EP1198689B1 - Procede d'extraction de jus naturel de matieres vegetales ligneuses, dispositif permettant la mise en oeuvre du procede et utilisation du procede pour la production de vegetaux ligneux seches, ou de jus - Google Patents

Procede d'extraction de jus naturel de matieres vegetales ligneuses, dispositif permettant la mise en oeuvre du procede et utilisation du procede pour la production de vegetaux ligneux seches, ou de jus Download PDF

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Publication number
EP1198689B1
EP1198689B1 EP00922783A EP00922783A EP1198689B1 EP 1198689 B1 EP1198689 B1 EP 1198689B1 EP 00922783 A EP00922783 A EP 00922783A EP 00922783 A EP00922783 A EP 00922783A EP 1198689 B1 EP1198689 B1 EP 1198689B1
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EP
European Patent Office
Prior art keywords
juice
enclosure
plant matter
pressure
ligneous
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP00922783A
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German (de)
English (en)
French (fr)
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EP1198689A1 (fr
Inventor
Bernard Dedieu
Abdelaâziz BOUIRDENE
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Valeurs Bois Industrie
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Valeurs Bois Industrie
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Valeurs Bois Industrie filed Critical Valeurs Bois Industrie
Priority to DK00922783T priority Critical patent/DK1198689T3/da
Priority to SI200030584T priority patent/SI1198689T1/xx
Publication of EP1198689A1 publication Critical patent/EP1198689A1/fr
Application granted granted Critical
Publication of EP1198689B1 publication Critical patent/EP1198689B1/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B7/00—Drying solid materials or objects by processes using a combination of processes not covered by a single one of groups F26B3/00 and F26B5/00
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B3/00—Drying solid materials or objects by processes involving the application of heat
    • F26B3/32—Drying solid materials or objects by processes involving the application of heat by development of heat within the materials or objects to be dried, e.g. by fermentation or other microbiological action
    • F26B3/34—Drying solid materials or objects by processes involving the application of heat by development of heat within the materials or objects to be dried, e.g. by fermentation or other microbiological action by using electrical effects
    • F26B3/343—Drying solid materials or objects by processes involving the application of heat by development of heat within the materials or objects to be dried, e.g. by fermentation or other microbiological action by using electrical effects in combination with convection

Definitions

  • the present invention relates to a method for extracting juice natural woody plant material, device for setting process work and use of the process for the production of plants dried wood, or juice.
  • sawn wood is meant a wood which comes from directly from the first transformation (sawing).
  • L ANTTI teaches to dry wood with microwaves operating at frequencies of 915 or 2450 MHz and a power density in the range of 25 to 78 kW / m 3 to raise the interior temperature of the wood to approximately 140 ° C and achieve vapor pressure internal to 25 KPa wood. The internal pressure thus produced is very high to allow very rapid evacuation of the water.
  • the disadvantage of the process is that it develops fiber breaks. The drying process begins with rapid microwave drying at around 70 ° C, then intermittent microwave exposure during drying, and finally a drying operation by controlling the temperature of the wood below saturation. fibers, limited to a maximum temperature of 110 ° C.
  • the object of the present invention is to propose a method which allows to optimize energy and to obtain, by quantity of materials treated fibrous plants, maximum yield in the production of juice.
  • the recovery stage can be performed at least in part during the creation or injection stage of saturated water vapor.
  • the total pressure is between 1.5 and 9.6 bars.
  • the total pressure is adapted in depending on the plant material treated and the vapor temperature surrounding this matter.
  • the power of the waves is modulated to allow the material to heat up, which is a few tenths of a degree to a few degrees above the vapor temperature resulting from the total pressure selected.
  • the volume of water under pressure atmospheric and outdoor ambient temperature is equivalent to two to four times the volume of air contained in the enclosure in the same conditions.
  • the volume necessary for the pressure of saturated steam, for the selected operating temperature is the order of three times the mass of air contained in the temperature enclosure room.
  • the frequency of the waves is adapted the dimensions of the mass of plant material to be treated in the enclosure, so as to allow the penetration of waves to the heart of the mass plant to be treated.
  • the frequency of the waves is understood between 13 MHz and 2450 MHz.
  • the method comprises a step juice evacuation outside the pressure enclosure during or in progress extraction process.
  • the method comprises a step adaptation, after draining the juices, of the conditions of total pressure, temperature and power control waves to promote penetration into the wood of additive products injected into the enclosure.
  • Another object of the invention is to propose a device allowing the implementation of the process.
  • the device consists of a pressure-resistant waterproof enclosure, of a plurality of windows in quartz or any other material suitable for waves with a generator electromagnetic waves arranged near each window, so as to emit waves transversely to the mass of matter plants placed in the enclosure, a device for generating water vapor saturated under pressure above atmospheric pressure to create or inject a saturated water vapor pressure at a temperature of steam and at a total pressure determined according to the plant to be treated.
  • the device comprises means for pressurized air circulation.
  • the steam generator device allows the injection of steam under pressure at the steam temperature and at the total pressure determined.
  • the steam generator device includes in the enclosure a receptacle for receiving a quantity of water corresponding to two to four times the mass of air contained in the enclosure to outdoor ambient temperature and means of heating this water to bring it to the vapor state.
  • the heating means are controlled by a device for measuring the total pressure prevailing at the interior of the enclosure to interrupt the heating of the water when the desired pressure is reached.
  • the enclosure comprises a device for juice recovery by runoff and / or gravity of the juice extracted from the material.
  • the juice recovery device communicates by a valve with the outside of the enclosure, said valve being ordered to perform partial juice purges during machine operation.
  • the mass of vegetable matter processed in a juice extraction operation consists of a type of pressure and temperature conditions are determined in depending on the type of vegetable essence to extract the active ingredients interesting in the best conditions.
  • the woods are treated with bark or without bark directly from felling.
  • the plants are the branches and the leaves resulting from pruning.
  • a final goal is to obtain a natural juice.
  • the device consists of a enclosure (1), preferably cylindrical, of metallic material ensuring on the one hand, both good thermal insulation and watertightness pressure and secondly, sealing against waves.
  • This enclosure is open to one end through a door (16, Figure 1B) or two.
  • Openings (14) are practiced in the enclosure to constitute windows in material airtight but allowing radiation to pass through electromagnetic such as for example microwaves.
  • These windows (14) under pressure are made of a material that can withstand pressures created in the enclosure and emit the waves towards the interior of the enclosure and say emitting windows.
  • These windows (14) are large and arranged at locations where the electromagnetic waves can be sent to the entire plant mass introduced into the enclosure and up to its heart.
  • the waves are brought by a waveguide (40) to a plurality of windows arranged longitudinally and on each side at intervals regular or not along the stack of wood (3) to obtain a distribution the the most homogeneous waves possible.
  • the waveguide (40) communicates to through an impedance adapter (41) and a 3-decibel divider (42) with an insulator (43) and the electromagnetic wave generator (44) of frequency in a frequency range between 1 MHz and 16 GHz.
  • an impedance adapter (41) and a 3-decibel divider (42) with an insulator (43) and the electromagnetic wave generator (44) of frequency in a frequency range between 1 MHz and 16 GHz.
  • Stack of wood or of woody plants preferably consists of pieces (30) under form of branches, beams or planks or planks of thickness and any width, from pruning or sawing and arranged for beams, planks or planks contiguously across their width or for bundle branches in a longitudinal direction to form a layer.
  • Each layer of wood or plants is spaced from the bottom layer by battens or rods (33) arranged perpendicularly so contiguous to spare between the contiguous layers or bundles of plants of air, wave, and water circulation passages.
  • the air circulation circuit is also made of material favoring the reflection of waves towards the interior of the enclosure and the wood.
  • the speaker is connected by a pipe (15) with a steam generator system (2) and possibly an air compressor (20). Moisture comes from the generator steam by diffusion grids (13), which allows it to be diffused from homogeneously in the enclosure without risk of creating frontal attacks on wood.
  • the air compressor (20) is used to produce air tablet intended to accelerate the circulation of water in the wood and, when the steam generator system (2) cannot generate steam under enough pressure to rise to the desired temperature or to support the rise in temperature and accelerate the circulation of water from wood. However, when using a steam generator system under sufficient pressure to reach temperatures and pressures the air compressor can be omitted.
  • the enclosure has means of loading and unloading the masses of plants to treat and recovery means of juice or liquid exudate extract Plant.
  • the wheels of the carriage rest on rails (10A, 10B) integral with the bottom of the tank (1) these are provided with a device for eliminating electric arcs.
  • a grid (19) avoids the wave propagation to liquid exudates or runoff collected in the bottom of the tank.
  • This runoff is discharged by a pipe (18) controlled by a valve (17).
  • This pipeline (18) opens into a removable or drainable recovery container liquid exudates resulting from the drying process.
  • the pipeline is open permanently or intermittently.
  • the upper part of the tank has a safety valve (11) which keeps the tank at the desired pressure, releases pressure if it is too high and finally put the tank in the atmosphere once the drying process completed.
  • the tank (1) is enclosed in an enclosure (5), which communicates through the airlock of the door (16) automatically controlled at the end and at the start by a system electronic control.
  • a preloading area (50) makes it possible to bring the carriages on a pair of rails (10C, 10D) which are not related electric with the rails (10A, 10B) of the enclosure (1).
  • a device for spraying (52) allows water to be sprayed during the use phase waves to prevent any leakage of radiation to the outside.
  • a tank reserve not shown, removable and drainable is connected to the enclosure (1) by a pipe (18) and makes it possible to collect the liquid exudates resulting from drying the wood.
  • the electromagnetic wave generator (44) is buried like the tank of reserve (6) and communicates with the drying chamber (1) through the guide wave (40).
  • FIG. 3 represents a second alternative embodiment of the enclosure in which on either side of the enclosure are arranged three windows (14 I), each of the windows facing a generator microwave (43) having a power, for example, of the order of 1000 watts, this power being controlled through a respective link (431), by a control system (48) which makes it possible to adapt, for each wave, power, depending on the temperature rise that we want to create by the waves inside the plant.
  • the enclosure also has a container (45) of sufficient size to allow the capacity of a mass of water corresponding to about four times the mass of air contained in the enclosure when it is at atmospheric pressure and temperature ambient outside air.
  • a heating resistor (46) arranged in the container (45) allows the temperature of the body of water to rise and gradually bring it to the vapor state while raising the pressure inside the enclosure.
  • This resistor (46) is connected to a circuit control (47) integrated or not in the control system (48) which controls the supply of the resistor according to the temperature of saturated steam desired for processing materials and a signal pressure supplied by a pressure sensor not shown allowing providing a signal to the control circuit (47) representing a correlation between the total pressure prevailing inside the enclosure and the temperature of saturated vapor created in this enclosure by heated water.
  • the amount of water required to reach the vapor state saturating obviously depends on the temperature at which one wishes perform the treatment of the plant mass but we can consider that in the saturated vapor temperature range which varies from 90 to 170 ° C, the mass required in relation to the mass of dry air contained in the enclosure at the start is of the order of two to four times the mass of air. Well Obviously, if you put too much water, it will remain at the bottom of the container and not will not transform into a vapor state, unless it still goes up in temperature and therefore pressure.
  • the temperature of 90 ° C corresponds to a total pressure prevailing inside the enclosure of 1.5 bars.
  • pressure total means the air pressure plus the saturated vapor pressure.
  • the saturation vapor temperature of 100 ° C corresponds to a pressure total pressure of 2 bars and 170 ° C at a total pressure of 9.6 bars.
  • the desirable conditions to extract the juices had to be a total pressure greater than the atmospheric pressure, and an ambient temperature in the enclosure higher than 100 ° C. As long as the ambient temperature is below 100 ° C, the juices contain very few molecules interesting for the chemical industry. Once the ambient temperature of 100 ° C has been reached, the temperature of the pile of woody material increases and juices can be recovered if it exceeds 170 ° C and therefore; the pressure of 9.6 bars, the molecules are either altered or have been destroyed.
  • the temperature and pressure increases can be done in stages successive or according to ramps or according to cycles allowing optimization of the desired result, namely production of juice or drying of woody materials.
  • the power of electromagnetic waves will be also controlled so that a slight temperature gradient so pressure materializes from the center of the pile outwards, the generators located near the extreme areas of the battery emitting a slightly lower power.
  • the frequency of the waves electromagnetic is adapted to the dimensions of the mass of material plants to be treated in the enclosure, so as to allow the penetration of waves to the heart of the plant mass to be treated and can be chosen in the frequency range from 1 MHz to 16 GHz.
  • the frequency of the waves can be chosen in the microwave range between 400 MHz and 2450 MHz or for applications requiring high penetration of waves. Frequencies of the order of 13 or 17 MHz can be used or even between 17 and 400 MHz.
  • the species will be chosen in depending on the desired results. For example, when dealing with beech, oak pedunculate or oak, we obtain a high calcareous folin index which is the sign of the presence of molecules interesting for industry chemical.
  • the pH formed by formic and acetic acids is also higher than for juices obtained by extraction processes traditional.
  • tannins wyskiline, gaiacole, phenol, and polyphenols.
  • Phenols are the basic products for thermosetting polymers or polymers thermoplastics. Polyphenols allow the production of anti-radicals free (anti-aging products).
  • terpene or insecticides By treating willow and poplars, salicylic acid can be extracted. Pine processing Sylvan produces insecticides. Similarly, poplar, we can extract salicylic acid.
  • deacetylbaccatin 3 also known as "taxol”.
  • Laricio pine produces terpenes and / or volatile terpene alcohols, such as isobomeol serving as the basic product for essential oils (perfume) or methylvaniline (natural vanilla extract, acids non-volatile resins, such as isomers or dehydroabietics.
  • isobomeol serving as the basic product for essential oils (perfume) or methylvaniline (natural vanilla extract, acids non-volatile resins, such as isomers or dehydroabietics.
  • This process can also be applied to any other species, such as that eucalyptus, spruce or mixtures of specific species or still processing branches and leaves from pruning.
  • the process also allows, in addition to the production of juice, obtain dried plant material for other applications, such as the manufacture of poles, dried wooden barriers or the use of other parts of dried plants as additives in for example the manufacture of insulating materials.
  • any transfer device can be used in place of the rail-mounted cart.
  • devices control and regulation will initiate the phases successive steps of the process in combination with more automation where less push.
  • the enclosure has a safety valve (11) allowing the enclosure to be vented, either at the end of the process or excess pressure detected by the control system.
EP00922783A 1999-04-30 2000-04-28 Procede d'extraction de jus naturel de matieres vegetales ligneuses, dispositif permettant la mise en oeuvre du procede et utilisation du procede pour la production de vegetaux ligneux seches, ou de jus Expired - Lifetime EP1198689B1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
DK00922783T DK1198689T3 (da) 1999-04-30 2000-04-28 Fremgangsmåde til udvinding af naturlig saft fra træagtige plantematerialer, apparat til udförelse af fremgangsmåden og anvendelse af fremgangsmåden til fremstilling af törret, træagtigt plantemateriale eller salt
SI200030584T SI1198689T1 (en) 1999-04-30 2000-04-28 Method for extracting the natural juice of ligneous plant material, device for carrying out said method and use of said method in the production of dried ligneous plant material

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR9905555A FR2793008B1 (fr) 1999-04-30 1999-04-30 Procede d'extraction de jus naturel de matieres vegetales ligneuses, dispositif permettant la mise en oeuvre du procede et utilisation du procede pour la production de vegetaux ligneux seches
FR9905555 1999-04-30
PCT/FR2000/001141 WO2000066960A1 (fr) 1999-04-30 2000-04-28 Procede d'extraction de jus naturel de matieres vegetales ligneuses, dispositif permettant la mise en oeuvre du procede et utilisation du procede pour la production de vegetaux ligneux seches, ou de jus

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Publication Number Publication Date
EP1198689A1 EP1198689A1 (fr) 2002-04-24
EP1198689B1 true EP1198689B1 (fr) 2004-11-17

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EP00922783A Expired - Lifetime EP1198689B1 (fr) 1999-04-30 2000-04-28 Procede d'extraction de jus naturel de matieres vegetales ligneuses, dispositif permettant la mise en oeuvre du procede et utilisation du procede pour la production de vegetaux ligneux seches, ou de jus

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US (1) US6581299B1 (ko)
EP (1) EP1198689B1 (ko)
JP (1) JP2002542941A (ko)
KR (1) KR100691536B1 (ko)
CN (2) CN1134641C (ko)
AT (1) ATE282809T1 (ko)
AU (1) AU771622B2 (ko)
BR (1) BR0010172B1 (ko)
CA (1) CA2370347C (ko)
DE (1) DE60015978T2 (ko)
EA (2) EA200200644A1 (ko)
ES (1) ES2233363T3 (ko)
FR (1) FR2793008B1 (ko)
HU (1) HU225731B1 (ko)
MX (1) MXPA01011042A (ko)
NO (1) NO20015315L (ko)
NZ (1) NZ515836A (ko)
OA (1) OA11880A (ko)
PL (1) PL351928A1 (ko)
PT (1) PT1198689E (ko)
WO (1) WO2000066960A1 (ko)
ZA (1) ZA200108919B (ko)

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KR100716450B1 (ko) * 2006-01-16 2007-05-09 임성근 알로에 유액(油液) 추출방법
JP5211429B2 (ja) * 2006-03-02 2013-06-12 東京電力株式会社 マイクロ波を用いた精油抽出装置
JP4923649B2 (ja) * 2006-03-17 2012-04-25 東京電力株式会社 マイクロ波を利用した植物バイオマス処理システム
JP4830749B2 (ja) * 2006-09-20 2011-12-07 東京電力株式会社 小型抽出装置
CN101290277B (zh) * 2007-04-20 2011-05-11 财团法人食品工业发展研究所 利用微波辐射的快速提取方法
TW200842336A (en) * 2007-04-26 2008-11-01 Food Industry Res & Dev Inst Microwave accelerating extraction equipment
JP5420858B2 (ja) * 2007-06-14 2014-02-19 仁 村上 黒液処理方法及び黒液処理装置並びに発電システム
JP2009029796A (ja) * 2007-07-04 2009-02-12 Hitoshi Murakami 多糖類由来化合物の生成方法並びに生成装置
US20120160837A1 (en) 2010-12-23 2012-06-28 Eastman Chemical Company Wood heater with enhanced microwave launch efficiency
CN103115481B (zh) * 2012-03-30 2016-04-13 北京林业大学 一种木材干燥设备及利用该设备干燥木材的方法
CN102721265B (zh) * 2012-06-28 2014-10-15 罗泽云 物料干燥方法及其干燥系统
KR101361756B1 (ko) * 2013-05-29 2014-02-12 허진희 편백오일의 추출방법
CN104019648A (zh) * 2014-06-25 2014-09-03 苏州创维晟自动化科技有限公司 一种电磁导热油式木材单板烘干机
WO2017015529A1 (en) 2015-07-22 2017-01-26 The University Of North Carolina At Chapel Hill Fluidic devices with freeze-thaw valves with ice-nucleating agents and related methods of operation and analysis
TWI610053B (zh) * 2015-12-31 2018-01-01 遠東科技大學 結合天氣判斷之自動乾燥系統
KR101651628B1 (ko) * 2016-01-25 2016-08-30 백제홍삼 주식회사 참나무 수액 채취방법 및 장치
US10588786B2 (en) * 2016-05-19 2020-03-17 The Procter & Gamble Company Method and apparatus for microwave product treatment
CL2017001517A1 (es) * 2017-06-13 2017-10-06 Univ De Concepción Proceso de disolución selectiva de componentes de corteza de especies arbóreas.
WO2018229448A1 (fr) * 2017-06-16 2018-12-20 Volfart David Procédé de traitement fongicide et/ou insecticide d'un élément contenu dans une enceinte et dispositif pour sa mise en œuvre
FR3067606A1 (fr) * 2017-06-16 2018-12-21 David Volfart Procede de traitement fongicide et/ou insecticide d'un element contenu dans une enceinte et dispositif pour sa mise en œuvre
CN107576149A (zh) * 2017-07-24 2018-01-12 张家界湘汇生物有限责任公司 一种植物提取产品的干燥方法
CN107525356A (zh) * 2017-08-11 2017-12-29 中南林业科技大学 樟木汽化水蒸汽干燥及精油与余热回收装置及使用方法
CN109331500B (zh) * 2018-12-19 2020-12-15 涂乙芬 一种环绕式超声波提取装置

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Publication number Publication date
AU771622B2 (en) 2004-04-01
EP1198689A1 (fr) 2002-04-24
MXPA01011042A (es) 2003-06-30
KR20020012193A (ko) 2002-02-15
HUP0201148A2 (en) 2002-07-29
CN1357096A (zh) 2002-07-03
CA2370347C (fr) 2007-07-24
ES2233363T3 (es) 2005-06-16
AU4306600A (en) 2000-11-17
ZA200108919B (en) 2003-03-26
NZ515836A (en) 2003-03-28
US6581299B1 (en) 2003-06-24
EA200200644A1 (ru) 2003-10-30
BR0010172A (pt) 2002-06-04
CN1515391A (zh) 2004-07-28
ATE282809T1 (de) 2004-12-15
PT1198689E (pt) 2005-04-29
DE60015978D1 (de) 2004-12-23
HU225731B1 (en) 2007-07-30
CA2370347A1 (fr) 2000-11-09
DE60015978T2 (de) 2005-11-03
OA11880A (fr) 2006-03-28
FR2793008B1 (fr) 2001-07-27
JP2002542941A (ja) 2002-12-17
WO2000066960A1 (fr) 2000-11-09
FR2793008A1 (fr) 2000-11-03
NO20015315L (no) 2001-12-28
EA200101146A1 (ru) 2002-04-25
BR0010172B1 (pt) 2010-11-03
CN1134641C (zh) 2004-01-14
NO20015315D0 (no) 2001-10-30
PL351928A1 (en) 2003-07-14
EA003071B1 (ru) 2002-12-26
KR100691536B1 (ko) 2007-03-09

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