EP1471993A1 - Dispersing device - Google Patents
Dispersing deviceInfo
- Publication number
- EP1471993A1 EP1471993A1 EP02712176A EP02712176A EP1471993A1 EP 1471993 A1 EP1471993 A1 EP 1471993A1 EP 02712176 A EP02712176 A EP 02712176A EP 02712176 A EP02712176 A EP 02712176A EP 1471993 A1 EP1471993 A1 EP 1471993A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- container
- stator
- rotor
- substances
- face
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
- B01F27/271—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/50—Mixing liquids with solids
- B01F23/53—Mixing liquids with solids using driven stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/50—Mixing liquids with solids
- B01F23/55—Mixing liquids with solids the mixture being submitted to electrical, sonic or similar energy
- B01F23/551—Mixing liquids with solids the mixture being submitted to electrical, sonic or similar energy using vibrations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
- B01F27/271—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator
- B01F27/2714—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator the relative position of the stator and the rotor, gap in between or gap with the walls being adjustable
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/85—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with two or more stirrers on separate shafts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
- B01F31/80—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
- B01F31/85—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations with a vibrating element inside the receptacle
Definitions
- the invention relates to a device for dispersing in particular liquid to viscous substance mixtures, comprising a container having one or more openings for introducing the substances to be dispersed and one or more openings for discharging the dispersed substances, and at least one rotor and a stator, wherein the at least one Rotor for the purpose of dispersing introduced into the container substances relative to the stator is rotatably mounted about a rotation axis.
- Dispersing devices of the type mentioned in the prior art are usually used to mix liquid substances with other liquid or powdery substances so that a substantially homogeneous deagglomerated mass is formed.
- the well-known Dispergier devices consistently have the disadvantage that in particular a rapid introduction of substances is not guaranteed.
- the energy input to the substances to be dispersed can only be controlled by the known dynamic devices during a dispersing process via a change in rotational speed of a rotor.
- a change in the energy input would only be possible with additional facilities such as the installation of other dispersing tools. In question would be multi-level tools or similar. For this purpose, however, a disassembly of the respective dispersing would be necessary.
- the object of the invention is therefore to provide a dispersing device by means of which, in particular, a rapid introduction of substances is made possible, wherein an energy input can be changed independently of a rotor speed.
- stator is mounted reciprocally in the direction of the axis of rotation of the rotor and by means of a displacement device within a predetermined Hub Suitees displaceable and thereby lockable in any position.
- the flange device is characterized by the feature that the stator is mounted reciprocally in the direction of the axis of rotation of the rotor and by means of a displacement device within a predetermined Hub Schlos displaced and thereby locked in any position, achieved that a dispersing device is provided by means of which by axial displacement of the stator from the dispersing an intensive pumping action is generated. This ensures that substances to be introduced according to their wetting behavior can be entered either in a high shear rate or very fast. Furthermore, the energy input into the product to be processed is influenced depending on the engagement of the stator in the dispersion zone.
- the displacement device includes a provided on the outer wall of the container sliding thread with a double external thread with two spaced to form a clearance between the spaced individual threads, wherein a both single thread covering nut along the double External thread is rotatably displaceable and the stator is connected via a guided through a slot in the container wall mandrel with the mother.
- the rotor is provided with coaxially arranged teeth.
- the coaxial teeth can support the pumping properties of the device according to the invention by their shape.
- rear-trained pump vanes may be mounted on the rotor bottom.
- the stator is provided according to preferred embodiments with coaxially arranged teeth.
- the dispersion is equipped with other tools. These may be conical or flat grinding tools.
- the coaxial toothed dispersing tools can also be designed in multiple stages.
- the stator is designed substantially as a hollow cylinder with a partially open and an open end face.
- two rotors are provided, one of which is arranged in the vicinity of the outer surface of the stator and another in the vicinity of the inner circumferential surface of the stator.
- a rotor is preferably formed substantially as a hollow cylinder with an open and a closed, a bottom forming end face, wherein the closed end face of the rotor faces the partially open end face of the stator in the operating state and wherein a rotor in the region of the open end face preferably arranged coaxially Teeth is provided.
- the partially open end face of the stator may form an outlet opening for the dispersed product.
- one or more premix vanes are provided within the container, which are mounted on a shaft which is aligned along the longitudinal axis of the container.
- the preferably hollow-cylindrical container is formed positioned vertically above, wherein above the container, a container having an upper cylindrical portion and a lower conical or spherical cutout portion is provided, wherein the conical or spherical cutout part opens into an upper part of the container, or in an open end face of the container.
- an agitator is preferably provided in the container.
- the apparatus preferably provides a piping system which opens from an opening for discharging dispersed substances in the conical or spherical part of the container, this embodiment being preferred for smaller quantities of the container becomes.
- a pipe system is alternatively or additionally provided, which opens from an opening for discharging dispersed substances in the cylindrical part of the container. This embodiment is preferred for larger quantities of the container. .
- the stator is designed as an ultrasonic sonotrode.
- the ultrasonic sonotrode can be designed substantially as a hollow cylinder with a partially open and an open end face, wherein it automatically assumes at least one waveform when introducing transversal ultrasonic vibrations in the partially open end face, in which the distance of the Cylinder wall periodically changes from the central cylinder longitudinal axis.
- FIG. 1 shows a first preferred embodiment of the device according to the invention in a cross-sectional view
- FIG. 2 shows an enlarged detail of the preferred embodiment of the device according to the invention shown in FIG. 1 in a cross-sectional view;
- FIG. 3 shows an enlarged detail of the preferred embodiment of the device according to the invention shown in FIG. 2 in a cross-sectional view.
- FIG. 4 shows an enlarged detail of the preferred embodiment of the device according to the invention shown in FIG. 3 in a cross-sectional view.
- the inventive device 100 shown in Figures 1 to 4 for dispersing particular liquid to viscous substances comprises a container 200 having an opening 210 for introducing the substances to be dispersed and an opening 220 for discharging the dispersed substances and contains two rotors 150, 160 and a stator 110, wherein the rotors 150, 160 for the purpose of dispersing introduced into the container 200 substances relative to the stator 110 'in each case by a Rotation axis 155, 165 are rotatably mounted.
- the stator 110 is essential to the invention mounted reciprocally in the direction of the axis of rotation 155 of the rotor 150 and displaceable by means of a displacement device 170 within a predetermined stroke range and can be releasably locked in any position. Due to the pumping action which is produced in the case of a displacement process effected by means of the displacement device 170, substances to be introduced can be entered very precisely controllably slowly or quickly in accordance with their wetting behavior.
- the displacement device 170 includes a provided on the outer wall of the container double external thread with two parallel spaced to form a clearance between the individual threads 171, 172, wherein a both individual threads 171, 172 covering the nut 173 along the double external thread is rotatably displaceable and the Stator 110 is connected via a guided through a slot 210 in the wall of the container 200 mandrel 220 with the nut 173.
- the two rotors 150, 160 are substantially formed as a hollow cylinder with a closed, a bottom 151, 161 forming face and an open end face 152, 162 and provided in the region of the open end face 152 of its lateral surface with coaxially arranged teeth.
- One of the rotors 150 is disposed in the vicinity of the outer circumferential surface of the stator 110 and the other rotor 160 is disposed in the vicinity of the inner circumferential surface of the stator 110.
- the stator 110 is also designed substantially as a hollow cylinder and has a partially open end face 111 and an open end face 112.
- the stator 110 is provided in the region of its lateral surface with coaxially arranged teeth, which are formed as slots in the lateral surface, which is able to pass through a substrate to be dispersed.
- premix vanes 300, 310 which are mounted on a shaft 330 which is aligned along the longitudinal axis 230 of the container 200, wherein above the container 200 a container 400 having an upper cylindrical portion 410 and a lower conical portion 420 is provided is provided, and in the container 400, a stirrer 430 is provided, wherein the conical portion 420 of the container 400 opens into an upper part 240 of the container 200.
- a piping system 500 opens from an opening 430 for discharging dispersed substances in the conical part 420 of the container 400, and another piping system 510 opens from an opening 440 for discharging dispersed substances in the cylindrical part 410 of the container 400.
- the illustrated dispersing device according to the invention has the peculiarity that the stator 110 is designed as an ultrasonic sonotrode, wherein the ultrasonic sonotrode is designed substantially as a hollow cylinder with a partially open and an open end face and assumes at least one waveform when ultrasonic vibrations are introduced the periodically changes the distance of the cylinder wall from the central cylinder longitudinal axis.
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
Description
Claims
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10204921 | 2002-02-07 | ||
DE10204921A DE10204921C1 (en) | 2002-02-07 | 2002-02-07 | Dispersing apparatus |
PCT/IB2002/000546 WO2003066203A1 (en) | 2002-02-07 | 2002-02-21 | Dispersing device |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1471993A1 true EP1471993A1 (en) | 2004-11-03 |
EP1471993B1 EP1471993B1 (en) | 2007-01-17 |
Family
ID=27674570
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP02712176A Expired - Lifetime EP1471993B1 (en) | 2002-02-07 | 2002-02-21 | Dispersing device |
Country Status (4)
Country | Link |
---|---|
US (1) | US7331540B2 (en) |
EP (1) | EP1471993B1 (en) |
DE (2) | DE10204921C1 (en) |
WO (1) | WO2003066203A1 (en) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7956623B2 (en) | 2007-02-16 | 2011-06-07 | Countlab, Inc | Container filling machine |
US8006468B2 (en) | 2008-04-14 | 2011-08-30 | Countlab Inc. | Container filling machine having vibration trays |
US8225925B2 (en) | 2008-12-02 | 2012-07-24 | Countlab Inc. | Discrete article spacing apparatus for vibration trays |
CN110694722A (en) * | 2019-10-17 | 2020-01-17 | 李洋斌 | Wall-mounted flour processing machine |
US10577186B2 (en) | 2011-08-18 | 2020-03-03 | Countlab, Inc. | Container filling machine |
Families Citing this family (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10361307A1 (en) * | 2003-11-24 | 2005-06-30 | Romaco Ag Frymakoruma | Apparatus for mixing and dispersing powder in liquid comprises tank containing rotor, into which pumps continuously feed liquid into tank through inlets and dosing unit dispenses fixed amounts of powder from above |
DE602006011824D1 (en) * | 2005-07-07 | 2010-03-11 | Rohm & Haas | Process for producing sludge |
DE202005018432U1 (en) * | 2005-11-23 | 2006-08-24 | Frymakoruma Ag | Homogenizer for viscous fluids has a central feed to two rotating concentric toothed profile rings and with flow guides to increase fluid pressure and prevent cavitation |
DE202006008820U1 (en) * | 2006-06-03 | 2006-08-17 | Frymakoruma Ag | Apparatus for dispersing and/or homogenizing liquids comprises processing unit comprising two independently rotating concentric toothed wheels driven on horizontal shafts |
KR100901429B1 (en) | 2007-07-16 | 2009-06-05 | 나노인텍 주식회사 | Apparatus for Milling and Dispersing without Clogging for Dispersion of Carbon Nano Tube |
GB2462821A (en) | 2008-08-18 | 2010-02-24 | Pa Knowledge Ltd | Extraction system and method |
DE102008045820A1 (en) * | 2008-09-05 | 2010-04-08 | Axel Wittek | Transition elements for passing a dispersion in the treatment in a rotor-stator dispersing machine |
DE102008049265B4 (en) * | 2008-09-26 | 2012-12-13 | Azo Holding Gmbh | mixer |
US20100082380A1 (en) * | 2008-09-30 | 2010-04-01 | Microsoft Corporation | Modeling and measuring value added networks |
DE102009047777A1 (en) | 2009-09-30 | 2011-04-07 | Azo Holding Gmbh | Homogenizer and homogenizer with such a homogenizer |
DE202010003100U1 (en) * | 2010-03-03 | 2010-05-12 | Mat Mischanlagentechnik Gmbh | Colloidal mixer, in particular for the treatment of building materials |
US9434487B2 (en) | 2011-09-30 | 2016-09-06 | Countlab, Inc | Container filling machine |
EP2574396B1 (en) * | 2011-09-30 | 2014-06-04 | Alfa Laval Corporate AB | Apparatus for mixing and pumping |
DE102015102261A1 (en) * | 2015-02-18 | 2016-08-18 | Netzsch Feinmahltechnik Gmbh | Mixing device and method for comminuting coarse components when discharging a product mixture from a mixing device |
DE202016000169U1 (en) * | 2016-01-14 | 2017-04-20 | Symex Gmbh & Co. Kg | Pumping and / or mixing device for conveying, homogenizing and / or dispersing flowable products |
CN105561854B (en) * | 2016-02-22 | 2018-02-09 | 上海诚兴机械电子有限公司 | With multi-layer impeller structure inner-outer circulation homogenizer |
CA3056425A1 (en) * | 2017-03-16 | 2018-09-20 | UGSI Chemical Feed, Inc. | High-capacity polymer system and method of preparing polymeric mixtures |
CN108554237B (en) * | 2018-05-09 | 2021-07-20 | 浙江中科磁业有限公司 | Homogenizing mixer |
CN111229432B (en) * | 2020-03-11 | 2021-12-07 | 平陆县秦晋石墨制品有限公司 | Multi-section combined ball mill |
CN113231132B (en) * | 2021-04-27 | 2022-08-26 | 上海达明精世化工有限公司 | Preparation method of leather fabric care agent |
DE102021209275A1 (en) * | 2021-08-24 | 2023-03-02 | A. Berents GmbH & Co. Kommanditgesellschaft | Mixing device for producing a flowable product and method for operating a mixing device |
CN114369383A (en) * | 2022-01-19 | 2022-04-19 | 广东邦荣新材料有限公司 | Environment-friendly fireproof paint coating and energy-saving production equipment thereof |
CN115041065A (en) * | 2022-06-10 | 2022-09-13 | 山东淄博沈淄耐火材料有限公司 | Novel vibration platform for producing low-heat-conduction molten tin bath bottom bricks and using method |
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CH271109A (en) | 1945-11-27 | 1950-10-15 | Separation L Emulsion Et Le Me | Apparatus for mixing fluid substances inside a tank. |
DE825084C (en) * | 1949-06-08 | 1951-12-17 | Atlas Werke Ag | Device for sonic vibration treatment of materials |
GB733693A (en) | 1952-06-30 | 1955-07-20 | Lang London Ltd | Improvements in or relating to mixing, emulsifying, and like machines |
US3420456A (en) * | 1965-04-30 | 1969-01-07 | Ulrich Christof Von Eiff | Industrial mixer |
US3583869A (en) | 1967-03-24 | 1971-06-08 | Ricoh Kk | Electrophotographic copying paper containing poly-n-vinyl-3-azo carbazole |
US3499373A (en) * | 1967-07-25 | 1970-03-10 | Polaroid Corp | Photographic apparatus |
US3514079A (en) * | 1968-01-04 | 1970-05-26 | Waukesha Foundry Co | Food emulsifying mill |
GB1500901A (en) | 1973-10-25 | 1978-02-15 | Cementation Res Ltd | Forming a colloidal suspension |
ZA806469B (en) * | 1979-10-30 | 1981-10-28 | British Rema Mfg Co Ltd | Pulverizing and classifying mill |
JPS6090052A (en) * | 1983-10-24 | 1985-05-21 | 特殊機化工業株式会社 | Recirculation type pulverizing and dispersing apparatus |
DE3417242A1 (en) * | 1984-05-10 | 1985-11-14 | Haagen & Rinau | Homogenising appliance |
JPS6438132A (en) | 1987-08-03 | 1989-02-08 | Brother Ind Ltd | Method and device for mixing adhesive |
DE4118870A1 (en) * | 1991-06-07 | 1992-12-17 | Ystral Gmbh Maschinenbau Und P | DEVICE FOR WETING AND DISPERSING POWDERS IN LIQUIDS |
US5195684A (en) * | 1992-05-06 | 1993-03-23 | Curt G. Joa, Inc. | Screenless disk mill |
EP0620039A1 (en) | 1993-04-15 | 1994-10-19 | KORUMA MASCHINENBAU GmbH | Homogenising device or similar |
DE29608713U1 (en) * | 1996-05-14 | 1996-08-08 | Wittek Axel | Dispersing device |
NL1008622C2 (en) | 1998-03-17 | 1999-09-27 | Marfil Machinery B V | Mixing apparatus with agitator comprising impeller and variable cross section impeller cage |
EP1121974B1 (en) * | 2000-01-31 | 2013-06-12 | Tetra Laval Holdings & Finance S.A. | Mixing apparatus and use |
-
2002
- 2002-02-07 DE DE10204921A patent/DE10204921C1/en not_active Expired - Lifetime
- 2002-02-21 WO PCT/IB2002/000546 patent/WO2003066203A1/en active Search and Examination
- 2002-02-21 US US10/503,964 patent/US7331540B2/en not_active Expired - Lifetime
- 2002-02-21 EP EP02712176A patent/EP1471993B1/en not_active Expired - Lifetime
- 2002-02-21 DE DE50209314T patent/DE50209314D1/en not_active Expired - Fee Related
Non-Patent Citations (1)
Title |
---|
See references of WO03066203A1 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7956623B2 (en) | 2007-02-16 | 2011-06-07 | Countlab, Inc | Container filling machine |
US8006468B2 (en) | 2008-04-14 | 2011-08-30 | Countlab Inc. | Container filling machine having vibration trays |
US8225925B2 (en) | 2008-12-02 | 2012-07-24 | Countlab Inc. | Discrete article spacing apparatus for vibration trays |
US10577186B2 (en) | 2011-08-18 | 2020-03-03 | Countlab, Inc. | Container filling machine |
CN110694722A (en) * | 2019-10-17 | 2020-01-17 | 李洋斌 | Wall-mounted flour processing machine |
Also Published As
Publication number | Publication date |
---|---|
WO2003066203A1 (en) | 2003-08-14 |
US7331540B2 (en) | 2008-02-19 |
DE50209314D1 (en) | 2007-03-08 |
EP1471993B1 (en) | 2007-01-17 |
US20060016922A1 (en) | 2006-01-26 |
DE10204921C1 (en) | 2003-10-16 |
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