EP1185609B1 - Verfahren zur herstellung flüssiger reinigungs- oder waschmittelzusammensetzungen - Google Patents

Verfahren zur herstellung flüssiger reinigungs- oder waschmittelzusammensetzungen Download PDF

Info

Publication number
EP1185609B1
EP1185609B1 EP00942070A EP00942070A EP1185609B1 EP 1185609 B1 EP1185609 B1 EP 1185609B1 EP 00942070 A EP00942070 A EP 00942070A EP 00942070 A EP00942070 A EP 00942070A EP 1185609 B1 EP1185609 B1 EP 1185609B1
Authority
EP
European Patent Office
Prior art keywords
composition
preliminary mixture
preliminary
water
substance
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP00942070A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP1185609A1 (de
Inventor
Edgar Endlein
Mike Kosub
Karl-Ludwig Gibis
Roger Kaiser
Alexandra Hary
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Reckitt Benckiser NV
Original Assignee
Reckitt Benckiser NV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Reckitt Benckiser NV filed Critical Reckitt Benckiser NV
Publication of EP1185609A1 publication Critical patent/EP1185609A1/de
Application granted granted Critical
Publication of EP1185609B1 publication Critical patent/EP1185609B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/835—Mixtures of non-ionic with cationic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0094—Process for making liquid detergent compositions, e.g. slurries, pastes or gels
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0008—Detergent materials or soaps characterised by their shape or physical properties aqueous liquid non soap compositions
    • C11D17/0017—Multi-phase liquid compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/62—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/722—Ethers of polyoxyalkylene glycols having mixed oxyalkylene groups; Polyalkoxylated fatty alcohols or polyalkoxylated alkylaryl alcohols with mixed oxyalkylele groups

Definitions

  • the alternative of separate formulation and filling of the plurality, preferably two phases, so that the multiphase product is obtained only at this stage provides not a satisfactory solution to the problem described, since each of the two phases on Equilibrium point and therefore any slight change in e.g. Pressure, temperature, etc. could influence the equilibrium so that corresponding multiphase precursors would arise where the same processing difficulties would arise, as described above.
  • the invention is therefore based on the object, a method for producing the generic To provide compositions that overcomes these problems.
  • this object is achieved in that at least two separate premixes be prepared in the temperature range of 0 ° C to 40 ° C no phase separation and these premixes only at or immediately before bottling Packaging container are mixed together.
  • a first premix besides the main constituent water, the substance (s) of the total composition contains, omitting the formation of separate aqueous phases of the Substance is substantially omitted, the remaining ingredients of the Total composition in a second premix, also together with the Main ingredient water, are included.
  • the distribution of the ingredients of the composition in the aqueous premixes depends of course, to a great extent, of the ingredients of the overall composition yourself off. Since it is not always clear from the start which connections or combinations of compounds are responsible for ensuring that the overall composition undergoes the desired phase separation, will be required in individual cases, to determine the composition of the premix by appropriate tests, wherein Their implementation is based on the knowledge of the effect of the individual compounds in the Total composition and its limited number for the skilled person readily and particular without their own inventive step is possible.
  • Example 1 For an alkaline product, as described for example in Example 1 below is the expert would be particularly hydrophobic due to the ingredients used Materials or those water-soluble compounds that have a low cloud point have, take in the first premix.
  • This could be, for example the perfume (s) or hydrophobic water-insoluble solvent (s) or alcohol or the quaternary ammonium salts or surfactants based on ethylene oxide and propylene oxide, which are known to have a low cloud point despite water solubility have to be that from the rest of the formulation, especially the builder system (Chloride, carbonate, phosphate) to separate.
  • the quaternary ammonium salt which was sufficient to produce two stable premixes.
  • a concrete solution lies in the formation of hydrophobic material that is the combination of sulfonate and quaternary ammonium salt in the overall composition, To avoid by one of these two substances or groups of substances in the first premix is separated into it.
  • the sulfonate was selected for this purpose. But you would also have the two quaternary ammonium salts in the first premix remove it and leave the sulfonate in the second premix.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)
EP00942070A 1999-06-14 2000-06-14 Verfahren zur herstellung flüssiger reinigungs- oder waschmittelzusammensetzungen Expired - Lifetime EP1185609B1 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19926925 1999-06-14
DE19926925A DE19926925A1 (de) 1999-06-14 1999-06-14 Verfahren zur Herstellung flüssiger Reinigungs- oder Waschmittelzusammensetzungen
PCT/EP2000/005475 WO2000077154A1 (de) 1999-06-14 2000-06-14 Verfahren zur herstellung flüssiger reinigungs- oder waschmittelzusammensetzungen

Publications (2)

Publication Number Publication Date
EP1185609A1 EP1185609A1 (de) 2002-03-13
EP1185609B1 true EP1185609B1 (de) 2004-09-29

Family

ID=7911087

Family Applications (1)

Application Number Title Priority Date Filing Date
EP00942070A Expired - Lifetime EP1185609B1 (de) 1999-06-14 2000-06-14 Verfahren zur herstellung flüssiger reinigungs- oder waschmittelzusammensetzungen

Country Status (13)

Country Link
US (1) US6841528B2 (es)
EP (1) EP1185609B1 (es)
CN (1) CN1203166C (es)
AT (1) ATE278005T1 (es)
AU (2) AU771578B2 (es)
BR (1) BR0011657A (es)
CA (1) CA2375469C (es)
DE (2) DE19926925A1 (es)
ES (1) ES2225168T3 (es)
MX (1) MXPA01012861A (es)
PL (1) PL193106B1 (es)
WO (1) WO2000077154A1 (es)
ZA (1) ZA200200219B (es)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2401110A (en) * 2003-05-02 2004-11-03 Reckitt Benckiser Inc Liquid hard surface cleaning agent
US7288513B2 (en) * 2005-04-14 2007-10-30 Illinois Tool Works, Inc. Disinfecting and sanitizing article for hands and skin and hard surfaces
DE102005061726A1 (de) * 2005-12-21 2007-07-05 Henkel Kgaa Wasch-, Spül- oder Reinigungsmittel mit vertikaler Phasengrenze
DE102006013104A1 (de) * 2006-03-20 2007-09-27 Henkel Kgaa Mehrphasiges Wasch-, Spül- oder Reinigungsmittel mit vertikalen Phasengrenzen

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA783534A (en) 1965-06-15 1968-04-23 Unilever Limited Liquid detergent compositions
LU55174A1 (es) * 1967-12-28 1969-08-08 Unilever Nv
US4107067A (en) 1976-06-25 1978-08-15 The Procter & Gamble Company Detergent composition
US4348292A (en) * 1980-10-17 1982-09-07 Walton-March, Inc. Multi-layered liquid detergent-builder concentrate compositions which on addition to water produce stable cleaning solutions
GB8303014D0 (en) * 1983-02-03 1983-03-09 Reckitt & Colmann Prod Ltd Liquid cleansing composition
JPS60243199A (ja) 1984-05-17 1985-12-03 ライオン株式会社 分離型液体洗浄剤組成物
GB8421196D0 (en) * 1984-08-21 1984-09-26 Reckitt & Colmann Prod Ltd Cleansing compositions
US4749516A (en) * 1985-09-24 1988-06-07 S. C. Johnson & Son, Inc. Anionic emulsion pre-spotting composition
IT1200285B (it) 1986-08-12 1989-01-12 Mira Lanza Spa Detersivo liquido non acquoso e procedimento per la sua fabbricazione
US5883065A (en) 1996-01-22 1999-03-16 The Procter & Gamble Company Phase separated detergent composition
ATE250919T1 (de) * 1996-08-02 2003-10-15 Plum Kemi Produktion As Oel-im-wasser emulsion zur gruendlichen reinigung,zum schutz oder verbesserung der haut
ES2200994T3 (es) * 1998-03-16 2004-03-16 Henkel Kommanditgesellschaft Auf Aktien Empleo de un agente de limpieza acuoso polifasico para la limpieza de superficies duras.
DE19811386A1 (de) * 1998-03-16 1999-09-23 Henkel Kgaa Wäßriges mehrphasiges Reinigungsmittel
DE19811387A1 (de) 1998-03-16 1999-09-23 Henkel Kgaa Flüssiges mehrphasiges Reinigungsmittel
DE19951635A1 (de) * 1999-10-26 2001-05-17 Henkel Kgaa Wäßriges mehrphasiges Reinigungsmittel

Also Published As

Publication number Publication date
DE19926925A1 (de) 2000-12-21
AU771578B2 (en) 2004-03-25
ATE278005T1 (de) 2004-10-15
AU2004201801A1 (en) 2004-05-27
US6841528B2 (en) 2005-01-11
BR0011657A (pt) 2002-03-26
CA2375469A1 (en) 2000-12-21
MXPA01012861A (es) 2002-09-02
CA2375469C (en) 2008-12-02
ES2225168T3 (es) 2005-03-16
CN1355838A (zh) 2002-06-26
EP1185609A1 (de) 2002-03-13
PL352275A1 (en) 2003-08-11
US20020077268A1 (en) 2002-06-20
AU5682000A (en) 2001-01-02
DE50008006D1 (de) 2004-11-04
PL193106B1 (pl) 2007-01-31
ZA200200219B (en) 2003-06-25
CN1203166C (zh) 2005-05-25
WO2000077154A1 (de) 2000-12-21

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