ES2177193T3 - Metodo para la produccion de acido nitrico. - Google Patents
Metodo para la produccion de acido nitrico.Info
- Publication number
- ES2177193T3 ES2177193T3 ES99125583T ES99125583T ES2177193T3 ES 2177193 T3 ES2177193 T3 ES 2177193T3 ES 99125583 T ES99125583 T ES 99125583T ES 99125583 T ES99125583 T ES 99125583T ES 2177193 T3 ES2177193 T3 ES 2177193T3
- Authority
- ES
- Spain
- Prior art keywords
- nitric acid
- gaseous
- zone
- nitric
- production
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/20—Nitrogen oxides; Oxyacids of nitrogen; Salts thereof
- C01B21/24—Nitric oxide (NO)
- C01B21/26—Preparation by catalytic or non-catalytic oxidation of ammonia
- C01B21/262—Preparation by catalytic or non-catalytic oxidation of ammonia obtaining nitrogen dioxide or tetroxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/20—Nitrogen oxides; Oxyacids of nitrogen; Salts thereof
- C01B21/38—Nitric acid
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/20—Nitrogen oxides; Oxyacids of nitrogen; Salts thereof
- C01B21/38—Nitric acid
- C01B21/40—Preparation by absorption of oxides of nitrogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Treating Waste Gases (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Gas Separation By Absorption (AREA)
Abstract
Un procedimiento mejorado para producir ácido nítrico por oxidación de amoníaco gaseoso para formar tetróxido de dinitrógeno gaseoso, haciendo reaccionar el tetróxido de dinitrógeno con agua en una zona de absorción para formar ácido nítrico acuoso y óxido nítrico gaseoso, separando la corriente ácido nítrico/óxido nítrico de la zona de absorción y alimentando la corriente a una zona de blanqueo del ácido nítrico, eliminando las impurezas del ácido nítrico en la zona de blanqueo para formar ácido nítrico producto y añadiendo oxígeno gaseoso suplementario a una o más de las corrientes de reacción para aumentar la producción de ácido nítrico y/o su concentración, consistiendo la mejora en inyectar el oxígeno suplementario en una corriente del procedimiento que contiene ácido nítrico para formar en ella una mezcla de burbujas de gas/líquido que consiste en una dispersión fina de burbujas de gas que tienen diámetros de menos de aproximadamente 0,1 mm y que de ese modo proporcionan una mayor superficie interfacial entre las burbujas de gas y la mezcla líquida.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US09/220,818 US6165435A (en) | 1998-12-24 | 1998-12-24 | Method and production of nitric acid |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2177193T3 true ES2177193T3 (es) | 2002-12-01 |
Family
ID=22825105
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES99125583T Expired - Lifetime ES2177193T3 (es) | 1998-12-24 | 1999-12-21 | Metodo para la produccion de acido nitrico. |
Country Status (9)
Country | Link |
---|---|
US (1) | US6165435A (es) |
EP (1) | EP1013604B1 (es) |
KR (1) | KR100501462B1 (es) |
CN (1) | CN1157329C (es) |
BR (1) | BR9905929A (es) |
CA (1) | CA2293004C (es) |
DE (1) | DE69902139T2 (es) |
ES (1) | ES2177193T3 (es) |
ID (1) | ID24018A (es) |
Families Citing this family (33)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7410626B2 (en) * | 2003-09-10 | 2008-08-12 | Basf Catalysts Llc | Layered ammonia oxidation catalyst |
DE102005023161A1 (de) * | 2005-05-19 | 2006-11-23 | Siemens Ag | Verfahren und Anlage zur Herstellung von Salpetersäure |
CN100396360C (zh) * | 2006-04-24 | 2008-06-25 | 南京大学 | 一种工业过程氮氧化物(nox)废气治理及资源化的方法 |
BRPI0801209B1 (pt) * | 2008-04-14 | 2017-07-04 | White Martins Gases Industriais Ltda. | Ethanol fermentation system |
EP2687086B1 (en) * | 2008-07-24 | 2016-09-14 | Geno LLC | Methods for diagnosing and treating a heart condition in a patient |
UA91614C2 (uk) * | 2008-11-28 | 2010-08-10 | Іван Іванович Барабаш | Спосіб виробництва азотної кислоти (варіанти) і агрегат для виробництва азотної кислоти |
CN101575089B (zh) * | 2009-06-10 | 2010-12-29 | 上海化工研究院 | 一种18o-硝酸的制备方法 |
CN101837961B (zh) * | 2010-05-25 | 2012-08-22 | 安徽淮化股份有限公司 | 一种符合节能减排及低成本配制稀硝酸的方法及装置 |
BR112013013700B1 (pt) * | 2010-12-01 | 2020-04-07 | Orica Int Pte Ltd | processo para a produção de ácido nítrico |
CN102491292A (zh) * | 2011-12-06 | 2012-06-13 | 中国成达工程有限公司 | 一种低消耗、低排放的硝酸生产方法及其生产设备 |
KR102037702B1 (ko) | 2012-03-05 | 2019-10-29 | 바스프 에스이 | 내부 필터 요소를 갖는 암모니아 산화 반응기 |
CN103112835B (zh) * | 2012-11-11 | 2014-11-26 | 安徽金禾实业股份有限公司 | 一种浓硝酸生产过程中的间接漂白方法 |
DE102013002201A1 (de) * | 2013-02-07 | 2014-08-07 | Messer Austria Gmbh | Verfahren und Produktionsanlage zum Herstellen von Salpetersäure |
DE102013004341A1 (de) * | 2013-03-14 | 2014-09-18 | Thyssenkrupp Uhde Gmbh | Verfahren zur Oxidation von Ammoniak und dafür geeignete Anlage |
CN103395759B (zh) * | 2013-08-02 | 2015-01-14 | 柳州化工股份有限公司 | 一种配制硝酸水溶液脱色方法 |
CN103395758B (zh) * | 2013-08-02 | 2015-03-25 | 柳州化工股份有限公司 | 一种配制硝酸水溶液的装置 |
DE102014006017B4 (de) | 2014-04-23 | 2022-04-21 | Messer Group Gmbh | Verfahren und Vorrichtung zum Herstellen von Salpetersäure |
KR101669976B1 (ko) * | 2014-11-27 | 2016-11-09 | 휴켐스주식회사 | 질산의 제조방법 |
CN105134560A (zh) * | 2015-08-23 | 2015-12-09 | 安徽金禾实业股份有限公司 | 硝酸生产中对压缩机进口空气进行冷冻脱湿的方法 |
DE102015014185A1 (de) | 2015-11-03 | 2017-05-18 | Messer Group Gmbh | Verfahren zur Herstellung von Peroxosalpetersäure |
CN105883735A (zh) * | 2016-05-13 | 2016-08-24 | 河南心连心化肥有限公司 | 一种富氧法制硝酸装置及其硝酸生产方法 |
DE102016015322A1 (de) | 2016-12-22 | 2018-06-28 | Messer Group Gmbh | Vorrichtung und Verfahren zum Eintragen von Gas in eine Mehrzahl von Prozessfluiden |
CN106744746B (zh) * | 2017-02-17 | 2018-11-02 | 交城县金兰化工有限公司 | 一种环保高效的硝酸生产方法 |
EP3372556A1 (en) * | 2017-03-07 | 2018-09-12 | Casale Sa | A plant for the production of nitric acid, a related process and method of revamping |
DE102017004329A1 (de) * | 2017-05-04 | 2018-11-08 | Messer Group Gmbh | Verfahren und Vorrichtung zum Eintragen eines Gases in eine Flüssigkeit |
CN109879258B (zh) * | 2019-02-20 | 2024-03-08 | 浙江瀚普智慧科技有限公司 | 一种氮氧化物高效氧化吸收制硝酸的装置及方法 |
BR112021012336A2 (pt) * | 2019-02-22 | 2021-08-31 | Yara International Asa | Torre de branqueamento vertical, métodos de branqueamento e para produzir ácido nítrico, e, usos de uma torre de branqueamento vertical e de um recheio estruturado |
CN110540178B (zh) * | 2019-09-10 | 2024-02-02 | 中国成达工程有限公司 | 一种中压法硝酸生产工艺及其生产设备 |
CN112473570A (zh) * | 2019-09-11 | 2021-03-12 | 南京延长反应技术研究院有限公司 | 一种基于微界面强化的硝酸工业制备系统及工艺 |
DE102020002008A1 (de) | 2020-03-27 | 2021-09-30 | Messer Group Gmbh | Verfahren und Produktionsanlage zum Herstellen von Salpetersäure |
EP3904280A1 (en) * | 2020-04-29 | 2021-11-03 | Yara International ASA | Absorption column comprising a feed box having a serrated weir and a structured packing and process for the production of nitric acid |
DE102020003083A1 (de) * | 2020-05-22 | 2021-11-25 | Messer Group Gmbh | Verfahren und Produktionsanlage zum Herstellen von Salpetersäure |
CN116395715B (zh) * | 2023-06-07 | 2023-08-18 | 河北正元化工工程设计有限公司 | 一种绿氢、灰氢耦合制氨联产硝酸与硝酸铵工艺 |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE551022A (es) * | 1955-09-14 | 1900-01-01 | ||
US3927182A (en) * | 1971-02-25 | 1975-12-16 | James Basil Powell | Process for making nitric acid by the ammonia oxidation-nitric oxide oxidation-water absorption method |
IT1027882B (it) * | 1974-12-20 | 1978-12-20 | Sir Soc Italiana Resine Spa | Procedimento per la produzione di acito nitrico |
GB1603630A (en) * | 1977-06-16 | 1981-11-25 | Boc Ltd | Gas-liquid contact process |
EP0004746A3 (en) * | 1978-04-07 | 1979-10-31 | BOC Limited | Gas-liquid contact process |
DE2939674A1 (de) * | 1979-09-29 | 1981-04-09 | Hoechst Ag, 6000 Frankfurt | Verfahren zur absorption nitroser gase |
DE3704720A1 (de) * | 1987-02-14 | 1988-08-25 | Huels Troisdorf | Verfahren und vorrichtung zur herstellung von benzolcarbonsaeuren bzw. benzoldicarbonsaeureestern |
US4867918A (en) * | 1987-12-30 | 1989-09-19 | Union Carbide Corporation | Gas dispersion process and system |
US4931225A (en) * | 1987-12-30 | 1990-06-05 | Union Carbide Industrial Gases Technology Corporation | Method and apparatus for dispersing a gas into a liquid |
DE3826955A1 (de) * | 1988-08-09 | 1990-02-15 | Krupp Gmbh | Verfahren und vorrichtung zum eintragen von sauerstoff in fluessigkeiten |
US5167935A (en) * | 1989-01-26 | 1992-12-01 | Beco Engineering Company | Apparatus for treatment of nitrogen oxides |
US5356600A (en) * | 1990-09-24 | 1994-10-18 | Praxair Technology, Inc. | Oxygen enrichment method and system |
US5061406A (en) * | 1990-09-25 | 1991-10-29 | Union Carbide Industrial Gases Technology Corporation | In-line gas/liquid dispersion |
US5302325A (en) * | 1990-09-25 | 1994-04-12 | Praxair Technology, Inc. | In-line dispersion of gas in liquid |
US5108662A (en) * | 1991-05-01 | 1992-04-28 | Union Carbide Industrial Gases Technology Corporation | Gas-liquid mixing process and apparatus |
CA2200996A1 (en) * | 1996-04-01 | 1997-10-01 | Sandeep Bhatia | Oxygen injection in nitric acid production |
ID16932A (id) * | 1996-05-23 | 1997-11-20 | Praxair Technology Inc | Penyemprot oksigen langsung dalam produksi asam nitrat |
US5985230A (en) * | 1996-10-03 | 1999-11-16 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Nitric acid production |
-
1998
- 1998-12-24 US US09/220,818 patent/US6165435A/en not_active Expired - Fee Related
-
1999
- 1999-11-01 ID IDP991022D patent/ID24018A/id unknown
- 1999-12-21 EP EP99125583A patent/EP1013604B1/en not_active Expired - Lifetime
- 1999-12-21 CN CNB991269381A patent/CN1157329C/zh not_active Expired - Fee Related
- 1999-12-21 ES ES99125583T patent/ES2177193T3/es not_active Expired - Lifetime
- 1999-12-21 KR KR10-1999-0059636A patent/KR100501462B1/ko not_active IP Right Cessation
- 1999-12-21 BR BR9905929-0A patent/BR9905929A/pt not_active IP Right Cessation
- 1999-12-21 DE DE69902139T patent/DE69902139T2/de not_active Expired - Fee Related
- 1999-12-21 CA CA002293004A patent/CA2293004C/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP1013604B1 (en) | 2002-07-17 |
ID24018A (id) | 2000-06-29 |
EP1013604A1 (en) | 2000-06-28 |
CA2293004C (en) | 2003-05-13 |
CN1157329C (zh) | 2004-07-14 |
KR20000052536A (ko) | 2000-08-25 |
CA2293004A1 (en) | 2000-06-24 |
DE69902139D1 (de) | 2002-08-22 |
KR100501462B1 (ko) | 2005-07-18 |
BR9905929A (pt) | 2000-08-15 |
CN1261594A (zh) | 2000-08-02 |
DE69902139T2 (de) | 2003-01-16 |
US6165435A (en) | 2000-12-26 |
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