EP0489569A2 - Entgasen einer Flüssigkeit - Google Patents
Entgasen einer Flüssigkeit Download PDFInfo
- Publication number
- EP0489569A2 EP0489569A2 EP91311244A EP91311244A EP0489569A2 EP 0489569 A2 EP0489569 A2 EP 0489569A2 EP 91311244 A EP91311244 A EP 91311244A EP 91311244 A EP91311244 A EP 91311244A EP 0489569 A2 EP0489569 A2 EP 0489569A2
- Authority
- EP
- European Patent Office
- Prior art keywords
- solvent
- vacuum
- degassing unit
- vacuum degassing
- tubing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 37
- 238000007872 degassing Methods 0.000 title claims abstract description 33
- 238000009849 vacuum degassing Methods 0.000 claims abstract description 54
- 238000004811 liquid chromatography Methods 0.000 claims abstract description 20
- 239000002904 solvent Substances 0.000 claims description 165
- 239000007789 gas Substances 0.000 claims description 38
- 238000005086 pumping Methods 0.000 claims description 10
- 239000002245 particle Substances 0.000 claims description 3
- 238000010586 diagram Methods 0.000 description 15
- 230000003750 conditioning effect Effects 0.000 description 11
- 238000000034 method Methods 0.000 description 10
- 239000000243 solution Substances 0.000 description 9
- 239000003153 chemical reaction reagent Substances 0.000 description 7
- 238000010438 heat treatment Methods 0.000 description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 6
- 239000003085 diluting agent Substances 0.000 description 6
- 239000001301 oxygen Substances 0.000 description 6
- 229910052760 oxygen Inorganic materials 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 5
- 239000012046 mixed solvent Substances 0.000 description 5
- 239000004809 Teflon Substances 0.000 description 4
- 229920006362 Teflon® Polymers 0.000 description 4
- 238000004587 chromatography analysis Methods 0.000 description 4
- 239000004020 conductor Substances 0.000 description 4
- 239000006249 magnetic particle Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000012528 membrane Substances 0.000 description 4
- 239000002699 waste material Substances 0.000 description 4
- 239000011324 bead Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 238000004128 high performance liquid chromatography Methods 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000011877 solvent mixture Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000011144 upstream manufacturing Methods 0.000 description 2
- 230000002411 adverse Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 238000009428 plumbing Methods 0.000 description 1
- 239000012898 sample dilution Substances 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/34—Control of physical parameters of the fluid carrier of fluid composition, e.g. gradient
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0031—Degasification of liquids by filtration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0042—Degasification of liquids modifying the liquid flow
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0063—Regulation, control including valves and floats
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0073—Degasification of liquids by a method not covered by groups B01D19/0005 - B01D19/0042
- B01D19/0078—Degasification of liquids by a method not covered by groups B01D19/0005 - B01D19/0042 by vibration
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/24—Automatic injection systems
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US622999 | 1990-12-04 | ||
US07/622,999 US5183486A (en) | 1990-12-04 | 1990-12-04 | Apparatus for degassing a liquid |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0489569A2 true EP0489569A2 (de) | 1992-06-10 |
EP0489569A3 EP0489569A3 (en) | 1993-03-10 |
Family
ID=24496374
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP19910311244 Withdrawn EP0489569A3 (en) | 1990-12-04 | 1991-12-03 | Degassing a liquid |
Country Status (2)
Country | Link |
---|---|
US (3) | US5183486A (de) |
EP (1) | EP0489569A3 (de) |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1445610A1 (de) * | 2003-01-31 | 2004-08-11 | Systec Inc. | Integriertes Gerät zur Entgasung und Mischung von mehrfachen Strömungen mobiler Phasen |
WO2007091654A1 (ja) | 2006-02-09 | 2007-08-16 | Arkray, Inc. | 液体クロマトグラフィ装置 |
EP2017615A1 (de) * | 2006-02-16 | 2009-01-21 | Arkray, Inc. | Entgasungsvorrichtung und damit ausgestatteter flüssigkeitschromatograph |
JP2011133367A (ja) * | 2009-12-24 | 2011-07-07 | Tosoh Corp | 脱気装置 |
EP2668988A1 (de) * | 2012-05-30 | 2013-12-04 | ARKRAY, Inc. | Kanalblasenreduzierungsvorrichtung, Kanalblasenreduzierungsprogramm, Kanalblasenreduzierungsverfahren, Flüssigkeitsbereitstellungsvorrichtung und Chromatographievorrichtung |
EP2669673A1 (de) * | 2012-05-30 | 2013-12-04 | ARKRAY, Inc. | Blasenreduzierungsvorrichtung, Chromatographievorrichtung, Blasenreduzierungsverfahren und Blasenreduzierungsprogramm |
WO2019241116A1 (en) * | 2018-06-11 | 2019-12-19 | Waters Technologies Corporation | Detecting a fluid leak in a vacuum chamber |
JP2020516852A (ja) * | 2017-01-05 | 2020-06-11 | イラミーナ インコーポレーテッド | フローセル液体脱ガスシステム及び方法 |
GB2580983A (en) * | 2019-02-04 | 2020-08-05 | Agilent Technologies Inc | Combined degassing and circulation of liquid |
Families Citing this family (65)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5183486A (en) * | 1990-12-04 | 1993-02-02 | Spectra-Physics, Inc. | Apparatus for degassing a liquid |
EP0598424A3 (de) * | 1992-11-16 | 1996-05-15 | Novellus Systems Inc | Vorrichtung zur Entfernung von gelösten Gasen aus einer Flüssigkeit. |
WO1994020855A1 (en) * | 1993-03-04 | 1994-09-15 | Sapidyne, Inc. | Assay flow apparatus and method |
US5340384A (en) * | 1993-03-05 | 1994-08-23 | Systec, Inc. | Vacuum degassing |
DE4327582C1 (de) * | 1993-08-17 | 1994-10-06 | Hewlett Packard Gmbh | Verfahren zum Herstellen von Kunststoffteilen aus fluorhaltigen Polymeren für den Einsatz in einem analytischen Messgerät und nach dem Verfahren hergestellte Kunststoffteile |
US5578331A (en) * | 1994-06-10 | 1996-11-26 | Vision Products, Inc. | Automated apparatus for preparing contact lenses for inspection and packaging |
DE4446270C1 (de) * | 1994-12-23 | 1996-02-29 | Hewlett Packard Gmbh | Basisstruktur für einen Flüssigkeitschromatographie-Entgaser |
US5885332A (en) * | 1995-06-06 | 1999-03-23 | Gerner; Yuri | Solvent receptacle and degasser for use in high pressure liquid chromatography |
US5743941A (en) * | 1995-06-06 | 1998-04-28 | Systec, Inc. | Bottle top solvent degasser |
US5714696A (en) * | 1995-07-06 | 1998-02-03 | The Regents Of The University Of California | Fluid sampling apparatus and method |
US5607581A (en) * | 1995-10-31 | 1997-03-04 | Systec, Inc. | Debubbling and priming system for chromotography |
US5733500A (en) * | 1996-03-07 | 1998-03-31 | Phelps Dodge Industries, Inc. | Molten metal degassing and filtering apparatus |
JPH11137907A (ja) * | 1997-11-11 | 1999-05-25 | Moore Kk | 脱気装置 |
US7220596B2 (en) * | 1998-04-15 | 2007-05-22 | Utah State University | Real time detection of antigens |
US6024780A (en) * | 1998-05-19 | 2000-02-15 | Haselden, Jr.; Odell Kent | Method and apparatus for degassing a fluid in a reusable vaccum chamber with microprocessor based controls |
DE69828594T2 (de) * | 1998-07-17 | 2005-06-16 | Agilent Technologies Inc., A Delaware Corp., Palo Alto | Vorrichtung zum Entgasen von Flüssigkeiten |
JP3670851B2 (ja) * | 1998-07-21 | 2005-07-13 | アクト・サイエンス株式会社 | 液体クロマトグラフィー用送液ポンプ |
US6755899B2 (en) * | 1998-10-09 | 2004-06-29 | Erc, Inc. | Vacuum deaeration device |
JP2000275229A (ja) * | 1999-03-26 | 2000-10-06 | Moore Kk | 脱気装置 |
DE19917636B4 (de) * | 1999-04-19 | 2005-07-28 | Robert Bosch Gmbh | Verfahren und Vorrichtung zur Behandlung eines Druckmittels |
US6248157B1 (en) | 1999-08-20 | 2001-06-19 | Systec Inc. | Vacuum degassing |
US6391096B1 (en) | 2000-06-09 | 2002-05-21 | Serveron Corporation | Apparatus and method for extracting and analyzing gas |
US20020142618A1 (en) * | 2000-08-04 | 2002-10-03 | Caliper Technologies Corp. | Control of operation conditions within fluidic systems |
WO2002012856A1 (en) * | 2000-08-04 | 2002-02-14 | Caliper Technologies Corp. | Control of operation conditions within fluidic systems |
WO2003064585A1 (en) * | 2002-01-25 | 2003-08-07 | Irm, Llc | Devices, systems, and methods of manifolding materials |
US7314502B2 (en) * | 2002-09-25 | 2008-01-01 | Exxonmobil Upstream Research Company | Method and system for separating a component from a multi-component gas |
JP3868899B2 (ja) * | 2002-12-25 | 2007-01-17 | 株式会社島津製作所 | 液体クロマトグラフ |
DE10300957A1 (de) * | 2003-01-13 | 2004-07-22 | Ibidi Gmbh | Probenkammer für eine Flüssigkeit |
US6795484B1 (en) | 2003-05-19 | 2004-09-21 | Johns Manville International, Inc. | Method and system for reducing a foam in a glass melting furnace |
US7713331B2 (en) * | 2003-11-05 | 2010-05-11 | Rheodyne, Llc | Axial transfer line degassing |
US6949132B2 (en) * | 2003-11-05 | 2005-09-27 | Systel, Llc | Axial degassing transfer lines |
US20050100477A1 (en) * | 2003-11-06 | 2005-05-12 | Alltech Associates, Inc. | Apparatus and method for removing gas prior to sample detection and/or analysis |
US7041154B2 (en) * | 2003-12-12 | 2006-05-09 | United Technologies Corporation | Acoustic fuel deoxygenation system |
WO2006017820A1 (en) * | 2004-08-07 | 2006-02-16 | Waters Investments Limited | Passive column pre-heater with sample band spreading reduction feature |
WO2007051113A2 (en) * | 2005-10-27 | 2007-05-03 | Waters Investments Limited | Pump |
US20070148326A1 (en) * | 2005-12-28 | 2007-06-28 | Hastings Mitchell R | Syringe |
US7892321B2 (en) * | 2006-02-01 | 2011-02-22 | Intelligent Energy, Inc. | Integrated heated prevaporation module |
US20070181501A1 (en) * | 2006-02-08 | 2007-08-09 | Agilent Technologies, Inc. | Method and apparatus for packing chromatography column |
JP4898778B2 (ja) * | 2006-02-21 | 2012-03-21 | 武蔵エンジニアリング株式会社 | 脱泡機構を備える液材吐出装置 |
US20070199904A1 (en) * | 2006-02-27 | 2007-08-30 | Jonathan Thompson | Methods for treatment of organic matter in liquid |
TWI388368B (zh) * | 2006-05-01 | 2013-03-11 | Nitto Denko Corp | 脫氣裝置 |
WO2008035714A1 (fr) * | 2006-09-22 | 2008-03-27 | Nitto Denko Corporation | Dispositif de dégazage |
US20080098894A1 (en) * | 2006-11-01 | 2008-05-01 | Sabatino Daniel R | Acoustic degassing heat exchanger |
US20090044604A1 (en) * | 2007-08-15 | 2009-02-19 | Gregor Ocvirk | Portable Measuring Facility for Determining A Medically Significant Analyte Concentration |
US20090249949A1 (en) * | 2008-03-05 | 2009-10-08 | Helicos Biosciences Corporation | Methods and devices for bubble mitigation |
US8075675B2 (en) * | 2008-06-12 | 2011-12-13 | Serveron Corporation | Apparatus and method for extracting gas from liquid |
GB2477679A (en) * | 2008-10-30 | 2011-08-10 | Porous Media Corp | Venting and filtration systems with gas permeable membrane |
CN102481494B (zh) | 2009-09-14 | 2014-09-10 | 兰登姆科技有限责任公司 | 用于改变液体中的气体浓度的装置及方法 |
EP2524178B1 (de) * | 2010-01-11 | 2021-05-26 | Waters Technologies Corporation | Wärmesteuerung einer wärmekammer in hochleistungs-flüssigchromatographiesystemen |
FR2959315B1 (fr) * | 2010-04-22 | 2012-04-27 | Gdf Suez | Installation et procede de caracterisation de gaz dissous dans un liquide |
US8469503B2 (en) * | 2010-10-05 | 2013-06-25 | Eastman Kodak Company | Method of thermal degassing in an inkjet printer |
US8465139B2 (en) * | 2010-10-05 | 2013-06-18 | Eastman Kodak Company | Thermal degassing device for inkjet printer |
US20120103062A1 (en) * | 2010-11-02 | 2012-05-03 | Picarro, Inc. | Sample preparation for gas analysis using inductive heating |
US8425656B2 (en) * | 2011-01-25 | 2013-04-23 | Media And Process Technology, Inc. | Transport membrane condenser using turbulence promoters |
US9120580B2 (en) * | 2011-08-31 | 2015-09-01 | United Technologies Corporation | Ejector-driven fuel stabilization system |
US9044712B2 (en) | 2011-09-12 | 2015-06-02 | Idex Health & Science, Llc | Supersaturated fluid degassing |
DE102011088959B4 (de) * | 2011-12-19 | 2022-08-04 | Endress+Hauser Conducta Gmbh+Co. Kg | Vorrichtung zum Entgasen einer Flüssigkeit und Verwendung dieser Vorrichtung in einem Analysegerät |
US9114331B2 (en) | 2012-09-28 | 2015-08-25 | Random Technologies Llc | Apparatus and method for degassing liquids |
JP6519980B2 (ja) * | 2014-03-31 | 2019-05-29 | 株式会社島津製作所 | 液体クロマトグラフ |
DE102016007094B3 (de) * | 2016-06-10 | 2016-12-22 | Qfood Gmbh | Probenentnahmevorrichtung zur Entnahme von Getränkeproben aus einer Getränkeleitung, die ein unter Druck stehendes gashaltiges Getränk enthält |
GB2590130B (en) | 2019-09-23 | 2022-10-19 | Idex Health & Science Llc | Fluid degassing system with reduced pressure pulsatility |
CN114514422A (zh) * | 2019-10-01 | 2022-05-17 | 基础科学公司 | 用于在线分析的挥发性样品的自动在线制备和脱气 |
EP3808426A1 (de) | 2019-10-18 | 2021-04-21 | Roche Diagnostics GmbH | Techniken zur überprüfung des zustands von analysatoren |
GB2601489B (en) * | 2020-12-01 | 2024-01-17 | Agilent Technologies Inc | Vaccum degassing using electroactive material |
US20220347601A1 (en) * | 2021-05-03 | 2022-11-03 | Kazadi Enterprises Ltd. | Low energy liquid degasification devices and methods |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4469495A (en) * | 1983-01-29 | 1984-09-04 | Erma Optical Works, Ltd. | Method and device for degassifying liquid |
Family Cites Families (43)
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US3239998A (en) * | 1962-05-02 | 1966-03-15 | Eastman Kodak Co | Ultrasonic degassing of multiple emulsions in a vertical unit |
US3266631A (en) * | 1964-03-16 | 1966-08-16 | Alvin A Snaper | Apparatus for separating a fluid mixture by acoustic energy |
US3377778A (en) * | 1966-02-02 | 1968-04-16 | Gen Electric | Method and apparatus for degassing liquids |
US3751879A (en) * | 1971-04-26 | 1973-08-14 | Instrumentation Specialties Co | Apparatus for reducing the dissolved gas concentration in a liquid |
DE2545997C3 (de) * | 1975-10-14 | 1978-09-07 | Max-Planck-Gesellschaft Zur Foerderung Der Wissenschaften E.V., 3400 Goettingen | Vorrichtung für die Vielfach-Säulenchromatographie |
US4325715A (en) * | 1976-03-24 | 1982-04-20 | Bowman Donald B | Apparatus for degassing hemodialysis liquid |
US4430098A (en) * | 1976-03-24 | 1984-02-07 | Bowman Donald B | Apparatus for degassing hemodialysis liquid and the like |
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EP0360604A3 (de) * | 1988-09-23 | 1991-01-30 | Spectra-Physics, Inc. | Umlauf von flüssigen Proben |
JP2556115B2 (ja) * | 1988-10-31 | 1996-11-20 | 株式会社島津製作所 | 分取用液体クロマトグラフ |
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US5183486A (en) * | 1990-12-04 | 1993-02-02 | Spectra-Physics, Inc. | Apparatus for degassing a liquid |
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-
1990
- 1990-12-04 US US07/622,999 patent/US5183486A/en not_active Expired - Lifetime
-
1991
- 1991-12-03 EP EP19910311244 patent/EP0489569A3/en not_active Withdrawn
-
1992
- 1992-12-14 US US07/990,656 patent/US5290340A/en not_active Expired - Fee Related
- 1992-12-14 US US07/990,274 patent/US5279647A/en not_active Expired - Fee Related
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Also Published As
Publication number | Publication date |
---|---|
EP0489569A3 (en) | 1993-03-10 |
US5183486A (en) | 1993-02-02 |
US5279647A (en) | 1994-01-18 |
US5290340A (en) | 1994-03-01 |
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