EP0358923B1 - Verfahren und Vorrichtung zur Reinigung von Rohgas aus einer Feststoff-Vergasung - Google Patents

Verfahren und Vorrichtung zur Reinigung von Rohgas aus einer Feststoff-Vergasung Download PDF

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Publication number
EP0358923B1
EP0358923B1 EP89114339A EP89114339A EP0358923B1 EP 0358923 B1 EP0358923 B1 EP 0358923B1 EP 89114339 A EP89114339 A EP 89114339A EP 89114339 A EP89114339 A EP 89114339A EP 0358923 B1 EP0358923 B1 EP 0358923B1
Authority
EP
European Patent Office
Prior art keywords
gas
filter
chamber
raw gas
fixed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP89114339A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP0358923A1 (de
Inventor
Hartmut Dr. Hederer
Rolf Buchenau
Dieter Victor
Bernard Schleper
Harald Dr. Hoffmann
Rainer Dr. Dürrfeld
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ruhrkohle Oel und Gas GmbH
Hoechst AG
Original Assignee
Ruhrkohle Oel und Gas GmbH
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ruhrkohle Oel und Gas GmbH, Hoechst AG filed Critical Ruhrkohle Oel und Gas GmbH
Priority to AT89114339T priority Critical patent/ATE92949T1/de
Publication of EP0358923A1 publication Critical patent/EP0358923A1/de
Application granted granted Critical
Publication of EP0358923B1 publication Critical patent/EP0358923B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10JPRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J3/00Production of combustible gases containing carbon monoxide from solid carbonaceous fuels
    • C10J3/72Other features
    • C10J3/82Gas withdrawal means
    • C10J3/84Gas withdrawal means with means for removing dust or tar from the gas
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10KPURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K1/00Purifying combustible gases containing carbon monoxide
    • C10K1/02Dust removal
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10KPURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K1/00Purifying combustible gases containing carbon monoxide
    • C10K1/02Dust removal
    • C10K1/024Dust removal by filtration

Definitions

  • the invention relates to a method and a device for cleaning raw gas from a solid gasification with contents of granular and dusty solid particles.
  • Solid gasification means in particular the gasification of hard coal or lignite.
  • the coal can be used both as coal dust and as a slurry together with the oxidizing agent, e.g. Air or oxygen-enriched air are fed into the gasification reactor.
  • the hot crude gas obtained can either be passed through the applied coal layer or can be freely discharged in the opposite direction from the gasification reactor.
  • the invention does not relate to the purification of raw gas which is discharged through the abandoned coal layer, but only from that which is discharged freely.
  • Raw gas from solid gasification described above is not free of solids, but must be subjected to a separation of the solid parts before further processing. It is necessary to remove the solids before any further treatment of the raw gas, e.g. Cooling, to separate from this. So far, this demand could not be met or only in an inadequate form.
  • a gas cooler arrangement for cooling the reaction products of a coal gasification reactor is known.
  • the new gas cooler arrangement is intended to separate small ash particles on the pipes of the convective gas cooler.
  • the convective gas cooler comprises at least one ascent for the gas to be cooled.
  • special pipe cleaning agents e.g. Sootblower to be installed.
  • FR-E-55 473 discloses a gas generator for motor vehicles, but also for other types of use. It consists of a gasification reactor with a raw gas outlet arranged at the bottom, an ash collecting chamber, a fixed bed filter and a filter inflow chamber which connects peripherally to the raw gas outlet. Such a device is unsuitable for cleaning gases which contain sticky or liquid ash particles. Because these particles bake on the surface and in the interior of the filter, form solid layers and trigger blockages that reduce the cleaning effect of the filter and ultimately bring it to a standstill.
  • the invention is based, to remove the solid particles of any size occurring in the gasification of solids largely before entering cooling devices from the raw gas.
  • the method is carried out in a device which is characterized in that the gasification reactor has a gas outlet in the lower part, to which the filter inflow space connects peripherally, which is arranged above the fixed bed filter, the surface of the fixed bed facing the filter inflow space at least is three times larger than the circular area of the gas outlet pipe from the gasification reactor, the fixed bed is inclined and the top filter layer after covering the filter surface with dust is brought back into the ash collecting space by means of the gas backflushing by means of the nozzles.
  • the advantages achieved by the invention consist in particular in that, in terms of process engineering, the coarse and fine cleaning of the crude gas from granular and dusty solid particles takes place immediately one after the other, without interposing sensitive gas path sections or further containers. Because of the continued direct consequence of the strong gas speed reduction after the change in gas direction, there is an even flow through the following filter surface.
  • a radiation cooler 10 is installed in the lower part of the gasification reactor 1 in order to reduce the temperature of the raw gas to 500-700 ° C.
  • the raw gas flows through the radiation cooler without any noticeable deposition of solid particles on the heat exchanger surfaces.
  • the ash collecting space 5 can also be designed as a water bath.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Industrial Gases (AREA)
  • Filtering Of Dispersed Particles In Gases (AREA)
  • Treating Waste Gases (AREA)
  • Separation By Low-Temperature Treatments (AREA)
EP89114339A 1988-08-16 1989-08-03 Verfahren und Vorrichtung zur Reinigung von Rohgas aus einer Feststoff-Vergasung Expired - Lifetime EP0358923B1 (de)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AT89114339T ATE92949T1 (de) 1988-08-16 1989-08-03 Verfahren und vorrichtung zur reinigung von rohgas aus einer feststoff-vergasung.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE3827702A DE3827702A1 (de) 1988-08-16 1988-08-16 Verfahren und vorrichtung zur reinigung von rohgas aus einer feststoff-vergasung
DE3827702 1988-08-16

Publications (2)

Publication Number Publication Date
EP0358923A1 EP0358923A1 (de) 1990-03-21
EP0358923B1 true EP0358923B1 (de) 1993-08-11

Family

ID=6360915

Family Applications (1)

Application Number Title Priority Date Filing Date
EP89114339A Expired - Lifetime EP0358923B1 (de) 1988-08-16 1989-08-03 Verfahren und Vorrichtung zur Reinigung von Rohgas aus einer Feststoff-Vergasung

Country Status (7)

Country Link
EP (1) EP0358923B1 (xx)
JP (1) JPH0291192A (xx)
AT (1) ATE92949T1 (xx)
AU (1) AU620129B2 (xx)
DE (2) DE3827702A1 (xx)
ES (1) ES2045296T3 (xx)
ZA (1) ZA896204B (xx)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE9103432U1 (de) * 1991-03-20 1991-06-20 Babcock-BSH AG vormals Büttner-Schilde-Haas AG, 4150 Krefeld Körnerbettfilter
DE4318385C2 (de) * 1993-06-03 1997-04-10 Metallgesellschaft Ag Verfahren zum Abscheiden von Schlacketröpfchen aus einem Rohgas aus der Verbrennung oder Vergasung fester oder flüssiger Brennstoffe
DE102013112322A1 (de) * 2013-11-08 2015-05-13 Firma Nüsser Ingenieurges.Mbh Filtervorrichtung
EP3037164A1 (en) 2014-12-23 2016-06-29 Haldor Topsøe A/S Particle separating catalytic chemical reactor and particle separator
BR112017014483B1 (pt) 2015-01-05 2020-11-17 Haldor Tops0E A/S sistema de separação de partículas
RU2768913C2 (ru) 2017-07-14 2022-03-25 Хальдор Топсёэ А/С Каталитический химический реактор с отделением частиц с фильтрующим устройством
CN109806703B (zh) * 2019-03-11 2020-04-28 西安交通大学 一种含尘油气的除尘装置及除尘方法
EP3976231A4 (en) * 2019-05-24 2023-10-11 Entegris, Inc. METHOD AND SYSTEMS FOR ADSORPTION OF ORGANOMETALLIC VAPORS
CN113993613A (zh) 2019-06-27 2022-01-28 托普索公司 具有浮动颗粒捕集器的催化反应器
CN115397541A (zh) 2020-04-27 2022-11-25 国际壳牌研究有限公司 气相沉积(gps)塔盘

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE217475C (xx) * 1900-01-01
DE450472C (de) * 1927-10-08 Wilhelm Wurl Pressluft-Wasserabscheider
DE438269C (de) * 1924-01-15 1926-12-13 Bernhard Christoffels Vorrichtung zum Reinigen von Gasen durch schuettbares Filtermaterial
DE740134C (de) * 1942-02-19 1943-10-13 Johannes Christiansen Gaserzeuger mit abwaerts gerichtetem Zug
FR55473E (fr) * 1942-07-20 1952-06-30 Gazogène perfectionné pour l'alimentation des moteurs des véhicules automobiles et autres applications
US2493356A (en) * 1943-02-16 1950-01-03 Moore Inc Apparatus for removing dust from gases
FR981451A (fr) * 1943-04-12 1951-05-28 Sebia Sa Perfectionnements aux générateurs de gazogènes à bois
GB894761A (en) * 1960-12-14 1962-04-26 Max Berz A cleaning device for dust-carrying gas
DE1916612U (de) * 1964-11-24 1965-05-26 Max Dipl Ing Berz Staubabscheider fuer staubhaltige gase.
DE1507780A1 (de) * 1965-11-24 1970-02-12 Berz Dipl Ing Max Verfahren zum Abscheiden von Stabteilchen aus einem Gasstrom
CH653360A5 (de) * 1980-09-19 1985-12-31 Sulzer Ag Heissgaskuehler an einer kohlevergasungsanlage.
DE3213664A1 (de) * 1982-04-14 1983-10-27 Margraf, Adolf, Dipl.-Ing., 3060 Stadthagen Vorrichtung zur reinigung von staubgasen
DE3223702C2 (de) * 1982-06-25 1984-06-28 M.A.N. Maschinenfabrik Augsburg-Nürnberg AG, 4200 Oberhausen Verfahren zur Erzeugung von Synthesegas und Reaktor zur Durchführung des Verfahrens
US4482358A (en) * 1983-03-17 1984-11-13 General Electric Company Granular bed filtering device
DE3311108A1 (de) * 1983-03-26 1984-09-27 Klöckner-Humboldt-Deutz AG, 5000 Köln Filter zur reinigung von gasen
JPS62125818A (ja) * 1985-11-26 1987-06-08 Mitsui Eng & Shipbuild Co Ltd 集塵濾過装置
DD260622A3 (de) * 1986-07-31 1988-10-05 Freiberg Brennstoffinst Verfahren und vorrichtung zur entstaubung und entteerung von rohgas
DE3636467A1 (de) * 1986-10-25 1988-04-28 Kloeckner Humboldt Deutz Ag Filter zur reinigung von gasen

Also Published As

Publication number Publication date
DE3827702C2 (xx) 1993-07-01
AU4003089A (en) 1990-02-22
AU620129B2 (en) 1992-02-13
ATE92949T1 (de) 1993-08-15
EP0358923A1 (de) 1990-03-21
JPH0291192A (ja) 1990-03-30
DE58905238D1 (de) 1993-09-16
DE3827702A1 (de) 1990-02-22
ZA896204B (en) 1990-05-30
ES2045296T3 (es) 1994-01-16

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