ES2084020T3 - Proceso y catalizador para preparar 2,2'-bipiridilos. - Google Patents
Proceso y catalizador para preparar 2,2'-bipiridilos.Info
- Publication number
- ES2084020T3 ES2084020T3 ES90902013T ES90902013T ES2084020T3 ES 2084020 T3 ES2084020 T3 ES 2084020T3 ES 90902013 T ES90902013 T ES 90902013T ES 90902013 T ES90902013 T ES 90902013T ES 2084020 T3 ES2084020 T3 ES 2084020T3
- Authority
- ES
- Spain
- Prior art keywords
- catalyst
- bipiridilos
- prepare
- base
- bipyridyls
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/06—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom
- C07D213/22—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom containing two or more pyridine rings directly linked together, e.g. bipyridyl
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
UN PROCESO PARA LA PREPARACION DE 2,2''-BIPIRIDILOS QUE CONSISTE EN HACER REACCIONAR UNA BASE DE PIRIDINA ANTE LA PRESENCIA DE UN CATALIZADOR DE NIQUEL QUE CONTIENE UNA CANTIDAD SIGNIFICANTE DE UN ENLACE DE NIQUEL ELEMENTAL QUE SE ENCUENTRA SOBRE UN SOPORTE ADECUADO. LA REACCION DE ACOPLAMIENTO TIENE LUGAR EN VARIOS MODELOS DE REACTORES A UNA TEMPERATURA DE UNOS 200-240 C Y A UNA PRESION SUFICIENTE COMO PARA MANTENER POR LO MENOS PARTE DE LA BASE EN UN ESTADO LIQUIDO DURANTE LA REACCION.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/299,789 US4966972A (en) | 1989-01-19 | 1989-01-19 | Process and catalyst for the preparation of 2,2'-bipyridyls |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2084020T3 true ES2084020T3 (es) | 1996-05-01 |
Family
ID=23156313
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES90902013T Expired - Lifetime ES2084020T3 (es) | 1989-01-19 | 1990-01-16 | Proceso y catalizador para preparar 2,2'-bipiridilos. |
Country Status (13)
Country | Link |
---|---|
US (1) | US4966972A (es) |
EP (1) | EP0454731B1 (es) |
JP (1) | JP2828773B2 (es) |
KR (1) | KR930002274B1 (es) |
AT (1) | ATE135691T1 (es) |
AU (1) | AU626766B2 (es) |
BR (1) | BR9007042A (es) |
CA (1) | CA2008014C (es) |
DE (1) | DE69026073T2 (es) |
DK (1) | DK0454731T3 (es) |
ES (1) | ES2084020T3 (es) |
IL (1) | IL93109A (es) |
WO (1) | WO1990008139A1 (es) |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AU2882189A (en) * | 1988-02-05 | 1989-08-10 | Signode Corporation | Hot gas welding of thermoplastic material and transverse weld produced thereby |
US5221747A (en) * | 1989-01-19 | 1993-06-22 | Reilly Industries, Inc. | Improved process and catalyst for the preparation of 2,2' bipyridyls |
IE63524B1 (en) * | 1990-07-18 | 1995-05-03 | Reilly Ind Inc | Improved Processes and Catalysts for the Preparation of 2,2'-Bipyridyls |
GR1002169B (en) * | 1995-03-29 | 1996-03-06 | Georgios Karathanos | Welding tape machine for the packing of objects. |
JP3272326B2 (ja) | 1999-06-14 | 2002-04-08 | 三協化学株式会社 | 2−ピリジルピリジン誘導体の製造方法 |
JP3032980B1 (ja) | 1999-06-14 | 2000-04-17 | 三協化学株式会社 | 2―ピリジルピリジン誘導体の製造方法 |
CN105461620B (zh) * | 2015-11-23 | 2018-06-19 | 安徽千和新材料科技发展有限公司 | 一种2,2’-联吡啶的雷尼镍催化制备方法 |
CN107935919B (zh) * | 2017-11-17 | 2019-09-03 | 南京红太阳生物化学有限责任公司 | 一种2,2’-联吡啶及其衍生物的制备方法 |
CN108440392B (zh) * | 2018-04-19 | 2020-09-25 | 合肥工业大学 | 一种合成2,2’-联吡啶的连续化生产装置及生产方法 |
CN110801841A (zh) * | 2019-11-27 | 2020-02-18 | 中国科学院大连化学物理研究所 | 一种用于合成吡啶偶联制2,2’-联吡啶的催化剂及其制备方法和应用 |
GB2599981B (en) * | 2020-05-14 | 2023-06-14 | Johnson Matthey Plc | Catalyst for producing a substituted or unsubstituted pyridine |
CN114920687B (zh) * | 2022-05-25 | 2024-04-09 | 南京红太阳生物化学有限责任公司 | 一种4,4′-联吡啶的制备方法 |
CN115010654A (zh) * | 2022-06-14 | 2022-09-06 | 南京红太阳生物化学有限责任公司 | 一种2,2’联吡啶绿色合成工艺 |
CN115245841B (zh) * | 2022-08-22 | 2024-01-26 | 山东明化新材料有限公司 | 一种镍钴金属骨架催化剂在2,2’-联吡啶制备中的应用 |
CN115430365B (zh) * | 2022-11-09 | 2023-03-03 | 北京弗莱明科技有限公司 | 一种利用近等温反应装置制备2,2’-联吡啶的方法 |
CN116099218B (zh) * | 2023-03-07 | 2023-06-23 | 北京弗莱明科技有限公司 | 一种连续式制备α,α'-联氮杂苯的方法 |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3053846A (en) * | 1962-09-11 | Method for the manufacture of z | ||
US2526718A (en) * | 1950-10-24 | Coating compositions | ||
GB899015A (en) * | 1960-04-26 | 1962-06-20 | Ici Ltd | Preparation of catalyst |
DE1156768B (de) * | 1960-12-17 | 1963-11-07 | Varta Ag | Verfahren zur Aktivierung metallischer Katalysatoren |
GB1000656A (en) * | 1962-03-08 | 1965-08-11 | Ici Ltd | 2-2 dipyridyl and dialkyl derivatives thereof |
US3173920A (en) * | 1962-07-03 | 1965-03-16 | Ici Ltd | Process for preparing 2:2'-dipyridyls |
GB1014076A (en) * | 1963-06-18 | 1965-12-22 | Ici Ltd | Dipyridyls |
GB1060661A (en) * | 1963-09-12 | 1967-03-08 | Ici Ltd | Manufacture of bipyridyls |
US3560404A (en) * | 1966-12-30 | 1971-02-02 | Varta Ag | Reactivating pyrophoric type catalysts in an organic solvent |
GB1202711A (en) * | 1967-01-20 | 1970-08-19 | Ici Ltd | Catalyst regeneration process |
GB1283693A (en) * | 1968-10-03 | 1972-08-02 | Ici Ltd | Preparation of 2,2'-bipyridyls |
GB1377213A (en) * | 1971-05-03 | 1974-12-11 | Ici Ltd | Preparation of 2,2-bipyridyls |
US3822279A (en) * | 1971-07-15 | 1974-07-02 | Ici Ltd | Preparation of 2,2'-bipyridyls |
BE785802A (fr) * | 1971-07-15 | 1973-01-03 | Ici Ltd | Preparation de 2,2'-bipyridyles |
-
1989
- 1989-01-19 US US07/299,789 patent/US4966972A/en not_active Expired - Lifetime
-
1990
- 1990-01-16 KR KR1019900702059A patent/KR930002274B1/ko not_active IP Right Cessation
- 1990-01-16 AU AU49560/90A patent/AU626766B2/en not_active Expired
- 1990-01-16 BR BR909007042A patent/BR9007042A/pt not_active IP Right Cessation
- 1990-01-16 WO PCT/US1990/000295 patent/WO1990008139A1/en active IP Right Grant
- 1990-01-16 EP EP90902013A patent/EP0454731B1/en not_active Expired - Lifetime
- 1990-01-16 ES ES90902013T patent/ES2084020T3/es not_active Expired - Lifetime
- 1990-01-16 DK DK90902013.3T patent/DK0454731T3/da active
- 1990-01-16 AT AT90902013T patent/ATE135691T1/de not_active IP Right Cessation
- 1990-01-16 DE DE69026073T patent/DE69026073T2/de not_active Expired - Lifetime
- 1990-01-16 JP JP2502285A patent/JP2828773B2/ja not_active Expired - Lifetime
- 1990-01-18 CA CA002008014A patent/CA2008014C/en not_active Expired - Lifetime
- 1990-01-18 IL IL9310990A patent/IL93109A/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
IL93109A (en) | 1994-04-12 |
JPH04504567A (ja) | 1992-08-13 |
DE69026073T2 (de) | 1996-09-05 |
US4966972A (en) | 1990-10-30 |
DE69026073D1 (de) | 1996-04-25 |
WO1990008139A1 (en) | 1990-07-26 |
CA2008014C (en) | 1999-05-11 |
JP2828773B2 (ja) | 1998-11-25 |
EP0454731A1 (en) | 1991-11-06 |
KR930002274B1 (ko) | 1993-03-27 |
AU626766B2 (en) | 1992-08-06 |
ATE135691T1 (de) | 1996-04-15 |
KR910700235A (ko) | 1991-03-14 |
EP0454731B1 (en) | 1996-03-20 |
DK0454731T3 (da) | 1996-06-24 |
CA2008014A1 (en) | 1990-07-19 |
BR9007042A (pt) | 1991-11-12 |
AU4956090A (en) | 1990-08-13 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG2A | Definitive protection |
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