EP1322814B8 - Procede de blanchiment de pates a papier - Google Patents
Procede de blanchiment de pates a papier Download PDFInfo
- Publication number
- EP1322814B8 EP1322814B8 EP01969897A EP01969897A EP1322814B8 EP 1322814 B8 EP1322814 B8 EP 1322814B8 EP 01969897 A EP01969897 A EP 01969897A EP 01969897 A EP01969897 A EP 01969897A EP 1322814 B8 EP1322814 B8 EP 1322814B8
- Authority
- EP
- European Patent Office
- Prior art keywords
- peracids
- hydrogen peroxide
- acid
- unbleached
- pulp
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title claims abstract description 39
- 238000004061 bleaching Methods 0.000 title claims abstract description 30
- 229920001131 Pulp (paper) Polymers 0.000 title claims abstract description 16
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 80
- KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000000203 mixture Substances 0.000 claims abstract description 16
- LJGHYPLBDBRCRZ-UHFFFAOYSA-N 3-(3-aminophenyl)sulfonylaniline Chemical compound NC1=CC=CC(S(=O)(=O)C=2C=C(N)C=CC=2)=C1 LJGHYPLBDBRCRZ-UHFFFAOYSA-N 0.000 claims abstract description 12
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 4
- 150000004965 peroxy acids Chemical class 0.000 claims description 37
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 31
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 30
- 235000015927 pasta Nutrition 0.000 claims description 22
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims description 16
- 239000000243 solution Substances 0.000 claims description 15
- 235000019253 formic acid Nutrition 0.000 claims description 10
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims description 8
- 238000003825 pressing Methods 0.000 claims description 7
- 239000012429 reaction media Substances 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 238000004821 distillation Methods 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims 1
- 150000004967 organic peroxy acids Chemical class 0.000 claims 1
- 239000002253 acid Substances 0.000 description 12
- 238000006116 polymerization reaction Methods 0.000 description 11
- 150000007524 organic acids Chemical class 0.000 description 10
- 150000007513 acids Chemical class 0.000 description 9
- 235000005985 organic acids Nutrition 0.000 description 9
- 239000000123 paper Substances 0.000 description 9
- 235000011054 acetic acid Nutrition 0.000 description 8
- 229920005610 lignin Polymers 0.000 description 8
- 239000000126 substance Substances 0.000 description 7
- 239000012153 distilled water Substances 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000010902 straw Substances 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 4
- 230000015556 catabolic process Effects 0.000 description 4
- 239000000460 chlorine Substances 0.000 description 4
- 229910052801 chlorine Inorganic materials 0.000 description 4
- 239000012071 phase Substances 0.000 description 4
- 239000011122 softwood Substances 0.000 description 4
- 229920003043 Cellulose fiber Polymers 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000010411 cooking Methods 0.000 description 3
- 238000006731 degradation reaction Methods 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 230000036571 hydration Effects 0.000 description 3
- 238000006703 hydration reaction Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 230000007935 neutral effect Effects 0.000 description 3
- 239000007800 oxidant agent Substances 0.000 description 3
- 238000004537 pulping Methods 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- AOSFMYBATFLTAQ-UHFFFAOYSA-N 1-amino-3-(benzimidazol-1-yl)propan-2-ol Chemical compound C1=CC=C2N(CC(O)CN)C=NC2=C1 AOSFMYBATFLTAQ-UHFFFAOYSA-N 0.000 description 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 2
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 2
- SCKXCAADGDQQCS-UHFFFAOYSA-N Performic acid Chemical class OOC=O SCKXCAADGDQQCS-UHFFFAOYSA-N 0.000 description 2
- 241000209140 Triticum Species 0.000 description 2
- 235000021307 Triticum Nutrition 0.000 description 2
- 150000001243 acetic acids Chemical class 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 239000003637 basic solution Substances 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 230000000593 degrading effect Effects 0.000 description 2
- 150000004674 formic acids Chemical class 0.000 description 2
- 239000002655 kraft paper Substances 0.000 description 2
- 238000010525 oxidative degradation reaction Methods 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 235000000346 sugar Nutrition 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 230000002087 whitening effect Effects 0.000 description 2
- 241000609240 Ambelania acida Species 0.000 description 1
- 240000000111 Saccharum officinarum Species 0.000 description 1
- 235000007201 Saccharum officinarum Nutrition 0.000 description 1
- 239000005708 Sodium hypochlorite Substances 0.000 description 1
- 240000006394 Sorghum bicolor Species 0.000 description 1
- 235000011684 Sorghum saccharatum Nutrition 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000010533 azeotropic distillation Methods 0.000 description 1
- 239000010905 bagasse Substances 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000007336 electrophilic substitution reaction Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 239000011121 hardwood Substances 0.000 description 1
- JYVHOGDBFNJNMR-UHFFFAOYSA-N hexane;hydrate Chemical compound O.CCCCCC JYVHOGDBFNJNMR-UHFFFAOYSA-N 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 150000004045 organic chlorine compounds Chemical class 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 150000003138 primary alcohols Chemical class 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000010405 reoxidation reaction Methods 0.000 description 1
- 150000003333 secondary alcohols Chemical group 0.000 description 1
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 239000005418 vegetable material Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C9/00—After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
- D21C9/10—Bleaching ; Apparatus therefor
- D21C9/16—Bleaching ; Apparatus therefor with per compounds
- D21C9/166—Bleaching ; Apparatus therefor with per compounds with peracids
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C9/00—After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
- D21C9/10—Bleaching ; Apparatus therefor
- D21C9/101—Bleaching ; Apparatus therefor in solvent medium
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C9/00—After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
- D21C9/10—Bleaching ; Apparatus therefor
- D21C9/1057—Multistage, with compounds cited in more than one sub-group D21C9/10, D21C9/12, D21C9/16
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C9/00—After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
- D21C9/10—Bleaching ; Apparatus therefor
- D21C9/16—Bleaching ; Apparatus therefor with per compounds
- D21C9/163—Bleaching ; Apparatus therefor with per compounds with peroxides
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Paper (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Claims
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0011831 | 2000-09-18 | ||
FR0011831A FR2814180B1 (fr) | 2000-09-18 | 2000-09-18 | Procede de blanchiment de pates a papier en milieu organique a hydratation controlee |
PCT/FR2001/002867 WO2002022945A1 (fr) | 2000-09-18 | 2001-09-14 | Procede de blanchiment de pates a papier |
Publications (3)
Publication Number | Publication Date |
---|---|
EP1322814A1 EP1322814A1 (fr) | 2003-07-02 |
EP1322814B1 EP1322814B1 (fr) | 2011-03-09 |
EP1322814B8 true EP1322814B8 (fr) | 2011-05-25 |
Family
ID=8854374
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP01969897A Expired - Lifetime EP1322814B8 (fr) | 2000-09-18 | 2001-09-14 | Procede de blanchiment de pates a papier |
Country Status (14)
Country | Link |
---|---|
US (1) | US6866749B2 (fr) |
EP (1) | EP1322814B8 (fr) |
CN (1) | CN1231634C (fr) |
AT (1) | ATE501305T1 (fr) |
AU (2) | AU2001290028B2 (fr) |
BR (1) | BR0113955A (fr) |
CA (1) | CA2422610C (fr) |
DE (1) | DE60144190D1 (fr) |
DK (1) | DK1322814T3 (fr) |
EA (1) | EA005240B1 (fr) |
ES (1) | ES2360503T3 (fr) |
FR (1) | FR2814180B1 (fr) |
PT (1) | PT1322814E (fr) |
WO (1) | WO2002022945A1 (fr) |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2885371B1 (fr) * | 2005-05-03 | 2007-08-03 | Cie Ind De La Matiere Vegetale | Installation pour la mise en oeuvre d'un procede de production de pate a papier, de lignines et de sucres et procede de production au moyen d'une telle installation |
FI118735B (fi) | 2005-09-13 | 2008-02-29 | Kemira Oyj | Menetelmä peroksihappojen valmistamiseksi |
FI119800B (fi) * | 2006-11-09 | 2009-03-31 | Kemira Oyj | Menetelmä mikro-organismien kasvun estämiseksi ja mikro-organismien kasvua estävä yhdistelmä |
US8871807B2 (en) | 2008-03-28 | 2014-10-28 | Ecolab Usa Inc. | Detergents capable of cleaning, bleaching, sanitizing and/or disinfecting textiles including sulfoperoxycarboxylic acids |
US8809392B2 (en) | 2008-03-28 | 2014-08-19 | Ecolab Usa Inc. | Sulfoperoxycarboxylic acids, their preparation and methods of use as bleaching and antimicrobial agents |
CA2715175C (fr) | 2008-03-28 | 2017-11-21 | Ecolab Inc. | Acides peroxycarboxyliques sulfures, leur preparation et leurs procedes d'utilisation en tant qu'agents de blanchiment et antimicrobiens |
WO2012037294A2 (fr) | 2010-09-14 | 2012-03-22 | Pimi Agro Cleantech Ltd. (Israel) | Compositions et méthodes de traitement de substances comestibles et de leurs substrats |
US8845860B2 (en) | 2010-09-16 | 2014-09-30 | Georgia-Pacific Consumer Products Lp | High brightness pulps from lignin rich waste papers |
FI123052B (fi) | 2011-09-23 | 2012-10-15 | Chempolis Oy | Esikäsittelymenetelmä vesiliukoisten sokereiden tuottamiseksi lignoselluloosamateriaalista |
US9321664B2 (en) | 2011-12-20 | 2016-04-26 | Ecolab Usa Inc. | Stable percarboxylic acid compositions and uses thereof |
AU2013240312C1 (en) | 2012-03-30 | 2018-02-01 | Ecolab Usa Inc. | Use of peracetic acid/hydrogen peroxide and peroxide-reducing agents for treatment of drilling fluids, frac fluids, flowback water and disposal water |
US8822719B1 (en) | 2013-03-05 | 2014-09-02 | Ecolab Usa Inc. | Peroxycarboxylic acid compositions suitable for inline optical or conductivity monitoring |
US20140256811A1 (en) | 2013-03-05 | 2014-09-11 | Ecolab Usa Inc. | Efficient stabilizer in controlling self accelerated decomposition temperature of peroxycarboxylic acid compositions with mineral acids |
US10165774B2 (en) | 2013-03-05 | 2019-01-01 | Ecolab Usa Inc. | Defoamer useful in a peracid composition with anionic surfactants |
FR3016359B1 (fr) | 2014-01-10 | 2022-04-29 | Arkema France | Compositions de peroxyde d'hydrogene pour la delignification de matiere vegetale et leurs utilisations |
CN117142998A (zh) | 2014-12-18 | 2023-12-01 | 艺康美国股份有限公司 | 通过多元醇甲酸酯生产过氧甲酸 |
US11040902B2 (en) | 2014-12-18 | 2021-06-22 | Ecolab Usa Inc. | Use of percarboxylic acids for scale prevention in treatment systems |
US9845290B2 (en) | 2014-12-18 | 2017-12-19 | Ecolab Usa Inc. | Methods for forming peroxyformic acid and uses thereof |
CN107604731A (zh) * | 2017-11-02 | 2018-01-19 | 山东东平容业达植物纤维科技有限公司 | 一种秸秆纤维提取过程中的漂白工艺 |
CN112312769A (zh) | 2018-06-15 | 2021-02-02 | 埃科莱布美国股份有限公司 | 用于乳头治疗的现场产生的过甲酸组合物 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3005947B1 (de) * | 1980-02-16 | 1981-01-29 | Degussa | Verfahren zur Bleiche von Zellstoffen mittels organischer Persaeure |
ATE132926T1 (de) * | 1992-07-06 | 1996-01-15 | Solvay Interox | Verfahren zur delignifizierung von chemischen zellstoffen |
US6007678A (en) * | 1992-11-27 | 1999-12-28 | Eka Nobel Ab | Process for delignification of lignocellulose-containing pulp with an organic peracid or salts thereof |
EP0862669B1 (fr) * | 1995-06-29 | 2003-05-07 | Reijo K. Salminen | Lessiveur de pate continu |
FI103899B (fi) * | 1996-11-06 | 1999-10-15 | Chempolis Oy | Menetelmä erityisen vaalean massan valmistamiseksi |
-
2000
- 2000-09-18 FR FR0011831A patent/FR2814180B1/fr not_active Expired - Fee Related
-
2001
- 2001-09-14 CN CNB018158587A patent/CN1231634C/zh not_active Expired - Lifetime
- 2001-09-14 AU AU2001290028A patent/AU2001290028B2/en not_active Expired
- 2001-09-14 EP EP01969897A patent/EP1322814B8/fr not_active Expired - Lifetime
- 2001-09-14 DE DE60144190T patent/DE60144190D1/de not_active Expired - Lifetime
- 2001-09-14 BR BR0113955-0A patent/BR0113955A/pt not_active IP Right Cessation
- 2001-09-14 PT PT01969897T patent/PT1322814E/pt unknown
- 2001-09-14 AU AU9002801A patent/AU9002801A/xx active Pending
- 2001-09-14 CA CA002422610A patent/CA2422610C/fr not_active Expired - Lifetime
- 2001-09-14 EA EA200300383A patent/EA005240B1/ru not_active IP Right Cessation
- 2001-09-14 ES ES01969897T patent/ES2360503T3/es not_active Expired - Lifetime
- 2001-09-14 WO PCT/FR2001/002867 patent/WO2002022945A1/fr active IP Right Grant
- 2001-09-14 DK DK01969897.6T patent/DK1322814T3/da active
- 2001-09-14 US US10/380,066 patent/US6866749B2/en not_active Expired - Lifetime
- 2001-09-14 AT AT01969897T patent/ATE501305T1/de active
Also Published As
Publication number | Publication date |
---|---|
AU9002801A (en) | 2002-03-26 |
US20040035537A1 (en) | 2004-02-26 |
EP1322814B1 (fr) | 2011-03-09 |
WO2002022945A1 (fr) | 2002-03-21 |
EP1322814A1 (fr) | 2003-07-02 |
CA2422610A1 (fr) | 2002-03-21 |
ATE501305T1 (de) | 2011-03-15 |
PT1322814E (pt) | 2011-05-02 |
AU2001290028B2 (en) | 2005-12-01 |
EA200300383A1 (ru) | 2003-08-28 |
CN1231634C (zh) | 2005-12-14 |
DE60144190D1 (de) | 2011-04-21 |
EA005240B1 (ru) | 2004-12-30 |
ES2360503T3 (es) | 2011-06-06 |
BR0113955A (pt) | 2003-07-22 |
DK1322814T3 (da) | 2011-06-14 |
CA2422610C (fr) | 2009-12-01 |
CN1458996A (zh) | 2003-11-26 |
FR2814180B1 (fr) | 2003-12-05 |
FR2814180A1 (fr) | 2002-03-22 |
US6866749B2 (en) | 2005-03-15 |
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