EP3625321B2 - Procédé de production de préparations gélifiées - Google Patents

Procédé de production de préparations gélifiées Download PDF

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Publication number
EP3625321B2
EP3625321B2 EP18720246.0A EP18720246A EP3625321B2 EP 3625321 B2 EP3625321 B2 EP 3625321B2 EP 18720246 A EP18720246 A EP 18720246A EP 3625321 B2 EP3625321 B2 EP 3625321B2
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EP
European Patent Office
Prior art keywords
production line
batch production
premixture
filling
line
Prior art date
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Application number
EP18720246.0A
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German (de)
English (en)
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EP3625321B1 (fr
EP3625321A1 (fr
Inventor
Uwe Trebbe
Harald Müller
Thomas Holderbaum
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
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Henkel AG and Co KGaA
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Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Priority to PL18720246.0T priority Critical patent/PL3625321T5/pl
Publication of EP3625321A1 publication Critical patent/EP3625321A1/fr
Publication of EP3625321B1 publication Critical patent/EP3625321B1/fr
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0094—Process for making liquid detergent compositions, e.g. slurries, pastes or gels
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0008—Detergent materials or soaps characterised by their shape or physical properties aqueous liquid non soap compositions
    • C11D17/003—Colloidal solutions, e.g. gels; Thixotropic solutions or pastes
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2065—Polyhydric alcohols

Definitions

  • EP2746379A1 discloses the production of liquid detergent preparations by mixing a perfume-free solution with a solution containing surfactant and perfume.
  • From the EN 10 2010 055 770 A1 is a process for producing cosmetic and/or dermatological emulsions in which all ingredients are mixed in several stages in a batch production line. The finished emulsion is then pumped to a filling line and filled.
  • a method for producing gel-form washing or cleaning agents comprises providing a premix on a batch production line, wherein the premix contains at least water, glycerin and surfactants.
  • the method further comprises adding supplements to the premix, wherein the supplements comprise at least fragrances, on a filling line following the batch production line.
  • supplements in particular fragrances
  • a filling line is understood here and below to be the part of a production line from which the finished product is filled, for example, into individual quantity containers.
  • Upstream of the filling line is the batch production line, in which all ingredients apart from the supplements are mixed and on which the almost finished product is held in a collecting container if necessary to be fed to the filling line.
  • a first starting mixture containing water, glycerin and liquid non-ionic surfactants and a second starting mixture containing at least fatty alcohol ethoxylates (FAEO) are provided to prepare the premix.
  • the two starting mixtures are mixed in a mixer of the batch production line. This can in particular be a static mixer.
  • the premix is provided on the batch production line at a temperature of at least 60 °C, in particular at least 75 °C.
  • a temperature of at least 60 °C, in particular at least 75 °C Such high temperatures on the batch production line have the advantage that the premix has a relatively low viscosity and the individual components can be mixed well.
  • the supplements are mixed on the filling line at temperatures of no more than 40°C.
  • the supplements can be mixed on the filling line at room temperature.
  • At least one colorant can also be added on the filling line.
  • the premix is divided after the batch production line into at least two parts which are further processed on different filling lines, wherein different supplements are added to a first part of the premix than to a second part.
  • This approach has the advantage that different branches of filling lines provide different end products. Production can therefore be varied in some parameters in the final section of filling by adding different additives. This has the advantage that production is particularly economical and flexible. In particular, cleaning effort and waste are reduced because the same premix on the batch production line can be used for different end products on different filling lines.
  • Figure 1 shows a production line 1 for producing gel-form washing or cleaning agents.
  • the production line 1 is divided into a batch production line 2 and a subsequent filling line 3.
  • a batch is produced, ie a large quantity of the washing or cleaning agent by mixing different starting substances.
  • the filling line 3 the finished washing or cleaning agent is filled, for example, into a number of individual quantity containers.
  • supplementary agents are also added on the filling line 3.
  • the gel-form detergent or cleaning agent is not yet finished, but a premix is provided which still has to be supplemented with the additives in order to obtain the finished gel-form detergent or cleaning agent.
  • a first starting mixture 4 is first provided.
  • the first starting mixture 4 contains at least water, glycerin and liquid non-ionic surfactants. This first starting mixture 4 is typically provided at a temperature of about 80 °C.
  • the components of the first starting mixture can be mixed statically or dynamically, for example by means of a planetary mixer. After mixing, the first starting mixture 4 can be kept in a collection container 5 for further steps.
  • a second starting mixture 6 is then added to the first starting mixture 4, the second starting mixture 6 containing fatty alcohol ethoxylates (FAEO).
  • the second starting mixture 6 is also typically provided at a temperature of 80 °C.
  • the first starting mixture 4 and the second starting mixture 6 are mixed in a mixer 7, in particular a static mixer, to provide the premix.
  • the finished premix is thus available at the outlet of the batch production line 2 at a temperature of 80 °C.
  • the premix can be divided into different branches.
  • the premix is divided into a first branch 8 and a second branch 9 of the filling line 3.
  • a first supplementary agent 10 is added to the premix and mixed with it in a mixer 11, in particular a static mixer.
  • the first supplementary agent 10 contains in particular at least one first fragrance.
  • the first supplementary agent 10 in the embodiment shown contains a first dye. This produces the gel-like washing or cleaning agent. It can be kept in a collecting container 12 for filling and, if necessary, circulated until filling.
  • a second supplementary agent 13 is added to the premix instead of the first supplementary agent 10.
  • a second supplementary agent 13 is used which comprises at least a second fragrance and a second colorant.
  • the second supplementary agent 13 is added to the premix at a temperature of 25°C in order to obtain the finished gel-like washing or cleaning agent with a second fragrance and a second colorant.
  • a collecting container 15 can also be provided in the second branch 9, in which the finished gel-like washing or cleaning agent is kept ready for filling and, if necessary, circulated.
  • Figure 2 shows a flow chart of the Figure 1 described method.
  • a first starting mixture 4 and a second starting mixture 6 are provided at temperatures of about 80 °C on the batch production line 2.
  • a second step 200 the two starting mixtures 4, 6 are mixed together, in particular by means of a static mixer 7.
  • a third step 300 the premix thus obtained is fed to a filling line 3 of the production line 1.
  • a fourth step 400 at least one supplementary agent 10, 13 is added to the premix on the filling line 3.
  • a fifth step 500 the finished gel-like washing or cleaning agent is filled.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Claims (7)

  1. Procédé de production d'un agent de lavage ou de nettoyage gélifiées, dans lequel le procédé comprend les étapes suivantes :
    - fourniture d'un prémélange sur une ligne de production en lots (2), le prémélange contenant au moins de l'eau, de la glycérine et des tensioactifs, et
    - mélange d'additifs (10, 13) permettant le prémélange sur une ligne de remplissage (3) suivant la ligne de production en lots (2), les additifs (10, 13) comprenant au moins des matières odorantes,
    dans lequel un premier mélange initial (4) contenant de l'eau, de la glycérine et des tensioactifs non ioniques liquides et un second mélange initial (6) contenant au moins des éthoxylates d'alcool gras sont fournis pour fournir le prémélange, et les deux mélanges initiaux (4, 6) sont mélangés dans un mélangeur (7) de la ligne de production en lots (2).
  2. Procédé selon la revendication 1,
    dans lequel le prémélange est fourni à une température d'au moins 60 °C sur la ligne de production en lots (2).
  3. Procédé selon l'une des revendications 1 ou 2,
    dans lequel le prémélange est fourni à une température d'au moins 75 °C sur la ligne de production en lots (2).
  4. Procédé selon l'une des revendications 1 à 3,
    dans lequel les additifs (10, 13) sont mélangés à des températures d'au plus 40 °C sur la ligne de remplissage (3).
  5. Procédé selon l'une des revendications 1 à 4,
    dans lequel les additifs (10, 13) sont mélangés à température ambiante sur la ligne de remplissage (3).
  6. Procédé selon l'une des revendications 1 à 5,
    dans lequel, en plus des matières odorantes sur la ligne de remplissage (3), au moins un colorant est également ajouté au mélange.
  7. Procédé selon l'une des revendications 1 à 6,
    dans lequel le prémélange est divisé en au moins deux parties après la ligne de production en lots (2), lesquelles parties sont post-traitées sur différentes lignes de remplissage (3), d'autres additifs (10, 13) étant ajoutés à une première partie du prémélange par rapport à une seconde partie.
EP18720246.0A 2017-05-19 2018-04-26 Procédé de production de préparations gélifiées Active EP3625321B2 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL18720246.0T PL3625321T5 (pl) 2017-05-19 2018-04-26 Sposób wytwarzania preparatów w postaci żelu

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102017208559.2A DE102017208559A1 (de) 2017-05-19 2017-05-19 Verfahren zur Herstellung gelförmiger Substanzen
PCT/EP2018/060659 WO2018210542A1 (fr) 2017-05-19 2018-04-26 Procédé de production de préparations gélifiées

Publications (3)

Publication Number Publication Date
EP3625321A1 EP3625321A1 (fr) 2020-03-25
EP3625321B1 EP3625321B1 (fr) 2021-06-09
EP3625321B2 true EP3625321B2 (fr) 2024-05-01

Family

ID=62063074

Family Applications (1)

Application Number Title Priority Date Filing Date
EP18720246.0A Active EP3625321B2 (fr) 2017-05-19 2018-04-26 Procédé de production de préparations gélifiées

Country Status (5)

Country Link
EP (1) EP3625321B2 (fr)
DE (1) DE102017208559A1 (fr)
ES (1) ES2880777T3 (fr)
PL (1) PL3625321T5 (fr)
WO (1) WO2018210542A1 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US12042552B2 (en) 2020-09-10 2024-07-23 The Procter & Gamble Company Late-stage product differentiation process for personal care products
DE102021200796A1 (de) 2021-01-28 2022-07-28 Psa Automobiles Sa Verstausystem für ein Ladekabel eines Elektrofahrzeugs

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2606393B1 (fr) † 1986-11-10 1989-03-10 Erca Procede et installation de remplissage de recipients avec un melange d'au moins deux produits pateux et/ou liquides
GB2217341A (en) † 1988-02-04 1989-10-25 Colgate Palmolive Co Thixotropic aqueous automatic dishwashing detergent composition
US5296157A (en) † 1991-03-05 1994-03-22 The Proctor & Gamble Company Liquid soap personal cleanser with critical heat cycle stabilizing system
US5518645A (en) † 1992-05-19 1996-05-21 Henkel Kommanditgesellschaft Auf Aktien Process for the production of paste-form detergents
US20040116539A1 (en) † 2002-12-16 2004-06-17 Unilever Home & Personal Care Usa, Division Of Conopco, Inc. Late variant addition process for personal care products
US20040247534A1 (en) † 2003-06-06 2004-12-09 Sultan Dental Products, Ltd Foamable fluoride gel compositions and methods of treatment using the same
JP2008031115A (ja) † 2006-07-31 2008-02-14 Sunstar Inc 液体組成物の製造方法及び装置
WO2010034736A1 (fr) † 2008-09-25 2010-04-01 Unilever Plc Détergents liquides
WO2012061991A1 (fr) † 2010-11-11 2012-05-18 Unilever Plc Compositions revitalisantes pour la peau sans rinçage à l'état non solide contenant de l'acide 12-hydroxystéarique

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102010055770A1 (de) 2010-12-23 2012-06-28 Beiersdorf Ag Verfahren zur Herstellung kosmetischer und/oder dermatologischer Emulsionen mit einem oder mehreren Glucosylglyceriden
EP2746379B1 (fr) * 2012-12-20 2017-03-29 The Procter & Gamble Company Procédé de production d'une composition liquide
EP3031891B1 (fr) * 2014-12-12 2019-03-20 The Procter and Gamble Company Sachet soluble dans l'eau de détergent de lessive à compartiments multiples
WO2016139133A1 (fr) * 2015-03-02 2016-09-09 Unilever Plc Fluides de nettoyage liquides parfumés

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2606393B1 (fr) † 1986-11-10 1989-03-10 Erca Procede et installation de remplissage de recipients avec un melange d'au moins deux produits pateux et/ou liquides
GB2217341A (en) † 1988-02-04 1989-10-25 Colgate Palmolive Co Thixotropic aqueous automatic dishwashing detergent composition
US5296157A (en) † 1991-03-05 1994-03-22 The Proctor & Gamble Company Liquid soap personal cleanser with critical heat cycle stabilizing system
US5518645A (en) † 1992-05-19 1996-05-21 Henkel Kommanditgesellschaft Auf Aktien Process for the production of paste-form detergents
US20040116539A1 (en) † 2002-12-16 2004-06-17 Unilever Home & Personal Care Usa, Division Of Conopco, Inc. Late variant addition process for personal care products
US20040247534A1 (en) † 2003-06-06 2004-12-09 Sultan Dental Products, Ltd Foamable fluoride gel compositions and methods of treatment using the same
JP2008031115A (ja) † 2006-07-31 2008-02-14 Sunstar Inc 液体組成物の製造方法及び装置
WO2010034736A1 (fr) † 2008-09-25 2010-04-01 Unilever Plc Détergents liquides
WO2012061991A1 (fr) † 2010-11-11 2012-05-18 Unilever Plc Compositions revitalisantes pour la peau sans rinçage à l'état non solide contenant de l'acide 12-hydroxystéarique

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
"Handbook of Detergents", 1 January 2009, CRC PRESS, article BAYLY A. E., D. J. SMITH, NIGEL S. ROBERTS, DAVID W. YORK, S. CAPECI, URI ZOLLER, SOSIS P.: "Detergent Processing", pages: 323 - 331 †
"Perfumes, Cosmetics and Soaps", 1 January 1974, article HOWARD G M., POUCHER W. A.: "CHAPTER TWELVE The Skin-Preparations for the Face and Hands", pages: 310 - 401 †
"Waschmittel. Chemie, Umwelt, Nachhaltigkeit", 1 January 2005, WILEY-VCH, article WAGNER GÜNTER: "Herstellung von flüssigen Waschmitteln", pages: 140 - 142 †

Also Published As

Publication number Publication date
PL3625321T3 (pl) 2021-10-04
WO2018210542A1 (fr) 2018-11-22
EP3625321B1 (fr) 2021-06-09
ES2880777T3 (es) 2021-11-25
DE102017208559A1 (de) 2018-11-22
EP3625321A1 (fr) 2020-03-25
PL3625321T5 (pl) 2024-07-15

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