EP0776314B1 - Verfahren zum befüllen von behältern mit einer unter druck stehenden flüssigkeit - Google Patents
Verfahren zum befüllen von behältern mit einer unter druck stehenden flüssigkeit Download PDFInfo
- Publication number
- EP0776314B1 EP0776314B1 EP96916004A EP96916004A EP0776314B1 EP 0776314 B1 EP0776314 B1 EP 0776314B1 EP 96916004 A EP96916004 A EP 96916004A EP 96916004 A EP96916004 A EP 96916004A EP 0776314 B1 EP0776314 B1 EP 0776314B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- filling
- liquid
- pressure
- control device
- measured
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Revoked
Links
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
- B67C3/02—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
- B67C3/20—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus with provision for metering the liquids to be introduced, e.g. when adding syrups
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
- B67C3/02—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
- B67C3/20—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus with provision for metering the liquids to be introduced, e.g. when adding syrups
- B67C3/202—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus with provision for metering the liquids to be introduced, e.g. when adding syrups by weighing
Definitions
- the invention is based on a method for filling Containers with a liquid under pressure the genus of claim 1. From JP 10 46 392 B4 Such a method has already become known. At This procedure uses the fluid pressure after opening of a filling valve measured once, whereupon a Control device based on the measured Liquid pressure a filling time or opening time for the Filling valve calculated for a certain filling quantity.
- a disadvantage of the known method is that during the Filling process occurring pressure fluctuations that lead to a Do not change the flow rate at the filling valve be taken into account. The fill quantities also remain during the opening and closing process of the filling valve disregarded. The accuracy of the known Filling process is therefore limited.
- the method according to the invention for filling containers with a pressurized liquid with the characteristic features of claim 1 has in contrast the advantage that it works very precisely. This will achieved according to the invention in that the liquid pressure is constantly measured during the filling process, so that occurring pressure fluctuations are taken into account.
- the flow rates during the Opening and closing process of the filling valve is detected, and be taken into account when calculating the filling volumes.
- the Conveying device 11 has a screw conveyor 12 for intermittent or continuous transport of the Packaging container 10 on.
- the packaging container 10 stand and slide on rail sections 13 to 15. Between the rail sections 13 and 14 or 14 and 15 one controllable via a reject device 16 Weighing device 17, 18 for one packaging container each 10 arranged, one of which 17 the tare weight G1, and the other 18 the gross weight G2 the Packaging container 10 detected and a control device 19th as input variable.
- control device 19 are, for example product-specific data, such as the viscosity curve of the Fluid over temperature as well as device data saved.
- product-specific data such as the viscosity curve of the Fluid over temperature
- device data saved With the control device 19 is an input / output unit 20 connected, in particular a Target filling quantity M or a target filling weight of Packaging container 10 to the control device 19th can be entered.
- the Filling device 22 includes a cyclical transport the packaging container 10 one of the number of each conveying cycle to be filled packaging container 10 corresponding number of Filling heads 23, for example six, each one on and have removable hollow filling needle 24. Every filling head 23 is with a metering valve 25 for the liquid coupled, with all metering valves 25 of the Control device 19 can be controlled synchronously together.
- the metering valves 25 are connected to a via short lines 26 common tubular manifold 30 connected in the one Liquid pressure P1 prevails.
- the distributor 30 is in turn via a line 33 and a Quick release device 34 with a storage container 35 for the liquid connected.
- the pressure drop between the with the liquid fully filled manifold 30 and individual metering valves 25 is, for example, by a Arrangement of the metering valves 25 in the same vertical Distance to the distributor 30 always the same size, and in the Control device 10 stored as a factor.
- the reservoir 35 is a Pressure line 36 is pressurized with a gas pressure P2.
- Pressure P2 generally increases the pressure Liquid at the metering valves 25, and thus a large one Outflow rate from the reservoir 35 enables which is especially the case with highly viscous liquids Flow behavior favors.
- a temperature sensor 31 for detection is in the distributor 30 a liquid temperature T and a pressure sensor 32 for Detection of the liquid pressure P1 arranged.
- the two Sensors 31, 32 are also connected to the control device 19 connected.
- the liquid pressure P1 continuously at certain time intervals ⁇ t, for example every 150 ⁇ sec. until every 250 ⁇ sec. measured, and supplied to the control device 19 as an input variable becomes.
- the duration of the time intervals ⁇ t between the individual Measurements of fluid pressure P1 should be chosen this way be that even during the opening and closing process of the metering valves 25 detects liquid pressures P1, and on the control device 19 are forwarded. From these For reasons there is a value for ⁇ t of 200 ⁇ sec. proven, the adequate resolution even during opening and Closing process of the filling valves 25 guaranteed.
- the device described above works as follows:
- the packaging container 10 are from the screw conveyor 21 fed to the filling device 22 in cycles.
- the filling needles 24 of the Filling heads 23 lowered and into the packaging container 10 introduced.
- a corresponding Control signal Z to the metering valves 25 through the Control device 19 the filling of the target filling quantity M in the Packaging container 10 initiated, i.e. the control signal Z, for example, energizes a coil in the Metering valve 25 so that its needle lifts off the valve seat.
- the calculation of the filled filling quantity M (ist), and thus the duration of the control signal Z to the metering valves 25 takes place in that the control device 19th continuous partial volumes ⁇ M calculated and during the duration of the control signal Z are added up.
- the partial volumes ⁇ M are calculated from the time intervals ⁇ t between the individual measurements of the liquid pressures P1, the respective the value supplied to the control device 19 Fluid pressure of P1, as well as one in the Control device 19 stored functional relationship k (p1) between the respective value of P1 and the resulting value in the Dosing valves 25 resulting flow rate per Time unit.
- This limit value M (max) which causes the control signal Z to end, is in the simplest case the desired filling quantity M itself.
- the limit value M (max) stored in the control device 19 can also be selected to be smaller in accordance with the closing characteristics of the filling valves 25, so that for example, the filling quantity or the partial volumes .DELTA.M are also taken into account that enter the containers 10 during the closing process (after the control signal Z has failed) of the metering valves 25. This means that in this case the limit value M (max) is smaller than the target filling quantity M.
- Control device 19 The accuracy of the partial volume calculation ⁇ M Control device 19 is by taking into account the Temperature sensor 31 detected temperature T of the liquid elevated. This is achieved in that Control device 19 for the flow / viscosity characteristics the respective liquid are stored so that for Calculation of the individual partial volumes ⁇ M additionally on the corresponding temperature-corrected functional context k is accessed, i.e. the value of factor k is also depends on the temperature [k (P1, T)].
- the filling needles 24 are introduced through the Filling heads 23 again from the packaging containers 10 lifted out. Then the packaging container 10 by the conveyor screw 12 cyclically another Processing station, for example a sealing station, promoted. At the same time repeats itself for new in the Filling machine conveyed packaging container 10 the process as described above.
- the value is sufficient of the liquid pressure P1 only during the actual one Filling process. Usually and for Control purposes in the event of any malfunction of the Filling machine, however, the fluid pressure P1 becomes constant measured and fed to the control device 19.
- the time intervals ⁇ t it is also conceivable for the time intervals ⁇ t to be so large to choose that the opening and closing of the Dosing valves 25 with respect to the partial volumes ⁇ M no longer is taken into account exactly, and in this case for opening and closing the metering valves 25 fixed partial volumes ⁇ M (fixed) (according to the metering valve characteristics) to assume. Even in this case, the accuracy improved compared to known filling methods because Pressure fluctuations during the actual filling be taken into account.
Landscapes
- Filling Of Jars Or Cans And Processes For Cleaning And Sealing Jars (AREA)
- Basic Packing Technique (AREA)
Description
Claims (8)
- Verfahren zum Befüllen von Behältern (10) mit einer unter Druck (P1) stehenden Flüssigkeit, bei der die Flüssigkeit aus einem Vorratsbehälter (35) mittels jeweils einem Füllventil (25) dem jeweiligen Behälter (10) zugeführt wird, wobei der Druck (P1) der Flüssigkeit gemessen, und einer Steuereinrichtung (19) zugeleitet wird, welche aus dem gemessenen Druck (P1) der Flüssigkeit und der abzufüllenden Sollfüllmenge (M) das Füllventil (25) mittels eines Ansteuersignales (Z) ansteuert, dadurch gekennzeichnet, daß der Druck (P1) der Flüssigkeit kontinuierlich in bestimmten Zeitabständen (Δt) während des Füllvorganges durch das Füllventil (25) gemessen wird, daß die Steuereinrichtung (19) die tatsächlich abgefüllte Füllmenge (M (ist)) aus einer Aufsummierung von Teilvolumina (ΔM) berechnet, welche sich unter Berücksichtigung des jeweils gemessenen Drucks (P1) der Flüssigkeit, den Zeitabständen (Δt) zwischen den einzelnen Druckmessungen und einer Druck/Durchflußkenncharakteristik (k) des Füllventils (25) ergibt, und daß die Steuereinrichtung (19) beim Überschreiten einer Grenzfüllmenge (M (max)) das Ansteuersignal (Z) an das Dosierventil (25) stoppt.
- Verfahren nach Anspruch 1, dadurch gekennzeichnet, daß die Zeitabstände (Δt) zwischen den einzelnen Messungen des Drucks (P1) der Flüssigkeit konstant sind.
- Verfahren nach Anspruch 2, dadurch gekennzeichnet, daß die Zeitabstände (Δt) zwischen 150 µsec und 250 µsec, bevorzugt 200 µsec betragen.
- Verfahren nach einem der Ansprüche 1 bis 3, dadurch gekennzeichnet, daß während der gesamten Betriebsdauer einer Füllmaschine der Druck (P1) der Flüssigkeit gemessen wird.
- Verfahren nach einem der Ansprüche 1 bis 4, dadurch gekennzeichnet, daß das Ansteuersignal (Z) zum Betätigen des Füllventils (25) bei einer Grenzfüllmenge (M (max)) gestoppt wird, die kleiner als die Sollfüllmenge (M) ist.
- Verfahren nach einem der Ansprüche 1 bis 4, dadurch gekennzeichnet, daß das Ansteuersignal (Z) zum Betätigen des Füllventils (25) bei einer Grenzfüllmenge (M (max)) gestoppt wird, die der Sollfüllmenge (M) entspricht.
- Verfahren nach einem der Ansprüche 1 bis 6, dadurch gekennzeichnet, daß für den Öffnungs- und Schließvorgang des Füllventils (25) vorgegebene Volumina (ΔM fest) angenommen werden, so daß während des Öffnens und Schließens des Füllventils keine Teilvolumina (ΔM) berechnet werden.
- Verfahren nach einem der Ansprüche 1 bis 7, dadurch gekennzeichnet, daß die Teilvolumina (ΔM) unter Berücksichtigung einer in der Flüssigkeit mittels eines Temperatursensors (31) gemessenen Temperatur (T) berechnet werden.
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP150670/95 | 1995-06-16 | ||
JP15067095 | 1995-06-16 | ||
JP7150670A JP2633820B2 (ja) | 1995-06-16 | 1995-06-16 | 液体の圧力充填方法 |
PCT/DE1996/001037 WO1997000224A1 (de) | 1995-06-16 | 1996-06-13 | Verfahren zum befüllen von behältern mit einer unter druck stehenden flüssigkeit |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0776314A1 EP0776314A1 (de) | 1997-06-04 |
EP0776314B1 true EP0776314B1 (de) | 2000-05-03 |
Family
ID=15501916
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP96916004A Revoked EP0776314B1 (de) | 1995-06-16 | 1996-06-13 | Verfahren zum befüllen von behältern mit einer unter druck stehenden flüssigkeit |
Country Status (7)
Country | Link |
---|---|
US (1) | US5823234A (de) |
EP (1) | EP0776314B1 (de) |
JP (1) | JP2633820B2 (de) |
DE (1) | DE59605120D1 (de) |
ES (1) | ES2147378T3 (de) |
TR (1) | TR199700101T1 (de) |
WO (1) | WO1997000224A1 (de) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101817493A (zh) * | 2010-03-16 | 2010-09-01 | 广州达意隆包装机械股份有限公司 | 换向控制阀、换向式定量灌装机及其灌装方法 |
DE102013100702A1 (de) * | 2013-01-24 | 2014-07-24 | Endress + Hauser Process Solutions Ag | Steuermodul für eine Abfüllanlage |
Families Citing this family (35)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3844029B2 (ja) * | 1997-09-19 | 2006-11-08 | 澁谷工業株式会社 | 液体の圧力充填方法と充填装置 |
IT1304458B1 (it) * | 1998-07-24 | 2001-03-19 | Azionaria Costruzioni Acma Spa | Metodo e serbatoio per l'erogazione di sostanze liquide all'internodi contenitori. |
DE19844011C1 (de) * | 1998-09-25 | 2000-03-09 | Bosch Gmbh Robert | Vorrichtung zum Abfüllen einer unter Druck stehenden pharmazeutischen Flüssigkeit in Verpackungsbehälter |
DE19917441C2 (de) * | 1999-04-17 | 2001-10-11 | Bosch Gmbh Robert | Vorrichtung zum Dosieren und Abfüllen einer Flüssigkeit in Verpackungsbehälter |
US6145552A (en) * | 1999-09-16 | 2000-11-14 | Multi-Fill, Inc. | Particulate product following system and method |
US6689621B2 (en) * | 2000-11-29 | 2004-02-10 | Liquid Logic, Llc | Fluid dispensing system and valve control |
ITVI20030170A1 (it) * | 2003-09-11 | 2005-03-12 | Franco Stocchiero | Piano di trattamento per impianto di formazione di batterie |
ITBO20040625A1 (it) * | 2004-10-13 | 2005-01-13 | Marchesini Group Spa | Metodo per la pesatura statistica del prodotto immesso in contenitori e similari, in una linea di riempimento |
US7182110B2 (en) * | 2005-04-25 | 2007-02-27 | Roebuck John T | Fluid dispensing system with timed sequence fill cycle |
DE102005052197A1 (de) | 2005-10-28 | 2007-05-16 | Endress & Hauser Process Solut | Verfahren zum sicheren Abfüllen bei ventilgesteuerten Abfüllanlagen |
JP2009521655A (ja) * | 2005-12-23 | 2009-06-04 | クウォンタム・フューエル・システムズ・テクノロジーズ・ワールドワイド・インコーポレイテッド | 水素貯蔵コンテナの安全警告および運転停止システムおよびその方法 |
EP1813898A1 (de) * | 2006-01-30 | 2007-08-01 | L'AIR LIQUIDE, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude | System zur Nutzung und Steuerung einer Gruppe von eigenständigen Kühlbehältern |
DE102006029490C5 (de) * | 2006-06-27 | 2015-07-02 | Khs Gmbh | Verfahren zur Steuerung einer Füllanlage |
KR200452382Y1 (ko) * | 2008-10-13 | 2011-02-22 | (주)아모레퍼시픽 | 화장품 내부접시용 접착액 멀티 도포장치 |
ITRM20090067A1 (it) * | 2009-02-16 | 2010-08-17 | Gian Paolo Arcangeli | Gruppo di trasferimento dosi unitarie calibrate di prodotti viscosi e/o creme |
DE102010053201A1 (de) | 2010-12-03 | 2012-06-06 | Krones Aktiengesellschaft | Vorrichtung und Verfahren zum Befüllen von Behältnissen |
KR101569603B1 (ko) | 2011-04-06 | 2015-11-16 | 미쯔비시 쥬우꼬오 쇼구힌호오소오기까이 가부시키가이샤 | 회전식 충전기 및 회전식 충전기의 충전량 연산 방법 |
JP5970788B2 (ja) * | 2011-11-22 | 2016-08-17 | 凸版印刷株式会社 | 液体充填方法及び装置 |
BR122020019098B1 (pt) * | 2012-02-28 | 2021-09-21 | The Procter & Gamble Company | Sistema de dispensação com controle lógico programável |
WO2014015477A1 (en) | 2012-07-24 | 2014-01-30 | The Procter & Gamble Company | Method and apparatus for packing products into containers |
KR101522928B1 (ko) * | 2013-10-04 | 2015-05-28 | 디에스플랜트(주) | 압력센서를 구비한 고속 유체 회전 충진시스템 |
EP3057904B1 (de) * | 2013-10-18 | 2019-05-22 | Tetra Laval Holdings & Finance S.A. | Verfahren für ein füllventil und füllventilsystem |
US9643812B2 (en) | 2014-03-06 | 2017-05-09 | The Procter & Gamble Company | Method for pleating or shaping a web |
US9783330B2 (en) | 2014-03-06 | 2017-10-10 | The Procter & Gamble Company | Method and apparatus for shaping webs in a vertical form, fill, and sealing system |
EP2949618B1 (de) * | 2014-05-30 | 2016-08-31 | Sidel S.p.a. Con Socio Unico | Verfahren und Vorrichtung zum Kontaktfüllen eines Artikels mit einem fliessfähigen Produkt |
CN104671172B (zh) * | 2015-02-09 | 2017-05-31 | 长沙今朝科技股份有限公司 | 一种负压式定量灌装机、灌装方法 |
KR20180045006A (ko) * | 2015-09-03 | 2018-05-03 | 쌩-고벵 글래스 프랑스 | 절연 글레이징 제조용 스페이서 프레임을 충전하기 위한 방법 및 장치 |
CN105129692B (zh) * | 2015-09-06 | 2017-05-24 | 上海东富龙科技股份有限公司 | 一种应用于吹灌封一体机的时间压力法精确灌装系统 |
DE102017119069A1 (de) * | 2017-08-21 | 2019-02-21 | Krones Ag | Verfahren zum Befüllen von Behältern mit einem Füllprodukt |
EP3705450B1 (de) | 2019-03-08 | 2022-08-03 | Sidel Participations | Vorrichtung und verfahren zum befüllen eines behälters |
US11286148B2 (en) * | 2019-04-04 | 2022-03-29 | Zachary Hays | Liquid dispenser |
DE102019128324A1 (de) * | 2019-10-21 | 2021-04-22 | Krones Ag | Vorrichtung und Verfahren zum Befüllen eines Behälters mit einem Füllprodukt |
CN110980613A (zh) * | 2019-11-22 | 2020-04-10 | 湖南工业大学 | 一种高速罐装自适应控制系统和方法 |
CN113929039A (zh) * | 2021-09-16 | 2022-01-14 | 湖南金珠油脂有限公司 | 一种植物油加工用定量灌装设备 |
DE102022118522A1 (de) | 2022-07-25 | 2024-01-25 | Khs Gmbh | Verfahren zum Befüllen von Behältern sowie Füllanlage |
Family Cites Families (13)
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US2791353A (en) * | 1953-12-08 | 1957-05-07 | Herman W Dorn | Manually operable paint dispensing apparatus |
US4527600A (en) * | 1982-05-05 | 1985-07-09 | Rockwell International Corporation | Compressed natural gas dispensing system |
GB2123983B (en) * | 1982-07-15 | 1986-01-08 | Delta Technical Services Ltd | Pressure controllers |
DE3335260A1 (de) * | 1982-11-09 | 1984-05-10 | Pirzer, Carl, 8402 Neutraubling | Verfahren zum steuern einer fuellmaschine, insbesondere flaschenfuellmaschine sowie anordnung zur durchfuehrung dieses verfahrens |
US4859375A (en) * | 1986-12-29 | 1989-08-22 | Air Products And Chemicals, Inc. | Chemical refill system |
ES2004035A6 (es) * | 1986-12-24 | 1988-12-01 | Construcciones Y Estructuras M | Dispositivo para el llenado volumetrico de envases |
US4890774A (en) * | 1987-10-29 | 1990-01-02 | The Coca-Cola Company | Beverage dispensing system |
US4821580A (en) * | 1988-01-27 | 1989-04-18 | Jorritsma Johannes N | Method and apparatus for calculating flow rates through a pumping station |
EP0406092B1 (de) * | 1989-06-27 | 1993-01-13 | Group S.E.R.A.C. | Vorrichtung zum Füllen von Behältern mit abgewogenen Mengen |
IT1236158B (it) * | 1989-11-23 | 1993-01-11 | Farmomac Srl | Metodo per il riempimento di contenitori con prodotti liquidi e/o gelatinosi,e/o corrosivi,o collanti,o sospensioni abrasive e macchina che attua tale metodo. |
JP2906548B2 (ja) * | 1990-03-14 | 1999-06-21 | 住友電気工業株式会社 | 流量制御装置 |
DE4117287A1 (de) * | 1991-05-27 | 1992-12-03 | Seitz Enzinger Noll Masch | Verfahren zum fuellen von flaschen, dosen o. dgl. behaelter sowie fuellmaschine zum durchfuehren dieses verfahrens |
JP2960590B2 (ja) * | 1991-09-27 | 1999-10-06 | 東芝機械株式会社 | 発泡飲料の自動定量注出装置 |
-
1995
- 1995-06-16 JP JP7150670A patent/JP2633820B2/ja not_active Expired - Lifetime
-
1996
- 1996-06-03 US US08/776,948 patent/US5823234A/en not_active Expired - Fee Related
- 1996-06-13 TR TR97/00101T patent/TR199700101T1/xx unknown
- 1996-06-13 DE DE59605120T patent/DE59605120D1/de not_active Revoked
- 1996-06-13 WO PCT/DE1996/001037 patent/WO1997000224A1/de not_active Application Discontinuation
- 1996-06-13 ES ES96916004T patent/ES2147378T3/es not_active Expired - Lifetime
- 1996-06-13 EP EP96916004A patent/EP0776314B1/de not_active Revoked
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101817493A (zh) * | 2010-03-16 | 2010-09-01 | 广州达意隆包装机械股份有限公司 | 换向控制阀、换向式定量灌装机及其灌装方法 |
CN101817493B (zh) * | 2010-03-16 | 2013-09-18 | 广州达意隆包装机械股份有限公司 | 换向控制阀、换向式定量灌装机及其灌装方法 |
DE102013100702A1 (de) * | 2013-01-24 | 2014-07-24 | Endress + Hauser Process Solutions Ag | Steuermodul für eine Abfüllanlage |
Also Published As
Publication number | Publication date |
---|---|
JPH092583A (ja) | 1997-01-07 |
JP2633820B2 (ja) | 1997-07-23 |
ES2147378T3 (es) | 2000-09-01 |
US5823234A (en) | 1998-10-20 |
TR199700101T1 (tr) | 1997-04-22 |
WO1997000224A1 (de) | 1997-01-03 |
DE59605120D1 (de) | 2000-06-08 |
EP0776314A1 (de) | 1997-06-04 |
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