EP2242866A1 - Système de couches calorifuges et son procédé de fabrication - Google Patents
Système de couches calorifuges et son procédé de fabricationInfo
- Publication number
- EP2242866A1 EP2242866A1 EP09708297A EP09708297A EP2242866A1 EP 2242866 A1 EP2242866 A1 EP 2242866A1 EP 09708297 A EP09708297 A EP 09708297A EP 09708297 A EP09708297 A EP 09708297A EP 2242866 A1 EP2242866 A1 EP 2242866A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- layer
- aps
- sps
- thermal barrier
- barrier coating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C28/00—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
- C23C28/30—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer
- C23C28/36—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer including layers graded in composition or physical properties
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C28/00—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
- C23C28/30—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer
- C23C28/32—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer including at least one pure metallic layer
- C23C28/322—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer including at least one pure metallic layer only coatings of metal elements only
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C28/00—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
- C23C28/30—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer
- C23C28/34—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer including at least one inorganic non-metallic material layer, e.g. metal carbide, nitride, boride, silicide layer and their mixtures, enamels, phosphates and sulphates
- C23C28/345—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer including at least one inorganic non-metallic material layer, e.g. metal carbide, nitride, boride, silicide layer and their mixtures, enamels, phosphates and sulphates with at least one oxide layer
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C28/00—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
- C23C28/30—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer
- C23C28/34—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer including at least one inorganic non-metallic material layer, e.g. metal carbide, nitride, boride, silicide layer and their mixtures, enamels, phosphates and sulphates
- C23C28/345—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer including at least one inorganic non-metallic material layer, e.g. metal carbide, nitride, boride, silicide layer and their mixtures, enamels, phosphates and sulphates with at least one oxide layer
- C23C28/3455—Coatings combining at least one metallic layer and at least one inorganic non-metallic layer including at least one inorganic non-metallic material layer, e.g. metal carbide, nitride, boride, silicide layer and their mixtures, enamels, phosphates and sulphates with at least one oxide layer with a refractory ceramic layer, e.g. refractory metal oxide, ZrO2, rare earth oxides or a thermal barrier system comprising at least one refractory oxide layer
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C4/00—Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge
- C23C4/04—Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge characterised by the coating material
- C23C4/10—Oxides, borides, carbides, nitrides or silicides; Mixtures thereof
- C23C4/11—Oxides
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C4/00—Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge
- C23C4/12—Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge characterised by the method of spraying
- C23C4/134—Plasma spraying
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/249921—Web or sheet containing structurally defined element or component
- Y10T428/249953—Composite having voids in a component [e.g., porous, cellular, etc.]
- Y10T428/249981—Plural void-containing components
Definitions
- the turbine inlet temperature of about 1230 0 C to about 1350 0 C is necessary.
- This goal can be achieved by using ceramic thermal barrier coatings in addition to the use of improved base materials and effective cooling methods.
- the permissible surface temperature can be increased by a few 100 K by the thermal insulating effect of the ceramic thermal barrier layer while maintaining the same cooling conditions depending on the thickness of the thermal barrier coating.
- the greater thermal load often leads to a shortened life of the thermal layer system.
- thermal conductivity of thermal barrier coatings can be achieved by using ceramic materials with a correspondingly small intrinsic
- Thermal conductivity can be reliably achieved.
- thermal barrier coatings in the form of duplex structures are used.
- the first layer consists of a metallic layer, which has the task of protecting the underlying substrate (component) from corrosion and oxidation.
- this layer usually serves as a primer layer for the actual thermal barrier coating, as the second layer of the duplex structure.
- This second layer which performs the actual function of thermal insulation, is often a ceramic layer.
- These typically consist of yttria-stabilized zirconia (YSZ) or other oxide ceramics.
- YSZ yttria-stabilized zirconia
- Newer thermal barrier coating systems sometimes also have multilayer coating systems of various ceramics.
- suspension solution evaporates abruptly and the small solid particles are aggregated into partially or completely molten droplets, accelerated and impacted on the substrate in order to form a layer there.
- the suspension plasma spraying can be used for coatings of both ceramic and metallic materials, wherein in each case very fine, dense spherical particles are used.
- thermal barrier coatings are determined by the thermal conductivity of the material of the thermal barrier coating and by the layer thickness. Under the insulating effect of thermal barrier coatings is understood here the temperature drop across the thermal barrier coating. The layer thickness is limited due to mechanical properties to be fulfilled and can not be made arbitrarily large. These two parameters represent a principal barrier for all thermal barrier coating systems.
- the APS layer can be used in particular as a mechanically and erosively stable layer and the SPS layer in particular for improving the reflectivity and reducing the thermal conductivity.
- the advantages of the individual layers can be optimally combined, thus enabling applications that can not be fulfilled by the single-layer systems.
- the solids content of the powder in the suspension was 10% by weight (Example 1) and 20% by weight (Example 2).
- the suspension pressure was 2 bar and was operated at an air pressure of 0.5 bar.
- the layer thickness of the SPS layer was varied between 60 and 150 ⁇ m.
- the thermal conductivity of this layer was only 0.58 W / mK, the layer having a porosity of about 29%.
- FIGS. 4a to 4c Shown in FIGS. 4a to 4c are photographs of the layer systems according to the invention.
- the microstructures in the transverse section of the two double layers are shown in FIGS. 4a and 4b.
- the layer thickness of the SPS layer is 60 or 150 ⁇ m and for the APS layer 270 or 200 ⁇ m.
- the SPS layer is interspersed with significantly finer pores and cracks are visible, which in particular pass vertically through the layer. Within the APS layer significantly coarser pores are represented.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- Ceramic Engineering (AREA)
- Coating By Spraying Or Casting (AREA)
Abstract
La présente invention concerne un procédé de fabrication d'un système de couches sur un composant. Selon le procédé, au moins au moins une couche est déposée sur le composant par pulvérisation plasma atmosphérique (APS) et au moins une autre couche est déposée sur le composant par pulvérisation plasma en suspension (SPS). De manière avantageuse, on dépose en particulier les couches dans l'ordre suivant APS + SPS ou APS + SPS + APS ou également APS + SPS + couche d'érosion. Ces séries de couches ainsi appliquées ont ordinairement pour effet la création d'une première couche poreuse ainsi que d'une seconde couche poreuse disposée sur la première, la porosité et la réflectivité de la seconde couche étant supérieures à celle de la première couche. L'augmentation de la réflectivité de la couche, en particulier dans la gamme de longueurs d'ondes d'infrarouges visibles (VIS) et proches (NIR), produit de manière avantageuse une contrainte thermique plus faible du matériau de substrat, étant donné que seule une part plus faible de rayonnement thermique pénètre à travers la couche calorifuge céramique et entraîne ainsi un réchauffement moindre du substrat (composant).
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE200810007870 DE102008007870A1 (de) | 2008-02-06 | 2008-02-06 | Wärmedämmschichtsystem sowie Verfahren zu seiner Herstellung |
PCT/DE2009/000120 WO2009097834A1 (fr) | 2008-02-06 | 2009-01-29 | Système de couches calorifuges et son procédé de fabrication |
Publications (1)
Publication Number | Publication Date |
---|---|
EP2242866A1 true EP2242866A1 (fr) | 2010-10-27 |
Family
ID=40568290
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP09708297A Withdrawn EP2242866A1 (fr) | 2008-02-06 | 2009-01-29 | Système de couches calorifuges et son procédé de fabrication |
Country Status (4)
Country | Link |
---|---|
US (1) | US20110244216A1 (fr) |
EP (1) | EP2242866A1 (fr) |
DE (1) | DE102008007870A1 (fr) |
WO (1) | WO2009097834A1 (fr) |
Families Citing this family (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2450465A1 (fr) * | 2010-11-09 | 2012-05-09 | Siemens Aktiengesellschaft | Système de couche poreux doté d'une couche intérieure poreuse |
DE102011103731A1 (de) * | 2011-05-31 | 2012-12-06 | Man Diesel & Turbo Se | Verfahren zum Aufbringen einer Schutzschicht, mit einer Schutzschicht beschichtetes Bauteil und Gasturbine mit einem solchen Bauteil |
US20130260132A1 (en) * | 2012-04-02 | 2013-10-03 | United Technologies Corporation | Hybrid thermal barrier coating |
US9052111B2 (en) | 2012-06-22 | 2015-06-09 | United Technologies Corporation | Turbine engine combustor wall with non-uniform distribution of effusion apertures |
US9556505B2 (en) | 2012-08-31 | 2017-01-31 | General Electric Company | Thermal barrier coating systems and methods of making and using the same |
US11047033B2 (en) * | 2012-09-05 | 2021-06-29 | Raytheon Technologies Corporation | Thermal barrier coating for gas turbine engine components |
DE102012218198A1 (de) | 2012-10-05 | 2014-04-10 | Lufthansa Technik Ag | Wärmedämmschicht, Gasturbinenbauteil und Verfahren zur Beschichtung eines Gasturbinenbauteils |
WO2014126633A2 (fr) * | 2012-12-26 | 2014-08-21 | United Technologies Corporation | Revêtement de barrière thermique résistant à l'éclatement |
EP2971240B1 (fr) * | 2013-03-14 | 2018-11-21 | United Technologies Corporation | Revêtement de barrière thermique hybride et son procédé de fabrication |
DE102013217627A1 (de) * | 2013-09-04 | 2015-03-05 | MTU Aero Engines AG | Wärmedämmschichtsystem mit Korrosions- und Erosionsschutz |
EP2865781A1 (fr) * | 2013-10-22 | 2015-04-29 | Siemens Aktiengesellschaft | Couche céramique à deux couches dotée de microstructures différentes |
US10793941B2 (en) | 2013-10-25 | 2020-10-06 | Raytheon Technologies Corporation | Plasma spraying system with adjustable coating medium nozzle |
US20150147524A1 (en) * | 2013-11-26 | 2015-05-28 | Christopher A. Petorak | Modified thermal barrier composite coatings |
DE102014208216A1 (de) * | 2014-04-30 | 2015-11-05 | Siemens Aktiengesellschaft | CMAS resistente keramische Schicht durch Nanoporosität |
DE102014222686A1 (de) * | 2014-11-06 | 2016-05-12 | Siemens Aktiengesellschaft | Doppellagige Wärmedämmschicht durch unterschiedliche Beschichtungsverfahren |
US10253984B2 (en) | 2015-04-28 | 2019-04-09 | United Technologies Corporation | Reflective coating for components |
US10745793B2 (en) * | 2015-06-04 | 2020-08-18 | Raytheon Technologies Corporation | Ceramic coating deposition |
JP6908973B2 (ja) * | 2016-06-08 | 2021-07-28 | 三菱重工業株式会社 | 遮熱コーティング、タービン部材、ガスタービン、ならびに遮熱コーティングの製造方法 |
FR3057580A1 (fr) | 2016-10-18 | 2018-04-20 | Commissariat A L'energie Atomique Et Aux Energies Alternatives | Procede de revetement d'une surface d'un substrat solide par une couche comprenant un compose ceramique, et substrat revetu ainsi obtenu |
US20190017177A1 (en) | 2017-07-17 | 2019-01-17 | Rolls-Royce Corporation | Thermal barrier coatings for components in high-temperature mechanical systems |
US10822951B2 (en) * | 2017-07-21 | 2020-11-03 | Raytheon Technologies Corporation | Suspension plasma spray abradable coating for cantilever stator |
JP7284553B2 (ja) * | 2017-09-21 | 2023-05-31 | 日本特殊陶業株式会社 | 溶射膜を備えた基材及びその製造方法 |
US11015252B2 (en) * | 2018-04-27 | 2021-05-25 | Applied Materials, Inc. | Protection of components from corrosion |
US11673097B2 (en) | 2019-05-09 | 2023-06-13 | Valorbec, Societe En Commandite | Filtration membrane and methods of use and manufacture thereof |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA2110007A1 (fr) | 1992-12-29 | 1994-06-30 | Adrian M. Beltran | Methode de realisation d'un revetement isolant |
US6503575B1 (en) * | 2000-05-22 | 2003-01-07 | Praxair S.T. Technology, Inc. | Process for producing graded coated articles |
US6716539B2 (en) * | 2001-09-24 | 2004-04-06 | Siemens Westinghouse Power Corporation | Dual microstructure thermal barrier coating |
WO2004029330A1 (fr) | 2002-09-25 | 2004-04-08 | Volvo Aero Corporation | Revetement barriere thermique et son procede d'application |
US7150926B2 (en) * | 2003-07-16 | 2006-12-19 | Honeywell International, Inc. | Thermal barrier coating with stabilized compliant microstructure |
WO2005039872A1 (fr) | 2003-10-27 | 2005-05-06 | Mitsubishi Plastics, Inc. | Film reflechissant |
DE102004044597B3 (de) * | 2004-09-13 | 2006-02-02 | Forschungszentrum Jülich GmbH | Verfahren zur Herstellung dünner, dichter Keramikschichten |
US20060222777A1 (en) * | 2005-04-05 | 2006-10-05 | General Electric Company | Method for applying a plasma sprayed coating using liquid injection |
WO2006116844A1 (fr) * | 2005-05-02 | 2006-11-09 | National Research Council Of Canada | Procede et appareil destines a la suspension de particules fines dans un liquide, destines a un systeme d'aerosol thermique, et revetements formes au moyen de ces procede et appareil |
DE102005025054A1 (de) * | 2005-05-30 | 2006-12-07 | Forschungszentrum Jülich GmbH | Verfahren zur Herstellung gasdichter Schichten und Schichtsysteme mittels thermischem Spritzen |
DE102006005775A1 (de) * | 2006-02-07 | 2007-08-09 | Forschungszentrum Jülich GmbH | Thermisches Spritzverfahren mit kolloidaler Suspension |
WO2007112783A1 (fr) | 2006-04-06 | 2007-10-11 | Siemens Aktiengesellschaft | Revetement stratifie formant une barriere thermique a porosite elevee et composant |
US8591196B2 (en) * | 2008-06-18 | 2013-11-26 | General Electric Company | Vibration damping novel surface structures and methods of making the same |
-
2008
- 2008-02-06 DE DE200810007870 patent/DE102008007870A1/de not_active Withdrawn
-
2009
- 2009-01-29 WO PCT/DE2009/000120 patent/WO2009097834A1/fr active Application Filing
- 2009-01-29 EP EP09708297A patent/EP2242866A1/fr not_active Withdrawn
- 2009-01-29 US US12/735,609 patent/US20110244216A1/en not_active Abandoned
Non-Patent Citations (1)
Title |
---|
See references of WO2009097834A1 * |
Also Published As
Publication number | Publication date |
---|---|
WO2009097834A1 (fr) | 2009-08-13 |
US20110244216A1 (en) | 2011-10-06 |
DE102008007870A1 (de) | 2009-08-13 |
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