ES2138409T3 - Procedimiento para la preparacion de esteres alquilicos puros del acido alquilacetoacetico. - Google Patents
Procedimiento para la preparacion de esteres alquilicos puros del acido alquilacetoacetico.Info
- Publication number
- ES2138409T3 ES2138409T3 ES97104180T ES97104180T ES2138409T3 ES 2138409 T3 ES2138409 T3 ES 2138409T3 ES 97104180 T ES97104180 T ES 97104180T ES 97104180 T ES97104180 T ES 97104180T ES 2138409 T3 ES2138409 T3 ES 2138409T3
- Authority
- ES
- Spain
- Prior art keywords
- alkyl
- sup
- sub
- procedure
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- WDJHALXBUFZDSR-UHFFFAOYSA-N Acetoacetic acid Natural products CC(=O)CC(O)=O WDJHALXBUFZDSR-UHFFFAOYSA-N 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- WOWBFOBYOAGEEA-UHFFFAOYSA-N diafenthiuron Chemical compound CC(C)C1=C(NC(=S)NC(C)(C)C)C(C(C)C)=CC(OC=2C=CC=CC=2)=C1 WOWBFOBYOAGEEA-UHFFFAOYSA-N 0.000 title 1
- 239000002253 acid Substances 0.000 abstract 2
- 108010007666 IMP cyclohydrolase Proteins 0.000 abstract 1
- 102100020796 Inosine 5'-monophosphate cyclohydrolase Human genes 0.000 abstract 1
- 239000013067 intermediate product Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
SE DESCRIBE UN METODO PARA LA PURIFICACION DE ESTERES ALQUILICOS DEL ACIDO ALQUILACETILACETICO CON LA FORMULA GENERAL EN LA QUE R{SUP,1} REPRESENTA UN GRUPO ALQUILO C{SUB,1} C{SUB,10} Y R{SUP,2} REPRESENTA UN GRUPO ALQUILO C{SUB,1} C{SUB,4}. PARA ELLO EL ESTER ALQUILICO DEL ACIDO ALQUILACETILACETICO, QUE CONTIENE EL ESTER ALQUILICO DEL ACIDO ALQUENILACETILACETICO CON LA FORMULA GENERAL EN LA QUE R{SUP,1} Y R{SUP,2} TIENEN EL SIGNIFICADO YA MENCIONADO Y/O OTROS PRODUCTOS SECUNDARIOS COMO IMPUREZAS, CON UN ESTER DE LA FORMULA GENERAL EN LA QUE R{SUP,2} TIENE EL SIGNIFICADO MENCIONADO, Y EN PRESENCIA DE UNA BASE, SE TRANSFORMA EN UN PRODUCTO INTERMEDIO QUE SE SEPARA.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH65596 | 1996-03-13 | ||
| CH108796 | 1996-04-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2138409T3 true ES2138409T3 (es) | 2000-01-01 |
Family
ID=25685276
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES97104180T Expired - Lifetime ES2138409T3 (es) | 1996-03-13 | 1997-03-12 | Procedimiento para la preparacion de esteres alquilicos puros del acido alquilacetoacetico. |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US5786501A (es) |
| EP (1) | EP0795538B1 (es) |
| JP (1) | JP3981998B2 (es) |
| KR (1) | KR100465142B1 (es) |
| CN (1) | CN1116272C (es) |
| AT (1) | ATE184588T1 (es) |
| CA (1) | CA2198837C (es) |
| CZ (1) | CZ293618B6 (es) |
| DE (1) | DE59700429D1 (es) |
| DK (1) | DK0795538T3 (es) |
| ES (1) | ES2138409T3 (es) |
| HU (1) | HU216549B (es) |
| NO (1) | NO307044B1 (es) |
| PL (1) | PL187309B1 (es) |
| SK (1) | SK282381B6 (es) |
| TW (1) | TW349938B (es) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AT407249B (de) * | 1997-12-29 | 2001-01-25 | Chemie Linz Gmbh | Verbessertes verfahren zur herstellung von 2-acetylcarbonsäureestern |
| CN114920646B (zh) * | 2022-05-13 | 2023-10-27 | 安徽英瑞骐生物科技有限公司 | 一种2-正丁基乙酰乙酸乙酯的新合成方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2900311A (en) * | 1952-10-11 | 1959-08-18 | Union Carbide Corp | Purification of acetoacetic esters by distillation |
| US2843623A (en) * | 1954-10-01 | 1958-07-15 | Nat Distillers Chem Corp | Production of ethyl acetoacetate |
| BE760034A (fr) * | 1969-12-08 | 1971-06-08 | Ici Ltd | Production d'esters |
| DE3227388A1 (de) * | 1982-07-22 | 1984-01-26 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von (alpha)-substituierten ss-dicarbonyl-, ss-cyancarbonyl- und ss-dicyanverbindungen |
-
1997
- 1997-02-25 US US08/806,051 patent/US5786501A/en not_active Expired - Fee Related
- 1997-02-28 CA CA002198837A patent/CA2198837C/en not_active Expired - Fee Related
- 1997-03-04 TW TW086102538A patent/TW349938B/zh active
- 1997-03-05 SK SK286-97A patent/SK282381B6/sk not_active IP Right Cessation
- 1997-03-07 KR KR1019970007701A patent/KR100465142B1/ko not_active IP Right Cessation
- 1997-03-07 JP JP05297197A patent/JP3981998B2/ja not_active Expired - Lifetime
- 1997-03-12 AT AT97104180T patent/ATE184588T1/de not_active IP Right Cessation
- 1997-03-12 PL PL97318927A patent/PL187309B1/pl not_active IP Right Cessation
- 1997-03-12 NO NO971148A patent/NO307044B1/no not_active IP Right Cessation
- 1997-03-12 DK DK97104180T patent/DK0795538T3/da active
- 1997-03-12 ES ES97104180T patent/ES2138409T3/es not_active Expired - Lifetime
- 1997-03-12 HU HU9700580A patent/HU216549B/hu not_active IP Right Cessation
- 1997-03-12 CZ CZ1997748A patent/CZ293618B6/cs not_active IP Right Cessation
- 1997-03-12 EP EP97104180A patent/EP0795538B1/de not_active Expired - Lifetime
- 1997-03-12 DE DE59700429T patent/DE59700429D1/de not_active Expired - Fee Related
- 1997-03-13 CN CN97103475A patent/CN1116272C/zh not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| HU9700580D0 (en) | 1997-04-28 |
| CN1163260A (zh) | 1997-10-29 |
| ATE184588T1 (de) | 1999-10-15 |
| CA2198837C (en) | 2004-10-26 |
| CN1116272C (zh) | 2003-07-30 |
| EP0795538A1 (de) | 1997-09-17 |
| EP0795538B1 (de) | 1999-09-15 |
| SK28697A3 (en) | 1997-12-10 |
| CZ74897A3 (cs) | 1998-05-13 |
| JPH101456A (ja) | 1998-01-06 |
| HUP9700580A3 (en) | 1998-01-28 |
| JP3981998B2 (ja) | 2007-09-26 |
| NO971148L (no) | 1997-09-15 |
| DE59700429D1 (de) | 1999-10-21 |
| DK0795538T3 (da) | 1999-12-20 |
| NO971148D0 (no) | 1997-03-12 |
| KR100465142B1 (ko) | 2005-04-06 |
| PL187309B1 (pl) | 2004-06-30 |
| SK282381B6 (sk) | 2002-01-07 |
| US5786501A (en) | 1998-07-28 |
| HU216549B (hu) | 1999-07-28 |
| KR970069972A (ko) | 1997-11-07 |
| TW349938B (en) | 1999-01-11 |
| CZ293618B6 (cs) | 2004-06-16 |
| PL318927A1 (en) | 1997-09-15 |
| NO307044B1 (no) | 2000-01-31 |
| HUP9700580A2 (en) | 1997-12-29 |
| CA2198837A1 (en) | 1997-09-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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