EP2838648B1 - Verfahren zur emulsionsbehandlung - Google Patents

Verfahren zur emulsionsbehandlung Download PDF

Info

Publication number
EP2838648B1
EP2838648B1 EP13719443.7A EP13719443A EP2838648B1 EP 2838648 B1 EP2838648 B1 EP 2838648B1 EP 13719443 A EP13719443 A EP 13719443A EP 2838648 B1 EP2838648 B1 EP 2838648B1
Authority
EP
European Patent Office
Prior art keywords
mixture
screw
liquid
tube
diameter
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
EP13719443.7A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP2838648A1 (de
Inventor
Vladimier MOROZ
Wilhelm COSOV
Wolfgang Gesen
Timo GESEN
Viktor KLAUSER
Andre Linow
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EGM-Holding-International GmbH
Original Assignee
EGM-Holding-International GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EGM-Holding-International GmbH filed Critical EGM-Holding-International GmbH
Publication of EP2838648A1 publication Critical patent/EP2838648A1/de
Application granted granted Critical
Publication of EP2838648B1 publication Critical patent/EP2838648B1/de
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • B01F23/41—Emulsifying
    • B01F23/4105—Methods of emulsifying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/421—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path
    • B01F25/423—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path by means of elements placed in the receptacle for moving or guiding the components
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • B01F23/41—Emulsifying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
    • B01F25/431—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor
    • B01F25/4314—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor with helical baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
    • B01F25/434—Mixing tubes comprising cylindrical or conical inserts provided with grooves or protrusions
    • B01F25/4341—Mixing tubes comprising cylindrical or conical inserts provided with grooves or protrusions the insert being provided with helical grooves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/45—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads
    • B01F25/452—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces
    • B01F25/4521—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces the components being pressed through orifices in elements, e.g. flat plates or cylinders, which obstruct the whole diameter of the tube
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/45—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads
    • B01F25/452—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces
    • B01F25/4524—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces the components being pressed through foam-like inserts or through a bed of loose bodies, e.g. balls
    • B01F25/45241—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces the components being pressed through foam-like inserts or through a bed of loose bodies, e.g. balls through a bed of balls
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/46—Homogenising or emulsifying nozzles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/60—Pump mixers, i.e. mixing within a pump
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/60—Pump mixers, i.e. mixing within a pump
    • B01F25/64—Pump mixers, i.e. mixing within a pump of the centrifugal-pump type, i.e. turbo-mixers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00—Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80—Mixing plants; Combinations of mixers
    • B01F33/82—Combinations of dissimilar mixers
    • B01F33/821—Combinations of dissimilar mixers with consecutive receptacles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • B01F23/41—Emulsifying
    • B01F23/413—Homogenising a raw emulsion or making monodisperse or fine emulsions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • B01F23/41—Emulsifying
    • B01F23/414—Emulsifying characterised by the internal structure of the emulsion
    • B01F23/4145—Emulsions of oils, e.g. fuel, and water
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers

Definitions

  • the invention relates to a method for producing a single-phase phase-stable liquid.
  • hyperbolic funnels are made of, for example DE 10 2008 046 889 known to give liquids in rapid rotational motion.
  • the US-A-4,127,332 discloses a method according to the preamble of claim 1.
  • phase-stable liquids from a lipophilic phase and a hydrophilic phase without emulsifiers.
  • the object of the present invention is thus to produce a process for the preparation of single-phase phase-stable liquids from a lipophilic phase and a hydrophilic phase.
  • the object underlying the invention is achieved in a first embodiment by a method according to claim 1.
  • the lowering of the static pressure in the second step is preferably effected by the outlet of the mixture from a nozzle.
  • cavitation bubbles are formed by so-called hard cavitation, since the liquid has a considerable velocity (also due to the rotational movement, for example) when it passes through the nozzle. It is believed that chemical changes occur here, and in particular during the subsequent implosion of the cavitation bubbles.
  • the mixture is placed in a rotating motion before the second step.
  • the rotating movement of the mixture is produced by a screw having a helical tapering tube.
  • the tapered tube of the screw expands towards the end of the screw in the direction of flow preferably again, but particularly preferably the outlet opening of the screw is smaller than the inlet opening.
  • the pipe diameter can also be constant.
  • the method according to the invention is preferably a convergent and in particular a convergent-divergent nozzle.
  • the mixture is preferably first set in rotating motion by means of a centrifugal pump, and then the mixture in the screw is further accelerated, for example.
  • the mixture is then preferably passed through the tube with internal swirl-producing molds.
  • the swirl-producing forms preferably at least partially helicoid form.
  • the tube is preferably arranged vertically. As a result, a Taylor-Couette-like vortex can be generated.
  • the inner diameter of the tube is preferably in a range of 2 to 10 cm.
  • the length of the tube is preferably in a range of 1 to 3 m.
  • the tube of the screw at its smallest diameter has a diameter of at most 30% of the diameter at the inlet.
  • the liquid preferably surrounds the outlet of the nozzle.
  • the outlet of the nozzle is preferably not arranged in a gaseous environment.
  • the one-phase phase-stable liquid is preferably transferred to a storage container.
  • the hydrophilic liquid is preferably water.
  • the lipophilic liquid is preferably a fossil fuel, especially diesel or kerosene.
  • the weight ratio between the hydrophilic liquid and the lipophilic liquid is preferably in a range of 0.8: 1 to 1.2: 1.
  • the process according to the invention is preferably carried out at room temperature and atmospheric pressure.
  • the first step a. is for example at least partially carried out in a hopper.
  • a retaining device such as a retaining screen is arranged at the narrow end of the hopper.
  • balls are arranged in the funnel above this restraint device.
  • these balls may have a diameter in a range of 5 to 20 mm.
  • These balls may for example be made of metal and in particular of stainless steel. These balls have the function that the two liquids are already well mixed by the filling process.
  • the inner wall of the screw may, for example, be metallic, and more preferably copper.
  • a plurality of tubes and in particular 2 to 3 tubes can be arranged in parallel helical form.
  • FIG. 1 shows a typical experimental setup for the inventive method.
  • the following concrete description of the embodiment does not limit the scope and is merely illustrative of the invention.
  • the screw 9 had a total diameter of 20 cm at the upper end and a diameter of 5 cm at the smallest diameter. At the outlet, the screw 9 had a diameter of 10 cm.
  • the emulsion was pressed through a vertically arranged tube 10 with a diameter of 7 cm and a length of 1.5 m and a helicoid helical bender (as in a screw extruder in the field of plastics technology) arranged therein. Thereafter, the liquid was forced through nozzles in a container 11 with the liquid. Due to the sudden pressure difference at the exit from the nozzles and the high speed of the liquid (also the rotation speed) cavitation occurred. It created cavitation bubbles, which subsequently imploded immediately. This resulted in a single-phase phase-stable liquid, which apparently contained no more water and had a very good calorific value. The liquid was then transferred to a product container 12.
  • the calorific value of the kerosene used was 43.596 kJ / kg.
  • the calorific value of the liquid obtained was 43.343 kJ / kg.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Colloid Chemistry (AREA)
  • Liquid Carbonaceous Fuels (AREA)
  • Grain Derivatives (AREA)
EP13719443.7A 2012-04-18 2013-04-18 Verfahren zur emulsionsbehandlung Active EP2838648B1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102012206399.4A DE102012206399B4 (de) 2012-04-18 2012-04-18 Verfahren zur Emulsionsbehandlung
PCT/EP2013/058060 WO2013156556A1 (de) 2012-04-18 2013-04-18 Verfahren zur emulsionsbehandlung

Publications (2)

Publication Number Publication Date
EP2838648A1 EP2838648A1 (de) 2015-02-25
EP2838648B1 true EP2838648B1 (de) 2017-03-22

Family

ID=48227193

Family Applications (1)

Application Number Title Priority Date Filing Date
EP13719443.7A Active EP2838648B1 (de) 2012-04-18 2013-04-18 Verfahren zur emulsionsbehandlung

Country Status (13)

Country Link
US (1) US9815034B2 (ru)
EP (1) EP2838648B1 (ru)
JP (1) JP6158304B2 (ru)
CN (1) CN104245104B (ru)
AU (1) AU2013251106B2 (ru)
CA (1) CA2870701C (ru)
DE (1) DE102012206399B4 (ru)
IN (1) IN2014MN02281A (ru)
MY (1) MY164592A (ru)
RU (1) RU2633568C2 (ru)
SG (1) SG11201406627TA (ru)
WO (1) WO2013156556A1 (ru)
ZA (1) ZA201407215B (ru)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102014017938A1 (de) 2014-12-05 2016-06-09 Florian M. König Trichter-turbinenartige Vorrichtung mit elektromagnetischer Rotationssteuerung von Flüssigkeits-Mischvorgängen
DE102016109639A1 (de) 2016-05-25 2017-11-30 Anton LEDWON Vorrichtung zur atomaren oder molekularen Umstrukturierung von Edukten

Family Cites Families (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3164375A (en) * 1955-10-14 1965-01-05 Frenkel Ag C D Apparatus for intensive mixing
US3486740A (en) * 1967-03-02 1969-12-30 Packaged Power Terminals Inc Apparatus for treating flowable materials
US3647187A (en) * 1970-08-03 1972-03-07 Technicon Instr Static mixer and method of making same
US3762947A (en) * 1971-10-12 1973-10-02 Cpc International Inc Crystallizer
JPS5014275A (ru) 1973-06-06 1975-02-14
US3937445A (en) * 1974-02-11 1976-02-10 Vito Agosta Process and apparatus for obtaining the emulsification of nonmiscible liquids
US4111402A (en) * 1976-10-05 1978-09-05 Chemineer, Inc. Motionless mixer
US4127332A (en) * 1976-11-19 1978-11-28 Daedalean Associates, Inc. Homogenizing method and apparatus
US4194844A (en) * 1978-02-13 1980-03-25 Northern Telecom Limited Multiple powder conveyor system
US4422773A (en) * 1980-08-04 1983-12-27 Technicon Instruments Corporation Apparatus and method for the non-invasive mixing of a flowing fluid stream
US4410281A (en) * 1981-03-02 1983-10-18 Ralph B. Carter Company Mixing method and apparatus utilizing pipe elbows
JPS6242728A (ja) * 1985-08-14 1987-02-24 Ono Bankin Kogyosho:Kk 流体混合具
SU1699564A1 (ru) * 1986-09-11 1991-12-23 Одесский Политехнический Институт Способ стабилизации расхода жидкости или газа
JP3685305B2 (ja) * 1998-12-16 2005-08-17 福岡県 流体混合装置
US6112768A (en) * 1999-04-08 2000-09-05 Rath; Leslie B. In-line fluid agitator
US7264394B1 (en) * 2002-06-10 2007-09-04 Inflowsion L.L.C. Static device and method of making
US20040134557A1 (en) * 2002-06-28 2004-07-15 Cymbalisty Lubomyr M. Hydrodynamic static mixing apparatus and method for use thereof in transporting, conditioning and separating oil sands and the like
AU2003281265A1 (en) 2002-07-09 2004-01-23 Toshiba Plant Systems & Services Corporation Liquid mixing apparatus and method of liquid mixing
US7045060B1 (en) * 2002-12-05 2006-05-16 Inflowsion, L.L.C. Apparatus and method for treating a liquid
JP2004004881A (ja) * 2003-06-09 2004-01-08 Sharp Corp 電子学習機
EP1771385B1 (de) * 2004-07-26 2010-09-15 Frank Reiner Kolb Hydrodynamische homogenisation
ES2331361T3 (es) * 2004-08-06 2009-12-30 Ecofur, Lda Dispositivo para mezclar fluidos.
GB0420971D0 (en) * 2004-09-21 2004-10-20 Imp College Innovations Ltd Piping
DE102005009322A1 (de) * 2005-03-01 2006-09-14 Degussa Ag Durchmischungsreaktor
DE102005037026B4 (de) * 2005-08-05 2010-12-16 Cavitator Systems Gmbh Kavitationsmischer
DE202005015341U1 (de) * 2005-09-28 2006-01-19 IFAC GmbH & Co. KG Institut für Angewandte Colloidtechnologie Vorrichtung zur In-Line-Prozesskontrolle bei der Herstellung von Emulsionen oder Dispersionen
DE102006011881A1 (de) * 2006-03-09 2007-09-13 Vortex-Nanofluid Gmbh Langzeitstabile Dispersion und Verfahren zur Herstellung der Dispersion
DK2011850T3 (en) 2006-04-27 2016-08-01 Tapioca-Comércio E Servicos Soc Unipessoal Lda PROCEDURE FOR CONVERSING HEAVY OIL TO LIGHT OIL
RU66221U1 (ru) * 2007-05-07 2007-09-10 Общество с ограниченной ответственностью "ПДС" Автоматизированная установка для обработки нефтесодержащих жидкостей
EP2025392B1 (de) * 2007-07-30 2012-05-23 Cavitator Systems GmbH Steuerung einer Cavitator-Anlage
US20090122637A1 (en) * 2007-11-14 2009-05-14 Jan Kruyer Sinusoidal mixing and shearing apparatus and associated methods
DE102008046889B4 (de) 2008-09-11 2017-11-23 Egm-Holding-International Gmbh Hyperbolischer Trichter
US20110182134A1 (en) * 2010-01-22 2011-07-28 Dow Global Technologies Inc. Mixing system comprising an extensional flow mixer
FI122642B (fi) * 2010-09-16 2012-04-30 Outotec Oyj Laite ja menetelmä kahden liuoksen dispergoimiseksi toisiinsa neste-nesteuutossa
DE202011104310U1 (de) * 2011-08-15 2011-11-14 Rainer Schmieg Wirbelmischrohr

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
None *

Also Published As

Publication number Publication date
IN2014MN02281A (ru) 2015-08-07
CN104245104B (zh) 2017-10-20
RU2014146204A (ru) 2016-06-10
JP6158304B2 (ja) 2017-07-05
MY164592A (en) 2018-01-15
ZA201407215B (en) 2015-10-28
CA2870701A1 (en) 2013-10-24
DE102012206399B4 (de) 2018-01-04
RU2633568C2 (ru) 2017-10-13
WO2013156556A1 (de) 2013-10-24
JP2015517908A (ja) 2015-06-25
AU2013251106A1 (en) 2014-11-06
CA2870701C (en) 2020-05-05
SG11201406627TA (en) 2014-12-30
DE102012206399A1 (de) 2013-10-24
US20150071026A1 (en) 2015-03-12
US9815034B2 (en) 2017-11-14
EP2838648A1 (de) 2015-02-25
CN104245104A (zh) 2014-12-24
AU2013251106B2 (en) 2018-02-01

Similar Documents

Publication Publication Date Title
DE69825475T2 (de) Injektionsmischer
DE69803877T2 (de) Vorrichtung und verfahren zur trennung eines heterogenen gemisches
DE69623657T2 (de) Verfahren und vorrichtung zur herstellung eines frei dispersen systems in einer flüssigkeit
DE60117165T2 (de) Vorrichtung und verfahren zur erzeugung hydrodynamischer kavitationen in fluiden
EP1945337B1 (de) Wirbelkammer
DE102017116506A1 (de) Fluidzufuhrleitung
DE102010047782B3 (de) Strömungsgleichrichter für geschlossene Rohrleitungen
EP0644271A1 (de) Verfahren zur herstellung eines frei dispersen systems und einrichtung zur durchführung des verfahrens
EP2140920B1 (de) Drallelement, Einlaufventil, Vorrichtung und Verfahren zum Entgasen von Flüssigkeiten
EP2475443A1 (de) Drallelement, einlaufventil, vorrichtung und verfahren zum ausdampfen aus bzw. entgasen von leichtflüchtigen stoffen oder gasen aus flüssigkeiten nebst verwendung derselben in brauprozessen
EP2838648B1 (de) Verfahren zur emulsionsbehandlung
DE102012216912B4 (de) Lebensmittelfördervorrichtung, sowie Verfahren zum Fördern eines Lebensmittels
EP0595764B1 (de) Zahnradpumpe
DE202010000075U1 (de) Vorrichtung zur Behandlung von Strömungskomponenten mittels turbulenter Strömungen
EP3334519B1 (de) Vorrichtung und verfahren zum dispergieren mindestens einer substanz in einem fluid
DE102013101436B4 (de) Benetzungsvorrichtung zum Beaufschlagen von Feststoffpartikeln eines Partikelstroms mit einer Flüssigkeit
EP3651968B1 (de) Extrudersystem mit druckregeleinrichtung
DE1667242B2 (de) Vorrichtung zum Kontaktieren eines Gases mit einer Flüssigkeit
DE102016108872A1 (de) Vorrichtung und Verfahren für die Durchführung von Fällungsreaktionen unter Beteiligung von mindestens zwei Ausgangsprodukten
DE4200720C2 (de) Verfahren und Vorrichtung zum Vermischen einer ersten Flüssigkeit und/oder eines dispersen Feststoffes mit einer zweiten Flüssigkeit
DE2221263C3 (de) Mischvorrichtung für Solvent-Extraktoren
EP3189887A1 (de) Kavitationsreaktor zum behandeln von fliessfähigen substanzen
EP3187253A1 (de) Kavitationsreaktor zum behandeln einer fliessfähigen substanz
EP4309799A1 (de) Vorrichtung zur verwirbelung einer flüssigkeit
DE29608289U1 (de) Vorrichtung zum Mischen von Strömungsmedien

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 20141106

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR

AX Request for extension of the european patent

Extension state: BA ME

DAX Request for extension of the european patent (deleted)
17Q First examination report despatched

Effective date: 20151130

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

INTG Intention to grant announced

Effective date: 20161125

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

Free format text: NOT ENGLISH

REG Reference to a national code

Ref country code: CH

Ref legal event code: EP

REG Reference to a national code

Ref country code: AT

Ref legal event code: REF

Ref document number: 877164

Country of ref document: AT

Kind code of ref document: T

Effective date: 20170415

REG Reference to a national code

Ref country code: IE

Ref legal event code: FG4D

Free format text: LANGUAGE OF EP DOCUMENT: GERMAN

REG Reference to a national code

Ref country code: DE

Ref legal event code: R096

Ref document number: 502013006717

Country of ref document: DE

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 5

REG Reference to a national code

Ref country code: NL

Ref legal event code: FP

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: NO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170622

Ref country code: FI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

Ref country code: LT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170623

Ref country code: HR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

REG Reference to a national code

Ref country code: LT

Ref legal event code: MG4D

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

Ref country code: BG

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170622

Ref country code: RS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

Ref country code: LV

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: RO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

Ref country code: SK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

Ref country code: ES

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

Ref country code: EE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

Ref country code: CZ

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SM

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

Ref country code: IS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170722

Ref country code: PT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170724

Ref country code: PL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

REG Reference to a national code

Ref country code: DE

Ref legal event code: R097

Ref document number: 502013006717

Country of ref document: DE

REG Reference to a national code

Ref country code: IE

Ref legal event code: MM4A

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MC

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

Ref country code: DK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

26N No opposition filed

Effective date: 20180102

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20170430

Ref country code: SI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

Ref country code: CH

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20170430

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 6

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20170418

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

REG Reference to a national code

Ref country code: AT

Ref legal event code: MM01

Ref document number: 877164

Country of ref document: AT

Kind code of ref document: T

Effective date: 20180418

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: HU

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT; INVALID AB INITIO

Effective date: 20130418

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: AT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180418

Ref country code: CY

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: TR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: AL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20170322

REG Reference to a national code

Ref country code: DE

Ref legal event code: R079

Ref document number: 502013006717

Country of ref document: DE

Free format text: PREVIOUS MAIN CLASS: B01F0003080000

Ipc: B01F0023400000

REG Reference to a national code

Ref country code: DE

Ref legal event code: R082

Ref document number: 502013006717

Country of ref document: DE

Representative=s name: MICHALSKI HUETTERMANN & PARTNER PATENTANWAELTE, DE

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: LU

Payment date: 20240418

Year of fee payment: 12

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: NL

Payment date: 20240418

Year of fee payment: 12

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: GB

Payment date: 20240419

Year of fee payment: 12

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20240424

Year of fee payment: 12

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: IT

Payment date: 20240424

Year of fee payment: 12

Ref country code: FR

Payment date: 20240425

Year of fee payment: 12

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: BE

Payment date: 20240418

Year of fee payment: 12