EP3575422B1 - Titanium alloy material - Google Patents
Titanium alloy material Download PDFInfo
- Publication number
- EP3575422B1 EP3575422B1 EP19166195.8A EP19166195A EP3575422B1 EP 3575422 B1 EP3575422 B1 EP 3575422B1 EP 19166195 A EP19166195 A EP 19166195A EP 3575422 B1 EP3575422 B1 EP 3575422B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- titanium alloy
- alloy material
- corrosion
- contamination
- samples
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
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- 229910001069 Ti alloy Inorganic materials 0.000 title claims description 82
- 239000000956 alloy Substances 0.000 title claims description 71
- 238000004140 cleaning Methods 0.000 claims description 24
- 239000002253 acid Substances 0.000 claims description 19
- 238000004458 analytical method Methods 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 17
- 238000000137 annealing Methods 0.000 claims description 16
- 238000004519 manufacturing process Methods 0.000 claims description 16
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical group [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 14
- 238000005211 surface analysis Methods 0.000 claims description 14
- 229910052751 metal Inorganic materials 0.000 claims description 13
- 239000002184 metal Substances 0.000 claims description 13
- 238000013507 mapping Methods 0.000 claims description 10
- 239000010687 lubricating oil Substances 0.000 claims description 9
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims description 8
- 238000005098 hot rolling Methods 0.000 claims description 8
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims description 8
- 239000007864 aqueous solution Substances 0.000 claims description 7
- 238000005097 cold rolling Methods 0.000 claims description 6
- 230000001680 brushing effect Effects 0.000 claims description 5
- 150000003839 salts Chemical class 0.000 claims description 4
- 238000005480 shot peening Methods 0.000 claims description 4
- 238000004453 electron probe microanalysis Methods 0.000 claims description 3
- 229910052759 nickel Inorganic materials 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 2
- 239000012300 argon atmosphere Substances 0.000 claims description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 128
- 238000005260 corrosion Methods 0.000 description 116
- 230000007797 corrosion Effects 0.000 description 116
- 238000011109 contamination Methods 0.000 description 79
- 239000000463 material Substances 0.000 description 49
- 239000000523 sample Substances 0.000 description 47
- 229910052717 sulfur Inorganic materials 0.000 description 35
- 239000010936 titanium Substances 0.000 description 35
- 229910052742 iron Inorganic materials 0.000 description 33
- 229910052739 hydrogen Inorganic materials 0.000 description 31
- 239000001257 hydrogen Substances 0.000 description 31
- 238000012360 testing method Methods 0.000 description 25
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 24
- 230000000052 comparative effect Effects 0.000 description 20
- 239000002585 base Substances 0.000 description 18
- 238000005096 rolling process Methods 0.000 description 18
- 230000004580 weight loss Effects 0.000 description 18
- 239000011701 zinc Substances 0.000 description 18
- 229910052719 titanium Inorganic materials 0.000 description 16
- 238000007788 roughening Methods 0.000 description 14
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 12
- 150000004678 hydrides Chemical class 0.000 description 9
- 230000000694 effects Effects 0.000 description 8
- 229910052725 zinc Inorganic materials 0.000 description 8
- 238000010521 absorption reaction Methods 0.000 description 6
- 229910045601 alloy Inorganic materials 0.000 description 6
- 150000002431 hydrogen Chemical class 0.000 description 6
- 238000005259 measurement Methods 0.000 description 6
- 239000013256 coordination polymer Substances 0.000 description 5
- 230000003746 surface roughness Effects 0.000 description 5
- 239000005069 Extreme pressure additive Substances 0.000 description 4
- 239000000460 chlorine Substances 0.000 description 4
- 229910052801 chlorine Inorganic materials 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 239000011159 matrix material Substances 0.000 description 4
- 238000000682 scanning probe acoustic microscopy Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- 101000993059 Homo sapiens Hereditary hemochromatosis protein Proteins 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000002161 passivation Methods 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 229910052718 tin Inorganic materials 0.000 description 3
- 229910052726 zirconium Inorganic materials 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 description 2
- 230000001133 acceleration Effects 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- PXJJSXABGXMUSU-UHFFFAOYSA-N disulfur dichloride Chemical compound ClSSCl PXJJSXABGXMUSU-UHFFFAOYSA-N 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- SZVJSHCCFOBDDC-UHFFFAOYSA-N ferrosoferric oxide Chemical compound O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 2
- 229910052731 fluorine Inorganic materials 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000000314 lubricant Substances 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- 229910052758 niobium Inorganic materials 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000013535 sea water Substances 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- 238000004506 ultrasonic cleaning Methods 0.000 description 2
- 238000010313 vacuum arc remelting Methods 0.000 description 2
- 229920006367 Neoflon Polymers 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 235000019482 Palm oil Nutrition 0.000 description 1
- 229910001252 Pd alloy Inorganic materials 0.000 description 1
- 229910009972 Ti2Ni Inorganic materials 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 239000012267 brine Substances 0.000 description 1
- -1 chlorine ions Chemical class 0.000 description 1
- HPNSNYBUADCFDR-UHFFFAOYSA-N chromafenozide Chemical compound CC1=CC(C)=CC(C(=O)N(NC(=O)C=2C(=C3CCCOC3=CC=2)C)C(C)(C)C)=C1 HPNSNYBUADCFDR-UHFFFAOYSA-N 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000010612 desalination reaction Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910000856 hastalloy Inorganic materials 0.000 description 1
- 229910052738 indium Inorganic materials 0.000 description 1
- 239000006101 laboratory sample Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000005555 metalworking Methods 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- KDLHZDBZIXYQEI-UHFFFAOYSA-N palladium Substances [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- 101150031287 petH gene Proteins 0.000 description 1
- 229920002493 poly(chlorotrifluoroethylene) Polymers 0.000 description 1
- 239000005023 polychlorotrifluoroethylene (PCTFE) polymer Substances 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- 238000010248 power generation Methods 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000002250 progressing effect Effects 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000010731 rolling oil Substances 0.000 description 1
- 229910052707 ruthenium Inorganic materials 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Inorganic materials [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 238000005482 strain hardening Methods 0.000 description 1
- 230000002123 temporal effect Effects 0.000 description 1
- 229910000048 titanium hydride Inorganic materials 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
- LRXTYHSAJDENHV-UHFFFAOYSA-H zinc phosphate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LRXTYHSAJDENHV-UHFFFAOYSA-H 0.000 description 1
- 229910000165 zinc phosphate Inorganic materials 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C14/00—Alloys based on titanium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/16—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/16—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
- C22F1/18—High-melting or refractory metals or alloys based thereon
- C22F1/183—High-melting or refractory metals or alloys based thereon of titanium or alloys based thereon
Definitions
- Titanium is being actively used in the aircraft field and the like, utilizing its feature of lightness and strength. Further, having high corrosion resistance, titanium is beginning to be used in wide range of fields as a material for chemical industry equipment, a material for thermal and nuclear power generation equipment, and a material for seawater desalination equipment, and the like.
- Gr. 11, Gr. 13, and Gr. 17 materials having different surface contaminating degrees were commercially obtained and were subjected to surface analysis with an electron probe micro analyzer (EPMA) surface analysis apparatus to find out elements that are present on the surface.
- EPMA electron probe micro analyzer
- elements that are present on the surface are as follows.
- Example 17 to 21 and the samples of Comparative Examples 13 to 15 were subjected to the autoclave treatment (corrosion treatment) under the conditions shown in Table 3, and hydrogen content rates before and after the treatment were analyzed.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
- Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012179003 | 2012-08-10 | ||
| PCT/JP2013/071788 WO2014025059A1 (ja) | 2012-08-10 | 2013-08-12 | チタン合金材 |
| EP13828545.7A EP2883972A4 (en) | 2012-08-10 | 2013-08-12 | TITANIUM ALLOY MATERIAL |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP13828545.7A Division EP2883972A4 (en) | 2012-08-10 | 2013-08-12 | TITANIUM ALLOY MATERIAL |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EP3575422A1 EP3575422A1 (en) | 2019-12-04 |
| EP3575422B1 true EP3575422B1 (en) | 2023-03-01 |
Family
ID=50068272
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP13828545.7A Withdrawn EP2883972A4 (en) | 2012-08-10 | 2013-08-12 | TITANIUM ALLOY MATERIAL |
| EP19166195.8A Active EP3575422B1 (en) | 2012-08-10 | 2013-08-12 | Titanium alloy material |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP13828545.7A Withdrawn EP2883972A4 (en) | 2012-08-10 | 2013-08-12 | TITANIUM ALLOY MATERIAL |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US20150167121A1 (ja) |
| EP (2) | EP2883972A4 (ja) |
| JP (1) | JP5582266B2 (ja) |
| KR (1) | KR101699636B1 (ja) |
| CN (2) | CN104520456A (ja) |
| WO (1) | WO2014025059A1 (ja) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NZ739931A (en) * | 2012-07-13 | 2019-08-30 | X Chem Inc | Dna-encoded libraries having encoding oligonucleotide linkages not readable by polymerases |
| JP6536076B2 (ja) * | 2015-02-24 | 2019-07-03 | 日本製鉄株式会社 | チタン板とその製造方法 |
| CN107848258A (zh) | 2015-07-29 | 2018-03-27 | 新日铁住金株式会社 | 钛复合材料以及热加工用钛材 |
| CN113260734B (zh) * | 2019-01-23 | 2024-01-05 | 日本制铁株式会社 | 钛材和涂装钛材 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4666666A (en) * | 1984-11-22 | 1987-05-19 | Nippon Mining Co., Ltd. | Corrosion-resistant titanium-base alloy |
| JPH04350138A (ja) * | 1990-12-26 | 1992-12-04 | Nikko Kyodo Co Ltd | 耐食性に優れたチタン合金 |
| JPH0551777A (ja) * | 1991-08-21 | 1993-03-02 | Nippon Steel Corp | 純チタンの耐食性改善方法 |
| US5316722A (en) * | 1992-07-09 | 1994-05-31 | Kabushiki Kaisha Kobe Seiko Sho | Corrosion resistant Ti-Cr-Ni alloy containing a platinum group metal |
| DE19962585C2 (de) * | 1998-12-28 | 2003-06-26 | Kobe Steel Ltd | Korrosionsbeständige Titanlegierung und daraus bestehende Komponenten |
| JP2002194591A (ja) * | 2000-12-21 | 2002-07-10 | Nippon Steel Corp | チタン薄板とその製造方法 |
| EP1577402A4 (en) * | 2002-12-25 | 2006-07-05 | Sintokogio Ltd | METHOD OF REFINING METAL SURFACES AND METAL PRODUCT PRODUCED BY THE METHOD |
| JP4361834B2 (ja) | 2003-06-24 | 2009-11-11 | 株式会社神戸製鋼所 | チタン材 |
| EP1772528B1 (en) * | 2004-06-02 | 2013-01-30 | Nippon Steel & Sumitomo Metal Corporation | Titanium alloy and method of manufacturing titanium alloy material |
| JP3916088B2 (ja) | 2005-12-28 | 2007-05-16 | 住友金属工業株式会社 | 耐食材用チタン合金 |
| CN100537805C (zh) * | 2007-10-30 | 2009-09-09 | 沈阳宝鼎化工设备制造有限公司 | 耐磨、耐腐蚀备件及其表面处理工艺 |
| JP5390934B2 (ja) * | 2009-05-20 | 2014-01-15 | 株式会社神戸製鋼所 | チタン合金材および構造部材ならびに放射性廃棄物用容器 |
| US8287770B2 (en) * | 2010-03-05 | 2012-10-16 | General Cable Technologies Corporation | Semiconducting composition |
| JP5379752B2 (ja) * | 2010-06-29 | 2013-12-25 | 株式会社神戸製鋼所 | 耐粒界腐食性に優れたチタン合金 |
-
2013
- 2013-08-12 CN CN201380042581.9A patent/CN104520456A/zh active Pending
- 2013-08-12 JP JP2013555651A patent/JP5582266B2/ja active Active
- 2013-08-12 CN CN201710992010.1A patent/CN107746996A/zh active Pending
- 2013-08-12 EP EP13828545.7A patent/EP2883972A4/en not_active Withdrawn
- 2013-08-12 KR KR1020157003159A patent/KR101699636B1/ko active IP Right Grant
- 2013-08-12 WO PCT/JP2013/071788 patent/WO2014025059A1/ja active Application Filing
- 2013-08-12 EP EP19166195.8A patent/EP3575422B1/en active Active
- 2013-08-12 US US14/418,031 patent/US20150167121A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| KR20150030265A (ko) | 2015-03-19 |
| EP3575422A1 (en) | 2019-12-04 |
| JPWO2014025059A1 (ja) | 2016-07-25 |
| EP2883972A1 (en) | 2015-06-17 |
| US20150167121A1 (en) | 2015-06-18 |
| WO2014025059A1 (ja) | 2014-02-13 |
| CN107746996A (zh) | 2018-03-02 |
| KR101699636B1 (ko) | 2017-01-24 |
| EP2883972A4 (en) | 2016-04-06 |
| JP5582266B2 (ja) | 2014-09-03 |
| CN104520456A (zh) | 2015-04-15 |
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