EP1563113B1 - Verfahren und vorrichtung zur schmelztauchbeschichtung eines metallstranges - Google Patents
Verfahren und vorrichtung zur schmelztauchbeschichtung eines metallstranges Download PDFInfo
- Publication number
- EP1563113B1 EP1563113B1 EP03811347A EP03811347A EP1563113B1 EP 1563113 B1 EP1563113 B1 EP 1563113B1 EP 03811347 A EP03811347 A EP 03811347A EP 03811347 A EP03811347 A EP 03811347A EP 1563113 B1 EP1563113 B1 EP 1563113B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- container
- metal
- coating
- molten coating
- coating metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 103
- 239000002184 metal Substances 0.000 title claims abstract description 103
- 238000003618 dip coating Methods 0.000 title claims abstract description 19
- 238000000034 method Methods 0.000 title claims abstract description 17
- 238000000576 coating method Methods 0.000 claims abstract description 81
- 239000011248 coating agent Substances 0.000 claims abstract description 79
- 230000001105 regulatory effect Effects 0.000 claims abstract description 14
- 230000001276 controlling effect Effects 0.000 claims abstract description 7
- 229910000831 Steel Inorganic materials 0.000 claims abstract description 6
- 239000010959 steel Substances 0.000 claims abstract description 6
- 230000005672 electromagnetic field Effects 0.000 claims description 4
- 238000011144 upstream manufacturing Methods 0.000 claims description 4
- 230000014759 maintenance of location Effects 0.000 claims 2
- 230000033228 biological regulation Effects 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 14
- 238000003860 storage Methods 0.000 description 9
- 239000007788 liquid Substances 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 229910001338 liquidmetal Inorganic materials 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000005246 galvanizing Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 239000000411 inducer Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000003908 quality control method Methods 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
- C23C2/003—Apparatus
- C23C2/0034—Details related to elements immersed in bath
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
- C23C2/003—Apparatus
- C23C2/0035—Means for continuously moving substrate through, into or out of the bath
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
- C23C2/003—Apparatus
- C23C2/0036—Crucibles
- C23C2/00361—Crucibles characterised by structures including means for immersing or extracting the substrate through confining wall area
- C23C2/00362—Details related to seals, e.g. magnetic means
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
- C23C2/14—Removing excess of molten coatings; Controlling or regulating the coating thickness
- C23C2/24—Removing excess of molten coatings; Controlling or regulating the coating thickness using magnetic or electric fields
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
- C23C2/34—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor characterised by the shape of the material to be treated
- C23C2/36—Elongated material
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
- C23C2/50—Controlling or regulating the coating processes
- C23C2/52—Controlling or regulating the coating processes with means for measuring or sensing
- C23C2/523—Bath level or amount
Definitions
- the invention relates to a process for hot-dip coating a metal strand, in particular a steel strip, in which the metal strand is at least partially vertically passed through a container receiving the molten coating metal at a predetermined conveying speed. Furthermore, the invention relates to a device for hot dip coating of a metal strand.
- the belts are introduced from above into the dip-coating bath in a plunger.
- the coating metal is in liquid form and one desires to use gravity together with blowers to adjust the coating thickness, subsequent processes will contact the tape until complete solidification of the coating metal prohibit the tape in the coating vessel in the vertical direction must be deflected. This happens with a roller that runs in liquid metal. Due to the liquid coating metal, this roller is subject to heavy wear and is the cause of downtimes and thus failures in production.
- Such a solution is for example from the EP 0 673 444 B1 known.
- An electromagnetic closure for sealing the coating vessel down is also the solution according to the WO 96/03533 or the one according to the JP 5086446 one.
- Hot-dip coating methods and associated apparatuses which use an electromagnetic closure in the bottom area of the coating vessel are furthermore known from US Pat EP 0 803 586 A1 , of the US 5,665,437 and from the DE 101 60 949 A1 known.
- the invention is therefore based on the object, a method and an associated apparatus for hot dip coating a metal strand with which it is possible to efficiently influence the parameters of the hot-dip coating, without necessarily changing the flow rate of the metal strand through the molten coating metal.
- the solution of this problem by the invention is procedurally characterized in that the conveying speed of the metal strand is kept substantially constant by the container and that the residence time of the metal strand in the molten coating metal by controlling or regulating the level of the level of the molten coating metal in the container is set, the metal strand is passed exclusively vertically through the molten coating metal and through a guide channel upstream of the container, and wherein an electromagnetic field is generated by means of at least two inductors arranged on both sides of the metal strand for retaining the coating metal in the container in the region of the guide channel.
- the concept of the invention is based on the fact that the level of the level of the molten coating metal in the coating container is used for the targeted influencing of parameters which influence the quality of the hot dip coating process. With this procedure, it is possible to influence the coating quality without having to vary the conveying speed of the metal strand through the coating device.
- the inventive apparatus for hot dip coating a metal strand in which the metal strand is at least partially passed vertically through the container receiving the molten coating metal is characterized by means for controlling the level of the level of the molten coating metal in the container as a function of a predetermined residence time of the metal strand in molten coating metal, wherein the means comprise measuring means for measuring the level of the molten coating metal in the container and means for influencing the level associated with a control or regulating device, and wherein the device comprises a guide channel upstream of the container and at least two on both sides of the Metallstranges arranged in the region of the guide channel inductors for generating an electromagnetic field for retaining the Be Schweizersmet alls in the container.
- the means for influencing the level of the molten coating metal have a sequence for discharging molten coating metal from the container into a storage container and a pump for conveying molten coating metal from the storage container into the container.
- the storage container is preferably arranged below the container.
- the capacity of the container volume is many times smaller than that of the storage container; In this case, it is provided in particular that the capacity of the container is between 5 to 20% of that of the storage container.
- FIG. 1 An embodiment of the invention is shown.
- the single figure shows schematically a hot-dip coating device with a guided through this metal strand.
- the device has a container 3 which is filled with molten coating metal 2. This may be, for example, zinc or aluminum.
- molten coating metal 2 This may be, for example, zinc or aluminum.
- To be coated metal strand 1 in the form of a steel strip passes through the container 3 in the conveying direction R vertically upward with a predetermined and constant in the process conveyor speed v.
- the inductors 5 are two oppositely disposed alternating field or traveling field inductors, which are operated in the frequency range from 2 Hz to 10 kHz and establish an electromagnetic transverse field perpendicular to the conveying direction R.
- the preferred frequency range for single-phase systems (AC field inductors) is between 2 kHz and 10 kHz, that for multi-phase systems (eg traveling field inductors) between 2 Hz and 2 kHz.
- active action is taken on the level h of the molten coating metal 2 in the container 3 via suitable means and this is used specifically to influence the process parameters and thus the quality of the coating.
- means 6 for controlling or regulating the height h of the water level are provided, it being apparent from the figure that the water level h can move within wide limits between a minimum water level h min and a maximum water level h max .
- the means 6 for controlling or regulating the height h of the water level initially consist of a measuring means 7 with which the current water level h can be measured.
- the measured by the measuring means 7 value is fed to a control or regulating device 10.
- This also maintains the desired value of the residence time t of the metal strand 1 in the coating metal 2.
- the control or regulating device 10 can influence means 8, 9 for influencing the water level h, in particular a discharge 8, with the molten coating metal 2 from the container 3 can be drained, as well as on a variable speed pump 9, can be pumped with the coating metal 2 in the container 3.
- the desired or required level h can be controlled or regulated by the control or regulating device 10.
- a storage container 11 is arranged below the container 3.
- a pipe 12 connects the outlet 8 with the storage tank 11.
- a pipe 13 is provided, in which the pump is arranged, can be pumped with the coating metal 2 from the storage tank 11 into the container 3.
- the coating bath level is thus adjusted or regulated dynamically via the outlet 8 and the pump 9. This makes it possible to use the water level h as a control variable for quality control of the coated metal strand 1.
- the associated change in the residence time t of the metal strand 1 in the coating metal 2-quality features of the metal strand 1 coated behind the coating device are set or readjusted-at a constant conveying speed v.
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Coating With Molten Metal (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10254306A DE10254306A1 (de) | 2002-11-21 | 2002-11-21 | Verfahren und Vorrichtung zur Schmelztauchbeschichtung eines Metallstranges |
DE10254306 | 2002-11-21 | ||
PCT/EP2003/011080 WO2004046412A2 (de) | 2002-11-21 | 2003-10-06 | Verfahren und vorrichtung zur schmelztauchbeschichtung eines metallstranges |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1563113A2 EP1563113A2 (de) | 2005-08-17 |
EP1563113B1 true EP1563113B1 (de) | 2008-02-27 |
Family
ID=32240231
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP03811347A Expired - Lifetime EP1563113B1 (de) | 2002-11-21 | 2003-10-06 | Verfahren und vorrichtung zur schmelztauchbeschichtung eines metallstranges |
Country Status (17)
Country | Link |
---|---|
US (1) | US20060153992A1 (ko) |
EP (1) | EP1563113B1 (ko) |
JP (1) | JP4485955B2 (ko) |
KR (1) | KR101090094B1 (ko) |
CN (1) | CN100445416C (ko) |
AT (1) | ATE387518T1 (ko) |
AU (1) | AU2003276069B2 (ko) |
BR (1) | BR0316515B1 (ko) |
CA (1) | CA2506389C (ko) |
DE (2) | DE10254306A1 (ko) |
ES (1) | ES2298625T3 (ko) |
MX (1) | MXPA05005311A (ko) |
MY (1) | MY139905A (ko) |
PL (1) | PL212670B1 (ko) |
RU (1) | RU2338809C2 (ko) |
TW (1) | TWI334451B (ko) |
WO (1) | WO2004046412A2 (ko) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
PL376865A1 (pl) * | 2003-02-27 | 2006-01-09 | Sms Demag Aktiengesellschaft | Sposób i urządzenie do zanurzeniowego powlekania taśm metalowych, zwłaszcza taśm stalowych |
DE102005012296A1 (de) * | 2005-03-17 | 2006-09-21 | Sms Demag Ag | Verfahren und Vorrichtung zum Entzundern eines Metallbandes |
MY157670A (en) * | 2006-08-30 | 2016-07-15 | Bluescope Steel Ltd | Metal-coated steel strip |
RU2488644C2 (ru) * | 2011-10-25 | 2013-07-27 | Александр Александрович Кулаковский | Устройство для нанесения покрытия на протяженное изделие |
AT520084B1 (de) * | 2017-10-03 | 2019-01-15 | Primetals Technologies Austria GmbH | Verfahren zum Betrieb einer Gieß-Walz-Verbundanlage und Gieß-Walz-Verbundanlage |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2556109B2 (fr) * | 1983-08-29 | 1986-09-12 | Comp Generale Electricite | Dispositif pour deposer en regime continu une couche de silicium polycristallin sur un ruban de carbone |
FR2592064B1 (fr) * | 1985-12-23 | 1988-02-12 | Elf Aquitaine | Dispositif pour former un bain d'un materiau semi-conducteur fondu afin d'y faire croitre un element cristallin |
DE4242380A1 (de) * | 1992-12-08 | 1994-06-09 | Mannesmann Ag | Verfahren und Vorrichtung zum Beschichten der Oberfläche von strangförmigem Gut |
KR100264257B1 (ko) * | 1995-11-10 | 2000-08-16 | 에모토 간지 | 용융금속의 유지방법 및 장치와 이를 이용한 용융아연 도금장치 및 설비 |
CA2225537C (en) * | 1996-12-27 | 2001-05-15 | Mitsubishi Heavy Industries, Ltd. | Hot dip coating apparatus and method |
DE19758140A1 (de) * | 1997-12-19 | 1999-07-08 | Mannesmann Ag | Verfahren zum Erzeugen von Metallprodukten aus Verbundwerkstoff |
DE10146791A1 (de) * | 2001-09-20 | 2003-04-10 | Sms Demag Ag | Verfahren und Vorrichtung zum Beschichten der Oberfläche von strangförmigem metallischem Gut |
DE10160949A1 (de) * | 2001-12-12 | 2003-06-26 | Sms Demag Ag | System und Verfahren zum Beschichten der Oberfläche eines Metallbandes |
-
2002
- 2002-11-21 DE DE10254306A patent/DE10254306A1/de not_active Withdrawn
-
2003
- 2003-10-03 TW TW092127409A patent/TWI334451B/zh not_active IP Right Cessation
- 2003-10-06 WO PCT/EP2003/011080 patent/WO2004046412A2/de active IP Right Grant
- 2003-10-06 MX MXPA05005311A patent/MXPA05005311A/es active IP Right Grant
- 2003-10-06 JP JP2004552472A patent/JP4485955B2/ja not_active Expired - Fee Related
- 2003-10-06 RU RU2005119289/02A patent/RU2338809C2/ru not_active IP Right Cessation
- 2003-10-06 PL PL375258A patent/PL212670B1/pl not_active IP Right Cessation
- 2003-10-06 EP EP03811347A patent/EP1563113B1/de not_active Expired - Lifetime
- 2003-10-06 CA CA2506389A patent/CA2506389C/en not_active Expired - Fee Related
- 2003-10-06 CN CNB2003801037520A patent/CN100445416C/zh not_active Expired - Fee Related
- 2003-10-06 AT AT03811347T patent/ATE387518T1/de active
- 2003-10-06 DE DE50309275T patent/DE50309275D1/de not_active Expired - Lifetime
- 2003-10-06 US US10/535,772 patent/US20060153992A1/en not_active Abandoned
- 2003-10-06 AU AU2003276069A patent/AU2003276069B2/en not_active Ceased
- 2003-10-06 KR KR1020057008836A patent/KR101090094B1/ko not_active IP Right Cessation
- 2003-10-06 BR BRPI0316515-9A patent/BR0316515B1/pt not_active IP Right Cessation
- 2003-10-06 ES ES03811347T patent/ES2298625T3/es not_active Expired - Lifetime
- 2003-11-19 MY MYPI20034438A patent/MY139905A/en unknown
Also Published As
Publication number | Publication date |
---|---|
EP1563113A2 (de) | 2005-08-17 |
BR0316515A (pt) | 2005-10-04 |
JP4485955B2 (ja) | 2010-06-23 |
TW200408725A (en) | 2004-06-01 |
CN100445416C (zh) | 2008-12-24 |
CN1729309A (zh) | 2006-02-01 |
WO2004046412A2 (de) | 2004-06-03 |
US20060153992A1 (en) | 2006-07-13 |
BR0316515B1 (pt) | 2012-11-27 |
TWI334451B (en) | 2010-12-11 |
CA2506389A1 (en) | 2004-06-03 |
ATE387518T1 (de) | 2008-03-15 |
MY139905A (en) | 2009-11-30 |
PL212670B1 (pl) | 2012-11-30 |
RU2005119289A (ru) | 2006-02-10 |
DE10254306A1 (de) | 2004-06-03 |
MXPA05005311A (es) | 2005-08-16 |
KR101090094B1 (ko) | 2011-12-07 |
ES2298625T3 (es) | 2008-05-16 |
KR20050085016A (ko) | 2005-08-29 |
RU2338809C2 (ru) | 2008-11-20 |
AU2003276069B2 (en) | 2009-01-29 |
AU2003276069A1 (en) | 2004-06-15 |
WO2004046412A3 (de) | 2004-07-29 |
CA2506389C (en) | 2011-09-13 |
PL375258A1 (en) | 2005-11-28 |
JP2006508240A (ja) | 2006-03-09 |
DE50309275D1 (de) | 2008-04-10 |
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Legal Events
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Extension state: AL LT LV MK |
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