 0.000 claims description 2
- 239000007773 negative electrode material Substances 0.000 claims 1
- 239000007774 positive electrode material Substances 0.000 claims 1
- 230000000052 comparative effect Effects 0.000 description 20
- 238000009830 intercalation Methods 0.000 description 16
- 230000002687 intercalation Effects 0.000 description 15
- 238000003780 insertion Methods 0.000 description 13
- 230000037431 insertion Effects 0.000 description 13
- 239000002033 PVDF binder Substances 0.000 description 12
- 229920002981 polyvinylidene fluoride Polymers 0.000 description 12
- 239000002131 composite material Substances 0.000 description 11
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 10
- 229910052782 aluminium Inorganic materials 0.000 description 10
- 239000011248 coating agent Substances 0.000 description 10
- 238000000576 coating method Methods 0.000 description 10
- 238000002161 passivation Methods 0.000 description 10
- 150000001875 compounds Chemical class 0.000 description 8
- 239000000047 product Substances 0.000 description 8
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 6
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
- 230000001351 cycling effect Effects 0.000 description 6
- 230000007423 decrease Effects 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- HNAGHMKIPMKKBB-UHFFFAOYSA-N 1-benzylpyrrolidine-3-carboxamide Chemical compound C1C(C(=O)N)CCN1CC1=CC=CC=C1 HNAGHMKIPMKKBB-UHFFFAOYSA-N 0.000 description 5
- OBNCKNCVKJNDBV-UHFFFAOYSA-N butanoic acid ethyl ester Natural products CCCC(=O)OCC OBNCKNCVKJNDBV-UHFFFAOYSA-N 0.000 description 5
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 4
- 229910052802 copper Inorganic materials 0.000 description 4
- 239000010949 copper Substances 0.000 description 4
- XTHFKEDIFFGKHM-UHFFFAOYSA-N Dimethoxyethane Chemical compound COCCOC XTHFKEDIFFGKHM-UHFFFAOYSA-N 0.000 description 3
- 239000003990 capacitor Substances 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- 230000003247 decreasing effect Effects 0.000 description 3
- 238000009713 electroplating Methods 0.000 description 3
- 238000004146 energy storage Methods 0.000 description 3
- -1 lithium ionic compound Chemical class 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- BJWMSGRKJIOCNR-UHFFFAOYSA-N 4-ethenyl-1,3-dioxolan-2-one Chemical group C=CC1COC(=O)O1 BJWMSGRKJIOCNR-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 2
- 238000004769 chrono-potentiometry Methods 0.000 description 2
- FKRCODPIKNYEAC-UHFFFAOYSA-N ethyl propionate Chemical compound CCOC(=O)CC FKRCODPIKNYEAC-UHFFFAOYSA-N 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 description 1
- 238000004438 BET method Methods 0.000 description 1
- 206010014415 Electrolyte depletion Diseases 0.000 description 1
- JGFBQFKZKSSODQ-UHFFFAOYSA-N Isothiocyanatocyclopropane Chemical compound S=C=NC1CC1 JGFBQFKZKSSODQ-UHFFFAOYSA-N 0.000 description 1
- 229910052493 LiFePO4 Inorganic materials 0.000 description 1
- 229910012219 LiPFa Inorganic materials 0.000 description 1
- 239000006230 acetylene black Substances 0.000 description 1
- 125000005907 alkyl ester group Chemical group 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 125000003180 beta-lactone group Chemical group 0.000 description 1
- PWLNAUNEAKQYLH-UHFFFAOYSA-N butyric acid octyl ester Natural products CCCCCCCCOC(=O)CCC PWLNAUNEAKQYLH-UHFFFAOYSA-N 0.000 description 1
- 238000003490 calendering Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 150000001993 dienes Chemical class 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000012983 electrochemical energy storage Methods 0.000 description 1
- 239000007772 electrode material Substances 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 238000011066 ex-situ storage Methods 0.000 description 1
- 238000004299 exfoliation Methods 0.000 description 1
- 125000000457 gamma-lactone group Chemical group 0.000 description 1
- 150000008040 ionic compounds Chemical class 0.000 description 1
- 239000002608 ionic liquid Substances 0.000 description 1
- KQNPFQTWMSNSAP-UHFFFAOYSA-M isobutyrate Chemical compound CC(C)C([O-])=O KQNPFQTWMSNSAP-UHFFFAOYSA-M 0.000 description 1
- 239000003273 ketjen black Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- UUIQMZJEGPQKFD-UHFFFAOYSA-N n-butyric acid methyl ester Natural products CCCC(=O)OC UUIQMZJEGPQKFD-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000006259 organic additive Substances 0.000 description 1
- 239000005486 organic electrolyte Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 229910001868 water Inorganic materials 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/84—Processes for the manufacture of hybrid or EDL capacitors, or components thereof
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/54—Electrolytes
- H01G11/58—Liquid electrolytes
- H01G11/62—Liquid electrolytes characterised by the solute, e.g. salts, anions or cations therein
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/13—Energy storage using capacitors
Landscapes
- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Manufacturing & Machinery (AREA)
- Secondary Cells (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Electric Double-Layer Capacitors Or The Like (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1155048 | 2011-06-09 | ||
| FR1155048 | 2011-06-09 | ||
| PCT/FR2012/050837 WO2012172211A1 (fr) | 2011-06-09 | 2012-04-17 | Procede d'assemblage d'un supercondensateur hybride au lithium |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2641533T3 true ES2641533T3 (es) | 2017-11-10 |
Family
ID=46208615
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES12725858.0T Active ES2641533T3 (es) | 2011-06-09 | 2012-04-17 | Procedimiento de ensamblaje de un supercondensador híbrido con litio |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US9136066B2 (https=) |
| EP (1) | EP2718944B1 (https=) |
| JP (1) | JP6067003B2 (https=) |
| KR (1) | KR101985789B1 (https=) |
| CN (1) | CN103733290B (https=) |
| AU (1) | AU2012270250B2 (https=) |
| BR (1) | BR112013031315A2 (https=) |
| CA (1) | CA2835124C (https=) |
| ES (1) | ES2641533T3 (https=) |
| IL (1) | IL229655A (https=) |
| RU (1) | RU2591846C2 (https=) |
| UA (1) | UA110650C2 (https=) |
| WO (1) | WO2012172211A1 (https=) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2014225574A (ja) * | 2013-05-16 | 2014-12-04 | 住友電気工業株式会社 | キャパシタおよびその充放電方法 |
| WO2016081525A1 (en) * | 2014-11-20 | 2016-05-26 | Coors Tek Fluorochemicals, Inc. | Concentrated electrolyte solution |
| JP2017139435A (ja) * | 2016-01-29 | 2017-08-10 | 日本ケミコン株式会社 | 電極、電極を用いたキャパシタ、および電極の製造方法 |
| WO2017131016A1 (ja) * | 2016-01-29 | 2017-08-03 | 日本ケミコン株式会社 | 電極、電極を用いたキャパシタ、および電極の製造方法 |
| US10770716B2 (en) * | 2016-06-08 | 2020-09-08 | Envision Aesc Japan Ltd. | Non-aqueous electrolyte secondary battery |
| US10600583B1 (en) | 2018-08-30 | 2020-03-24 | King Saud University | Method of making a porous nitrogen-doped carbon electrode from biomass |
| FR3117888B1 (fr) * | 2020-12-17 | 2023-08-25 | Sweetch Energy | Dispositif de production d’energie par gradient de salinite comprenant des electrodes d’un textile de charbon actif |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4618929B2 (ja) * | 2000-05-09 | 2011-01-26 | 三菱化学株式会社 | 電気二重層キャパシタ用活性炭 |
| CA2327370A1 (fr) * | 2000-12-05 | 2002-06-05 | Hydro-Quebec | Nouvelle methode de fabrication de li4ti5o12 pur a partir du compose ternaire tix-liy-carbone: effet du carbone sur la synthese et la conductivite de l'electrode |
| AU2002244957B2 (en) | 2001-06-29 | 2005-07-21 | Subaru Corporation | Organic electrolyte capacitor |
| US7049032B2 (en) * | 2001-07-25 | 2006-05-23 | Asahi Glass Company, Limited | Secondary power source |
| KR100534845B1 (ko) * | 2003-12-30 | 2005-12-08 | 현대자동차주식회사 | 나노 크기의 금속산화물 전극의 제조 방법 |
| JP2006024785A (ja) * | 2004-07-08 | 2006-01-26 | Tomiyama Pure Chemical Industries Ltd | 電気二重層キャパシタ用非水電解液及び電気二重層キャパシタ |
| EP1879252A4 (en) * | 2005-04-19 | 2010-06-23 | Panasonic Corp | WATER-FREE ELECTROLYTE SOLUTION, ELECTROCHEMICAL ENERGY STORAGE DEVICE THEREFOR AND SECONDARY BATTERY WITH A WATER-FREE ELECTROLYTE |
| RU2391732C2 (ru) * | 2005-06-24 | 2010-06-10 | ЮНИВЕРСАЛ СУПЕРКАПАСИТОРЗ ЭлЭлСи | Гетерогенный электрохимический суперконденсатор и способ изготовления |
| JP2007299569A (ja) * | 2006-04-28 | 2007-11-15 | Matsushita Electric Ind Co Ltd | 電気化学エネルギー蓄積デバイス |
| JP2008177263A (ja) | 2007-01-17 | 2008-07-31 | Sanyo Electric Co Ltd | 活性炭電極及びその製造方法並びに電気二重層キャパシタ及びハイブリッドキャパシタ |
| JP4918418B2 (ja) * | 2007-06-13 | 2012-04-18 | アドバンスト・キャパシタ・テクノロジーズ株式会社 | リチウムイオンのプレドープ方法およびリチウムイオン・キャパシタ蓄電素子の製造方法 |
| CN100595965C (zh) * | 2007-06-28 | 2010-03-24 | 比亚迪股份有限公司 | 一种锂离子二次电池的化成方法 |
| FR2935547B1 (fr) * | 2008-08-29 | 2011-03-25 | Commissariat Energie Atomique | Electrolytes liquides ioniques et dispositifs electrochimiques tels que des accumulateurs les comprenant. |
| CN102171869B (zh) * | 2008-11-10 | 2016-01-20 | 株式会社爱考斯研究 | 二次电池用正极以及采用该正极的二次电池、和集电体以及采用该集电体的电池 |
| JP2010205846A (ja) * | 2009-03-02 | 2010-09-16 | Asahi Kasei Corp | 非水系リチウム型蓄電素子 |
-
2012
- 2012-04-17 AU AU2012270250A patent/AU2012270250B2/en not_active Ceased
- 2012-04-17 CA CA2835124A patent/CA2835124C/fr not_active Expired - Fee Related
- 2012-04-17 RU RU2013158932/07A patent/RU2591846C2/ru not_active IP Right Cessation
- 2012-04-17 CN CN201280028163.XA patent/CN103733290B/zh not_active Expired - Fee Related
- 2012-04-17 ES ES12725858.0T patent/ES2641533T3/es active Active
- 2012-04-17 UA UAA201400113A patent/UA110650C2/uk unknown
- 2012-04-17 WO PCT/FR2012/050837 patent/WO2012172211A1/fr not_active Ceased
- 2012-04-17 JP JP2014514126A patent/JP6067003B2/ja not_active Expired - Fee Related
- 2012-04-17 US US14/119,570 patent/US9136066B2/en not_active Expired - Fee Related
- 2012-04-17 KR KR1020147000680A patent/KR101985789B1/ko not_active Expired - Fee Related
- 2012-04-17 BR BR112013031315A patent/BR112013031315A2/pt active Search and Examination
- 2012-04-17 EP EP12725858.0A patent/EP2718944B1/fr not_active Not-in-force
-
2013
- 2013-11-27 IL IL229655A patent/IL229655A/en active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| RU2591846C2 (ru) | 2016-07-20 |
| EP2718944A1 (fr) | 2014-04-16 |
| JP2014520395A (ja) | 2014-08-21 |
| RU2013158932A (ru) | 2015-07-20 |
| CN103733290A (zh) | 2014-04-16 |
| UA110650C2 (uk) | 2016-01-25 |
| US9136066B2 (en) | 2015-09-15 |
| EP2718944B1 (fr) | 2017-08-02 |
| CN103733290B (zh) | 2017-06-30 |
| KR20140073479A (ko) | 2014-06-16 |
| BR112013031315A2 (pt) | 2016-11-29 |
| KR101985789B1 (ko) | 2019-06-04 |
| JP6067003B2 (ja) | 2017-01-25 |
| WO2012172211A1 (fr) | 2012-12-20 |
| US20140325807A1 (en) | 2014-11-06 |
| CA2835124C (fr) | 2019-06-25 |
| IL229655A (en) | 2017-06-29 |
| AU2012270250B2 (en) | 2016-07-21 |
| CA2835124A1 (fr) | 2012-12-20 |
| AU2012270250A1 (en) | 2013-12-12 |
| IL229655A0 (en) | 2014-01-30 |
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