EP1402099B1 - Verfahren zur herstellung eines verfestigten nonwoven aus zumindest teilweise mikrofeinen endlosfasern und nonwoven nach diesem verfahren - Google Patents

Verfahren zur herstellung eines verfestigten nonwoven aus zumindest teilweise mikrofeinen endlosfasern und nonwoven nach diesem verfahren Download PDF

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Publication number
EP1402099B1
EP1402099B1 EP02735401A EP02735401A EP1402099B1 EP 1402099 B1 EP1402099 B1 EP 1402099B1 EP 02735401 A EP02735401 A EP 02735401A EP 02735401 A EP02735401 A EP 02735401A EP 1402099 B1 EP1402099 B1 EP 1402099B1
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EP
European Patent Office
Prior art keywords
fibers
microfibers
endless
spun
nonwoven
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Revoked
Application number
EP02735401A
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English (en)
French (fr)
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EP1402099A1 (de
Inventor
Lüder GERKING
Gerold Fleissner
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Truetzschler Nonwovens GmbH
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Fleissner GmbH
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Application filed by Fleissner GmbH filed Critical Fleissner GmbH
Publication of EP1402099A1 publication Critical patent/EP1402099A1/de
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Anticipated expiration legal-status Critical
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Classifications

    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
    • D04H3/08—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating
    • D04H3/10—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between yarns or filaments made mechanically
    • D04H3/11—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between yarns or filaments made mechanically by fluid jet
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D4/00—Spinnerette packs; Cleaning thereof
    • D01D4/02—Spinnerettes
    • D01D4/025—Melt-blowing or solution-blowing dies
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00—Formation of filaments, threads, or the like
    • D01D5/08—Melt spinning methods
    • D01D5/098—Melt spinning methods with simultaneous stretching
    • D01D5/0985—Melt spinning methods with simultaneous stretching by means of a flowing gas (e.g. melt-blowing)
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4266—Natural fibres not provided for in group D04H1/425
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H18/00—Needling machines
    • D04H18/04—Needling machines with water jets
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
    • D04H3/016—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the fineness
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
    • D04H3/02—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of forming fleeces or layers, e.g. reorientation of yarns or filaments
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H5/00—Non woven fabrics formed of mixtures of relatively short fibres and yarns or like filamentary material of substantial length
    • D04H5/02—Non woven fabrics formed of mixtures of relatively short fibres and yarns or like filamentary material of substantial length strengthened or consolidated by mechanical methods, e.g. needling
    • D04H5/03—Non woven fabrics formed of mixtures of relatively short fibres and yarns or like filamentary material of substantial length strengthened or consolidated by mechanical methods, e.g. needling by fluid jet
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
    • Y10T442/60—Nonwoven fabric [i.e., nonwoven strand or fiber material]
    • Y10T442/608—Including strand or fiber material which is of specific structural definition
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
    • Y10T442/60—Nonwoven fabric [i.e., nonwoven strand or fiber material]
    • Y10T442/608—Including strand or fiber material which is of specific structural definition
    • Y10T442/614—Strand or fiber material specified as having microdimensions [i.e., microfiber]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
    • Y10T442/60—Nonwoven fabric [i.e., nonwoven strand or fiber material]
    • Y10T442/608—Including strand or fiber material which is of specific structural definition
    • Y10T442/614—Strand or fiber material specified as having microdimensions [i.e., microfiber]
    • Y10T442/62—Including another chemically different microfiber in a separate layer
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
    • Y10T442/60—Nonwoven fabric [i.e., nonwoven strand or fiber material]
    • Y10T442/608—Including strand or fiber material which is of specific structural definition
    • Y10T442/614—Strand or fiber material specified as having microdimensions [i.e., microfiber]
    • Y10T442/621—Including other strand or fiber material in a different layer not specified as having microdimensions
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
    • Y10T442/60—Nonwoven fabric [i.e., nonwoven strand or fiber material]
    • Y10T442/608—Including strand or fiber material which is of specific structural definition
    • Y10T442/614—Strand or fiber material specified as having microdimensions [i.e., microfiber]
    • Y10T442/626—Microfiber is synthetic polymer
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
    • Y10T442/60—Nonwoven fabric [i.e., nonwoven strand or fiber material]
    • Y10T442/696—Including strand or fiber material which is stated to have specific attributes [e.g., heat or fire resistance, chemical or solvent resistance, high absorption for aqueous compositions, water solubility, heat shrinkability, etc.]

Definitions

  • This fiber production process has considerable advantages over the prior art Technique using the meltblown process, which also produces microfibers.
  • the threads are very fine, they have an average diameter of about 2 microns and even with this diameter are essentially endless. Since she is not like that Meltblown process by a hot air stream, they are stretched not thermally damaged and have a high strength.
  • the threads can off made of any polymer but also from solutions according to the lyocell process become.
  • Microfibers are also called split fibers. They arise from threads that are made several polymers are spun and then z. B. by Water jets are split. But this microfiber manufacturing process is consuming.

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Nonwoven Fabrics (AREA)
  • Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
  • Multicomponent Fibers (AREA)

Description

Durch die DE-A-199 29 709 ist ein Faserherstellungsverfahren bekannt, bei dem aus einer Polymerschmelze nur eines bestimmten Polymers Fäden aus einer Vielzahl von Spinnbohrungen ausgesponnen und die ausgesponnenen Fäden durch mittels einer Beschleunigungs- wie Lavaldüse auf hohe Geschwindigkeit beschleunigte im wesentlichen kalte Gasströme verzogen werden und jeder Faden aufgrund von weiteren Herstellungsbedingungen vor dem Erstarren einen hydrostatischen Innendruck erhält, der größer ist als der umgebende Gasdruck, derart, dass jeder Faden in Längsrichtung platzt und sich in eine Vielzahl feiner Endlosfäden aufspleißt. Diese endlosen Mikrofasern können anschließend fortlaufend zu einem Nonwoven beliebiger Breite abgelegt werden.
Dieses Faserherstellungsverfahren hat erhebliche Vorteile gegenüber dem Stand der Technik nach dem Meltblownverfahren, mit dem auch Mikrofasern hergestellt werden. Die Fäden sind sehr fein, sie haben im Mittel einen Durchmesser von etwa 2 µm und sind selbst bei diesem Durchmesser im wesentlichen endlos. Da sie nicht wie beim Meltblownverfahren durch einen heißen Luftstrom, verstreckt werden, sind sie thermisch nicht geschädigt und haben eine hohe Festigkeit. Die Fäden können aus jeglichem Polymer aber auch aus Lösungen nach dem Lyocell-Verfahren hergestellt werden.
Mikrofasern sind auch sogenannte Splitfasem. Sie entstehen aus Fäden, die aus mehreren Polymeren gesponnen werden und anschließend z. B. durch Wasserstrahlen gesplittet werden. Dieses Mikrofaserherstellungsverfahren ist aber aufwendiger.
Es besteht die Notwendigkeit der Verfestigung der wie anfangs definiert hergestellten Mikrofasern.
Es ist die Idee der Erfindung dieses mit der hydrodynamischen Vernadelung zu bewirken. Diese ist hier besonders wirkungsvoll, weil diese so hergestellten sehr dünnen Endlosfasern leicht durch die Wasservernadelung verlagert und trotzt ihrer Endlosigkeit mit den benachbarten Fasern verschlungen werden können. Es entsteht ein abriebfestes Produkt, was auch gilt, wenn das Vlies nass geworden ist. Das Produkt ist nicht nur abriebfest, sondern es entsteht auch kein Pillingeffekt, da es sich um verschlungene Endlosfasern handelt, die ansonsten bei normalen Endlosfasern wegen ihrer Längsfestigkeit nur schwerlich mit Wasser verlagert werden können.
Die Anwendung des hydrodynamischen Vernadelns ist auf diesem Gebiet bereits mehrfach bekannt. Es wird bezüglich der schmelzgeblasenen Fasern auf die EP-A-0 333 228 und bezüglich Splitfasern auf die US-A-4 233 349 verwiesen. Im vorliegenden Fall ist die Anwendung der Wasservemadelung besonders vorteilhaft, weil das Produkt trotzt der endlosen Fasern mit Wasserstrahlen fest vernadelt werden kann, derart, dass ein Pillingeffekt beim späteren Benutzen des verfestigten Nonwoven nicht auftritt. Das Vlies hat eine weiche ganz gleichmäßige Oberfläche und kann deshalb für viele Anwendungszwecke in der Industrie mit großem Vorteil Verwendung finden.

Claims (5)

  1. Verfahren zur Herstellung eines verfestigten Nonwoven aus zumindest teilweise mikrofeinen Endlosfasern aus schmelzbaren Polymeren,
    a) bei dem eine Polymerschmelze nur eines bestimmten Polymers aus einer Vielzahl von Spinnbohrungen ausgesponnen und die ausgesponnenen Fäden durch mittels einer Beschleunigungs- wie Lavaldüse auf hohe Geschwindigkeit beschleunigte im wesentlichen kalte Gasströme verzogen werden und jeder Faden aufgrund von weiteren Herstellungsbedingungen vor dem Erstarren einen hydrostatischen Innendruck erhält, der größer ist als der umgebende Gasdruck, derart, dass jeder Faden in Längsrichtung platzt und sich in eine Vielzahl feiner Endlosfäden aufspleißt,
    b) kontinuierliches Ablegen dieser Mikrofasern zu einem Nonwoven beliebiger Breite
    c) und fortlaufendes Beaufschlagen dieses Vlieses mit hydrodynamischen Wasserstrahlen zum Verwirren der Mikrofasern untereinander, zum Verfestigen des Nonwoven aus den längs gespleißten Endlosfasern
    d) und Vermischen und Verbinden ggf. mit andern Fasern, die unter den Mikrofasern bereits vorgelegt sind und/oder auf die Mikrofasern anschließend abgelegt werden.
  2. Verfahren nach Anspruch 1, dadurch gekennzeichnet, dass die anderen Fasern aus natürlichen oder weiteren synthetischen Fasern - wie Stapel- und/oder Endlosfasern - bestehen.
  3. Verfahren nach Anspruch 1 oder 2, dadurch gekennzeichnet, dass die anderen Fasern aus Wood Pulpfasern ggf. zusammen mit den weiteren synthetischen Fasern bestehen.
  4. Verfestigtes Nonwoven, das zumindest teilweise aus Mikrofasern besteht,
    a) die aus einer Polymerschmelze nur eines bestimmten Polymers aus einer Vielzahl von Spinnbohrungen ausgesponnen und die ausgesponnenen Fäden durch mittels einer Beschleunigungs- wie Lavaldüse auf hohe Geschwindigkeit beschleunigte Gasströme verzogen werden und jeder Faden aufgrund von weiteren Herstellungsbedingungen vor dem Erstarren einen hydrostatischen Innendruck erhält, der größer ist als der umgebende Gasdruck, derart, dass jeder Faden in Längsrichtung platzt und sich in eine Vielzahl feiner Endlosfäden aufspleißt,
    b) und alleine oder zusammen mit anderen Fasern wie auch Stapel- und/oder Endlosfasern mittels einer hydrodynamischen Vernadelung verfestigt sind.
  5. Nonwöven nach Anspruch 4, dadurch gekennzeichnet, dass die Mikrofasern auf einer Trägerschicht aus stabileren Chemiefasern abgelegt sind und als Trennschicht für eine auf die Mikrofasern abgelegte Wood Pulpschicht dienen.
EP02735401A 2001-06-07 2002-06-04 Verfahren zur herstellung eines verfestigten nonwoven aus zumindest teilweise mikrofeinen endlosfasern und nonwoven nach diesem verfahren Revoked EP1402099B1 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10127471 2001-06-07
DE10127471A DE10127471A1 (de) 2001-06-07 2001-06-07 Verfahren zur Herstellung eines verfestigten Nonwoven aus zumindest teilweise mikrofeinen Endlosfilamenten und Nonwoven nach diesem Verfahren
PCT/EP2002/006075 WO2002099176A1 (de) 2001-06-07 2002-06-04 Verfahren zur herstellung eines verfestigten nonwoven aus zumindest teilweise mikrofeinen endlosfasern und nonwoven nach diesem verfahren

Publications (2)

Publication Number Publication Date
EP1402099A1 EP1402099A1 (de) 2004-03-31
EP1402099B1 true EP1402099B1 (de) 2005-11-30

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ID=7687382

Family Applications (1)

Application Number Title Priority Date Filing Date
EP02735401A Revoked EP1402099B1 (de) 2001-06-07 2002-06-04 Verfahren zur herstellung eines verfestigten nonwoven aus zumindest teilweise mikrofeinen endlosfasern und nonwoven nach diesem verfahren

Country Status (9)

Country Link
US (2) US20040222556A1 (de)
EP (1) EP1402099B1 (de)
JP (1) JP2004527673A (de)
CN (1) CN1330813C (de)
AT (1) ATE311493T1 (de)
DE (2) DE10127471A1 (de)
DK (1) DK1402099T3 (de)
ES (1) ES2254689T3 (de)
WO (1) WO2002099176A1 (de)

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DE10322460B4 (de) * 2003-05-16 2007-02-08 Corovin Gmbh Verfahren und Vorrichtung zur Herstellung eines Spinnvlieses aus Filamenten aus aufgeplatzten Fasern, Filamente aus aufgeplatzen Fasern und Vliesstoff
DE102006012052A1 (de) * 2006-03-08 2007-09-13 Lüder GERKING Spinnvorrichtung zur Erzeugung feiner Fäden durch Spleißen
AT505621B1 (de) * 2007-11-07 2009-03-15 Chemiefaser Lenzing Ag Vefahren zur herstellung eines wasserstrahlverfestigten produktes enthaltend cellulosische fasern
DE102009005387A1 (de) 2009-01-21 2010-07-22 Fleissner Gmbh Verbundvliesstoff sowie Verfahren und Vorrichtung zur Herstellung eines solchen Verbundvliesstoffes
DE102009010935A1 (de) 2009-02-27 2010-10-14 Fleissner Gmbh Verbundvliesstoff sowie Verfahren und Vorrichtung zur Herstellung eines solchen Verbundvliesstoffes
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DE102016010163A1 (de) * 2016-08-25 2018-03-01 Carl Freudenberg Kg Technisches Verpackungsmaterial

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Also Published As

Publication number Publication date
WO2002099176A1 (de) 2002-12-12
DE10127471A1 (de) 2002-12-12
US20040222556A1 (en) 2004-11-11
ATE311493T1 (de) 2005-12-15
ES2254689T3 (es) 2006-06-16
CN1330813C (zh) 2007-08-08
DK1402099T3 (da) 2006-03-27
DE50205125D1 (de) 2006-01-05
US20070004304A1 (en) 2007-01-04
EP1402099A1 (de) 2004-03-31
CN1513070A (zh) 2004-07-14
JP2004527673A (ja) 2004-09-09

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