EP0431426B1 - Verfahren und Vorrichtung zum Betrieb einer Filterzentrifuge - Google Patents
Verfahren und Vorrichtung zum Betrieb einer Filterzentrifuge Download PDFInfo
- Publication number
- EP0431426B1 EP0431426B1 EP90122453A EP90122453A EP0431426B1 EP 0431426 B1 EP0431426 B1 EP 0431426B1 EP 90122453 A EP90122453 A EP 90122453A EP 90122453 A EP90122453 A EP 90122453A EP 0431426 B1 EP0431426 B1 EP 0431426B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- hydroextraction
- time
- filter cake
- determined
- filter
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title claims description 30
- 238000009434 installation Methods 0.000 title 1
- 239000012065 filter cake Substances 0.000 claims description 33
- 239000007788 liquid Substances 0.000 claims description 33
- 238000005406 washing Methods 0.000 claims description 21
- 238000001914 filtration Methods 0.000 claims description 18
- 238000007654 immersion Methods 0.000 claims description 16
- 239000007787 solid Substances 0.000 claims description 12
- 239000000725 suspension Substances 0.000 claims description 12
- 230000001419 dependent effect Effects 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims 1
- 230000007423 decrease Effects 0.000 description 9
- 238000001035 drying Methods 0.000 description 7
- 239000012452 mother liquor Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 5
- 230000008929 regeneration Effects 0.000 description 3
- 238000011069 regeneration method Methods 0.000 description 3
- 238000010923 batch production Methods 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 238000009987 spinning Methods 0.000 description 2
- 230000001960 triggered effect Effects 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000011001 backwashing Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000000578 dry spinning Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- -1 feed concentration Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000001028 reflection method Methods 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 238000009751 slip forming Methods 0.000 description 1
- 230000002123 temporal effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B11/00—Feeding, charging, or discharging bowls
- B04B11/04—Periodical feeding or discharging; Control arrangements therefor
- B04B11/043—Load indication with or without control arrangements
Definitions
- the invention relates to a method for operating a filter centrifuge according to the preamble of patent claim 1.
- the level in the rotating drum decreases more or less quickly depending on the filtration properties. So that a certain height of the filter cake in the drum can be reached, one or more times suspension in the drum is refilled up to the maximum filling level, the level being monitored by means of a level controller.
- a sensor can be used which can detect a change in the surface condition of the filter material in the drum, so that the time of immersion of the liquid surface in the filter cake can be determined. Such a sensor is disclosed for example in DE-OS 37 26 227.
- a method for separating sugar from a sugar suspension in which a washing process is controlled depending on the surface density of the filter cake.
- the areal density is determined, for example, by the absorption of gamma radiation.
- Another method for monitoring sugar centrifuges is known from DE-A-32 15 915.
- the surface of the filter cake of a centrifuge is monitored using a reflection method and the time of immersion of the liquid surface is determined.
- a method according to the preamble of claim 1 is known from DE-C-36 15 013.
- the flow rate of the outflowing liquid is monitored during the dry spin process and the dry spin process is controlled as a function of the flow rate. It is therefore necessary to monitor the dry spin cycle yourself and to take additional measures to determine the liquid speed.
- the object of the invention is to minimize the individual cycle times despite fluctuations in the filtration conditions and to significantly increase the throughput of the filter centrifuge with a constant degree of washout and constant low final residual moisture.
- the level in the rotating centrifuge drum is measured continuously or at time intervals with a measuring device and the time course of the level is registered.
- the immersion points of the mother liquor or the washing liquid in the filter cake are determined. H. the times at which the liquid is filtered off to such an extent that it begins to disappear in the filter cake. From the temporal change in the filling level and the immersion times, the optimal number of filling cycles, the optimal start of the washing cycle and the required spin drying time are concluded, so that a desired final residual moisture of the filter cake is achieved with a minimal total cycle time.
- the filling, dehumidifying and washing processes in the filter centrifuge are controlled independently of fluctuations in the task in such a way that the throughput is maximized with a constant degree of washing out and constant final residual moisture.
- the invention is based on the finding that all the fluctuations and imponderables that affect the filtration, washing and drying spin times are expressed in the rate at which the liquids decrease in height. These can be due to the suspension properties such as grain shape, average grain size (d-p50), shape and slope of the total curve of the grain size analysis, fine particles, feed concentration, liquid temperature, viscosity, interfacial tension etc. or they can also be due to the operating properties of the filter media or the filter centrifuge.
- suspension properties such as grain shape, average grain size (d-p50), shape and slope of the total curve of the grain size analysis, fine particles, feed concentration, liquid temperature, viscosity, interfacial tension etc.
- Fluctuations from batch to batch can be compensated for by changing cycle times and incorrect batches whose solids discharge is too moist are avoided.
- Required regeneration steps such as backing up the base layer, clearing out the base layer or regenerating filter medium are displayed and triggered automatically. In spite of a discontinuous driving style, a uniform product quality is achieved and downstream devices such as dryers etc. can be driven to their performance limits.
- FIG. 1 The work processes taking place successively in a discontinuous filter centrifuge are shown in FIG. 1. After several filter processes in which a filter cake with the desired thickness has been formed, the filter cake is washed with a washing liquid which is introduced into the drum and passes through the filter cake.
- the filter cake is then dried in a dry spin cycle without adding any additional liquid.
- This dry spin process can optionally be followed by a further drying process in which the filter cake z. B. can be removed by supplying hot air or the like. Liquid.
- the dried filter cake is then removed from the centrifuge drum, for example by means of a peeling knife arranged in the centrifuge drum.
- the centrifuge drum can then either be refilled or a regeneration process follows. In this regeneration process, the solid fraction remaining in the drum during peeling, the so-called base layer, is removed, for example by backwashing, and filters are replaced if necessary.
- FIG. 2 shows the course over time of the fill level and the filter cake thickness in the above-described operations of the filter centrifuge for one work cycle.
- the washing process is started, in which a washing liquid is fed to the drum and filtered through the filter cake by centrifugation. As soon as the washing liquid has completely penetrated the surface of the filter cake, that is the immersion point ET, the filtering process is continued with the dry spin process without adding any additional liquid. The drum is then cleared and, if necessary, regenerated.
- the total cycle time t is relatively long in the case of products that are difficult to filter, the time fraction required for the dry centrifugation being particularly decisive.
- the height of the filter cake decreases only slightly during the spin drying process.
- Figure 3 shows schematically the decrease in height of the washing liquid applied before the spin-drying phase.
- the decreasing layer height h is measured and stored at regular intervals and the differential quotient dh / dt is continuously formed in a process computer from the decrease in height of the washing liquid layer above the filter cake.
- the total layer height decreases until the filter cake thickness h ET is reached, at which the liquid on the cake surface disappears and is immersed in the filter cake.
- the to this immersion point belonging time t ET is registered.
- the spin time t S starts to spin dry the solid cake.
- This essential time t S for the cycle duration can be determined from the values h ET and dh / dt measured for each batch and a constant K which is dependent on the machine data (size) and the drum speed.
- the fluctuating filtration properties depend on the fluctuating suspension properties such as grain shape, average grain size (d-p50), shape and slope of the total curve of the grain size analysis, fines, feed concentration, liquid temperature, viscosity, interfacial tension, etc. These product properties are determined by the parameters h ET and dh / dt recorded with sufficient accuracy.
- the dry spin time t S required for the respective batch to achieve the desired residual moisture is calculated from: t S ⁇ K a ⁇ H ET /H ETo ⁇ b t So ⁇ (ie / dt) O / (ie / dt) ⁇ c
- the ratio of the filter cake heights when immersing the washing liquid (h ET ) and when immersing the mother liquor (h ETo ) is formed; the removal speeds when immersing the mother liquor (dh / dt) o and when immersing the washing liquid (dh / dt) are calculated and also related.
- the values determined in this way are exponentiated by the exponents b or c and multiplied by the value K a , which depends on the machine data. Finally, the value thus obtained is multiplied by a time value t So for a normal dry spin cycle.
- the quantity t So can be calculated, formed from an empirical value or measured in a previous spinning process.
- the constant exponents a, b and c can be calculated or be determined by experiments; they do not change for the individual batches.
- FIG. 4 shows the filling level curve over time for two differently filtering products due to the influence of the batch-dependent suspension feed.
- the solid line shows the normal batch process with the operations: Filling, filtering, adding washing liquid, spinning to the immersion point ET0, dry spinning, clearing out
- the dashed line shows the batch process for grain enlargement and increasing the feed concentration.
- the rate of rise is somewhat slower when filling because the product filters better.
- the filling valve is closed and the liquid level drops more steeply.
- the washing liquid can be added immediately; the water level drops faster.
- the immersion point ET1 the dry spin phase begins, which 1 can be much shorter than in the normal case because of the steep drop (ie / dt). If the desired residual moisture has been reached, clearing can already start at R1. The cycle can then be repeated.
- Figure 5 shows a schematic representation of the process control.
- the quantities h and h ET to be measured on the centrifuge as a function of time are entered into the computer. From the differential quotient dh / dt during the filtering off of the mother liquor at point W and the differential quotient dh / dt during the washing liquid outflow at point ET, the batch-dependent change in the drying time required to reach a certain residual moisture at point R is calculated in a process computer and specified as the cycle time.
- the mean value from the linearized course of the decrease in height over time or the difference quotient ⁇ h / ⁇ t of the quantities can be determined.
- An analog computer or a digital computer can be used as the process computer.
Landscapes
- Centrifugal Separators (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE3940057A DE3940057A1 (de) | 1989-12-04 | 1989-12-04 | Verfahren und vorrichtung zum betrieb einer filterzentrifuge |
DE3940057 | 1989-12-04 |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0431426A1 EP0431426A1 (de) | 1991-06-12 |
EP0431426B1 true EP0431426B1 (de) | 1994-01-26 |
Family
ID=6394776
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP90122453A Expired - Lifetime EP0431426B1 (de) | 1989-12-04 | 1990-11-26 | Verfahren und Vorrichtung zum Betrieb einer Filterzentrifuge |
Country Status (5)
Country | Link |
---|---|
US (1) | US5093010A (ja) |
EP (1) | EP0431426B1 (ja) |
JP (1) | JPH03270750A (ja) |
DE (2) | DE3940057A1 (ja) |
ES (1) | ES2048391T3 (ja) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4204805A1 (de) * | 1992-02-18 | 1993-08-19 | Henkel Kgaa | Verfahren zum kontinuierlichen betreiben eines separators und zusatzeinrichtung fuer diesen separator |
US5897786A (en) * | 1997-03-24 | 1999-04-27 | The Western States Machine Company | Method and apparatus for determining thickness of a charge wall being formed in a centrifugal machine |
US6296774B1 (en) | 1999-01-29 | 2001-10-02 | The Western States Machine Company | Centrifuge load control for automatic infeed gate adjustment |
DE102013111576A1 (de) | 2013-10-21 | 2015-04-23 | Gea Mechanical Equipment Gmbh | Verfahren zur Klärung eines fließfähigen Produktes mit einer Zentrifuge, insbesondere einem Separator |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE516155A (ja) * | 1951-12-12 | |||
US3117233A (en) * | 1961-06-21 | 1964-01-07 | American Plant Equipment Compa | Filter cake thickness detector for filtering apparatus |
US3204766A (en) * | 1961-07-17 | 1965-09-07 | Industrial Filter Pump Mfg Co | Filter cake thickness detector |
US3141846A (en) * | 1962-04-05 | 1964-07-21 | Western States Machine Co | Load control unit for cyclical centrifugal installation |
DE1186411B (de) * | 1963-10-03 | 1965-01-28 | Krauss Maffei Ag | Schaelzentrifuge, insbesondere fuer langsam filtrierende Suspensionen |
DE2441849A1 (de) * | 1974-08-31 | 1976-03-18 | Titus Hans Joachim | Vollautomatische fuellsteuerung fuer zentrifugen |
US4014498A (en) * | 1975-01-15 | 1977-03-29 | Alfa-Laval Ab | Method and apparatus for centrifuging sludge-containing liquids |
DE2525232A1 (de) * | 1975-06-06 | 1976-12-16 | Riedel De Haen Ag | Vorrichtung zur messung der fuellschichthoehe einer siebschleuder |
CH604907A5 (ja) * | 1975-11-14 | 1978-09-15 | Sandoz Ag | |
DD218283A1 (de) * | 1983-05-31 | 1985-02-06 | Kali Veb K | Vorrichtung zur steuerung mehrerer schaelschleudern |
DE3515915C2 (de) * | 1985-05-03 | 1993-10-14 | Braunschweigische Masch Bau | Überwachungsverfahren und Vorrichtung zur Kontrolle des Sirupablaufes bei periodisch arbeitenden Zuckerzentrifugen |
GB8517762D0 (en) * | 1985-07-15 | 1985-08-21 | British Nuclear Fuels Plc | Centrifuges |
DE3615013C1 (en) * | 1986-05-02 | 1987-06-11 | Krauss Maffei Ag | Method for monitoring the drying phase in filtration centrifuges |
DE3632176A1 (de) * | 1986-09-22 | 1988-04-07 | Fresenius Ag | Steuerung eines systems zur trennung der bestandteile des einem spender "in vivo" entnommenen blutes |
DE3726227A1 (de) * | 1987-08-07 | 1989-02-16 | Krauss Maffei Ag | Vorrichtung zum ergebnisabhaengigen steuern einer filterzentrifuge |
DE3822225C1 (ja) * | 1988-07-01 | 1989-07-20 | Laboratorium Prof. Dr. Rudolf Berthold, 7547 Wildbad, De |
-
1989
- 1989-12-04 DE DE3940057A patent/DE3940057A1/de active Granted
-
1990
- 1990-11-26 EP EP90122453A patent/EP0431426B1/de not_active Expired - Lifetime
- 1990-11-26 JP JP2318177A patent/JPH03270750A/ja active Pending
- 1990-11-26 ES ES90122453T patent/ES2048391T3/es not_active Expired - Lifetime
- 1990-11-26 DE DE90122453T patent/DE59004414D1/de not_active Expired - Fee Related
- 1990-12-03 US US07/621,744 patent/US5093010A/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
DE59004414D1 (de) | 1994-03-10 |
DE3940057C2 (ja) | 1993-08-05 |
JPH03270750A (ja) | 1991-12-02 |
ES2048391T3 (es) | 1994-03-16 |
DE3940057A1 (de) | 1991-06-06 |
US5093010A (en) | 1992-03-03 |
EP0431426A1 (de) | 1991-06-12 |
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