EP0314609B1 - Druckbehälter zur Speicherung von Gasen hoher Reinheit - Google Patents

Druckbehälter zur Speicherung von Gasen hoher Reinheit Download PDF

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Publication number
EP0314609B1
EP0314609B1 EP88730233A EP88730233A EP0314609B1 EP 0314609 B1 EP0314609 B1 EP 0314609B1 EP 88730233 A EP88730233 A EP 88730233A EP 88730233 A EP88730233 A EP 88730233A EP 0314609 B1 EP0314609 B1 EP 0314609B1
Authority
EP
European Patent Office
Prior art keywords
grade steel
adapter piece
steel cylinder
cylinder according
neck
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP88730233A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP0314609A3 (en
EP0314609A2 (en
Inventor
Ernst W. Dr. Ing. Lange
Karl Dipl.-Ing. Scholl
Dieter Dr. Ing. Vesperman
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Vodafone GmbH
Original Assignee
Mannesmann AG
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Filing date
Publication date
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Application filed by Mannesmann AG filed Critical Mannesmann AG
Priority to AT88730233T priority Critical patent/ATE89904T1/de
Publication of EP0314609A2 publication Critical patent/EP0314609A2/en
Publication of EP0314609A3 publication Critical patent/EP0314609A3/de
Application granted granted Critical
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Expired - Lifetime legal-status Critical Current

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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C1/00Pressure vessels, e.g. gas cylinder, gas tank, replaceable cartridge
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C1/00Pressure vessels, e.g. gas cylinder, gas tank, replaceable cartridge
    • F17C1/10Pressure vessels, e.g. gas cylinder, gas tank, replaceable cartridge with provision for protection against corrosion, e.g. due to gaseous acid
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C13/00Details of vessels or of the filling or discharging of vessels
    • F17C13/002Details of vessels or of the filling or discharging of vessels for vessels under pressure
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2201/00Vessel construction, in particular geometry, arrangement or size
    • F17C2201/01Shape
    • F17C2201/0104Shape cylindrical
    • F17C2201/0119Shape cylindrical with flat end-piece
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2201/00Vessel construction, in particular geometry, arrangement or size
    • F17C2201/03Orientation
    • F17C2201/032Orientation with substantially vertical main axis
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2201/00Vessel construction, in particular geometry, arrangement or size
    • F17C2201/05Size
    • F17C2201/056Small (<1 m3)
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2203/00Vessel construction, in particular walls or details thereof
    • F17C2203/06Materials for walls or layers thereof; Properties or structures of walls or their materials
    • F17C2203/0602Wall structures; Special features thereof
    • F17C2203/0612Wall structures
    • F17C2203/0614Single wall
    • F17C2203/0617Single wall with one layer
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2203/00Vessel construction, in particular walls or details thereof
    • F17C2203/06Materials for walls or layers thereof; Properties or structures of walls or their materials
    • F17C2203/0634Materials for walls or layers thereof
    • F17C2203/0636Metals
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2203/00Vessel construction, in particular walls or details thereof
    • F17C2203/06Materials for walls or layers thereof; Properties or structures of walls or their materials
    • F17C2203/0634Materials for walls or layers thereof
    • F17C2203/0636Metals
    • F17C2203/0639Steels
    • F17C2203/0643Stainless steels
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2203/00Vessel construction, in particular walls or details thereof
    • F17C2203/06Materials for walls or layers thereof; Properties or structures of walls or their materials
    • F17C2203/0634Materials for walls or layers thereof
    • F17C2203/0636Metals
    • F17C2203/0648Alloys or compositions of metals
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2203/00Vessel construction, in particular walls or details thereof
    • F17C2203/06Materials for walls or layers thereof; Properties or structures of walls or their materials
    • F17C2203/0634Materials for walls or layers thereof
    • F17C2203/0658Synthetics
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2203/00Vessel construction, in particular walls or details thereof
    • F17C2203/06Materials for walls or layers thereof; Properties or structures of walls or their materials
    • F17C2203/0634Materials for walls or layers thereof
    • F17C2203/0658Synthetics
    • F17C2203/0663Synthetics in form of fibers or filaments
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2205/00Vessel construction, in particular mounting arrangements, attachments or identifications means
    • F17C2205/01Mounting arrangements
    • F17C2205/0153Details of mounting arrangements
    • F17C2205/018Supporting feet
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2205/00Vessel construction, in particular mounting arrangements, attachments or identifications means
    • F17C2205/03Fluid connections, filters, valves, closure means or other attachments
    • F17C2205/0302Fittings, valves, filters, or components in connection with the gas storage device
    • F17C2205/0305Bosses, e.g. boss collars
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2205/00Vessel construction, in particular mounting arrangements, attachments or identifications means
    • F17C2205/03Fluid connections, filters, valves, closure means or other attachments
    • F17C2205/0302Fittings, valves, filters, or components in connection with the gas storage device
    • F17C2205/0308Protective caps
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2205/00Vessel construction, in particular mounting arrangements, attachments or identifications means
    • F17C2205/03Fluid connections, filters, valves, closure means or other attachments
    • F17C2205/0302Fittings, valves, filters, or components in connection with the gas storage device
    • F17C2205/0323Valves
    • F17C2205/0329Valves manually actuated
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2205/00Vessel construction, in particular mounting arrangements, attachments or identifications means
    • F17C2205/03Fluid connections, filters, valves, closure means or other attachments
    • F17C2205/0302Fittings, valves, filters, or components in connection with the gas storage device
    • F17C2205/0382Constructional details of valves, regulators
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2205/00Vessel construction, in particular mounting arrangements, attachments or identifications means
    • F17C2205/03Fluid connections, filters, valves, closure means or other attachments
    • F17C2205/0388Arrangement of valves, regulators, filters
    • F17C2205/0394Arrangement of valves, regulators, filters in direct contact with the pressure vessel
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2209/00Vessel construction, in particular methods of manufacturing
    • F17C2209/21Shaping processes
    • F17C2209/2172Polishing
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2209/00Vessel construction, in particular methods of manufacturing
    • F17C2209/22Assembling processes
    • F17C2209/221Welding
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2221/00Handled fluid, in particular type of fluid
    • F17C2221/01Pure fluids
    • F17C2221/016Noble gases (Ar, Kr, Xe)
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2221/00Handled fluid, in particular type of fluid
    • F17C2221/03Mixtures
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2221/00Handled fluid, in particular type of fluid
    • F17C2221/05Ultrapure fluid
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/01Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the phase
    • F17C2223/0107Single phase
    • F17C2223/0123Single phase gaseous, e.g. CNG, GNC
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/03Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the pressure level
    • F17C2223/036Very high pressure (>80 bar)
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2260/00Purposes of gas storage and gas handling
    • F17C2260/01Improving mechanical properties or manufacturing
    • F17C2260/012Reducing weight
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2260/00Purposes of gas storage and gas handling
    • F17C2260/05Improving chemical properties
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2260/00Purposes of gas storage and gas handling
    • F17C2260/05Improving chemical properties
    • F17C2260/053Reducing corrosion
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2270/00Applications
    • F17C2270/05Applications for industrial use
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2270/00Applications
    • F17C2270/05Applications for industrial use
    • F17C2270/0518Semiconductors

Definitions

  • the invention relates to a pressure vessel for storing and removing noble gas, special gas or gas mixtures of high purity according to the preamble of the main claim.
  • a pressure gas container made of an austenitic steel alloy in which ultra pure gases can be stored.
  • a metastable CrNi steel with defined contents of Ti, Nb, Ni and C is used as the container material.
  • the raw containers can be electrolytically polished and are plastically deformed by applying internal pressure at temperatures below the martensite transformation and thereby solidified.
  • the object of the invention is to provide a pressure vessel with a connection with improved properties for the storage and removal of noble gases, special gases and gas mixtures of high purity in order to avoid contamination and / or impairment of the mixture constancy of the gases during storage.
  • the pressure vessel and the connection should also be suitable for gas pressures up to approx. 200 bar and inexpensive to manufacture.
  • the solution to the problem is a pressure vessel with the characterizing features of the main claim.
  • the material of the pressure vessel is chemically resistant to a great extent to all gases and gas mixtures under consideration. It also has the property that it can be electro-polished to a high gloss (electrochemical polishing), as a result of which the active surface is leveled and considerably reduced compared to the unpolished state. This greatly reduces the absorption effect of the gases on the inner wall of the container and the release of particles. In addition, after electropolishing, the inner surface is free of residual mechanical stresses that have arisen from the manufacturing process, which reduces the tendency of the container material to sorb.
  • the pressure vessels in particular gas bottles, which mainly have the usual unit dimensions, are polished in the dipping process.
  • the pressure vessel itself is the vessel for receiving the electrolyte required for electropolishing.
  • a cathodic direct current electrode of sufficient length is inserted into the pressure vessel, so that the bottom and the head part, as well as in the case of the multi-part welded pressure vessel the weld or solder seams are polished inside.
  • Such a pressure vessel, in particular with a nickel content at the upper limit will be quite heavy and therefore expensive for higher pressures in the specified range, since the material has only moderate strength properties in the annealed state. Therefore, the measures according to the subclaims are also proposed.
  • One of the possibilities is to create a ferritic-austenitic mixed structure with a reduced nickel content, which increases the yield strength of the material by about a factor of 2.5 compared to the usual austenitic material with a small amount of molybdenum.
  • Another measure for reducing weight in the case of the multi-part welded pressure vessel is the additional work hardening of the cylindrical jacket of the pressure vessel.
  • a seamless or welded pipe is stretched close to the connection area by at least 10 to 35% in the wall thickness before it is welded to the head and bottom part.
  • the original wall thickness must remain in the connection area, since tempering the work-hardened area through the connection welding or soldering would negate the desired increase in strength. Because of the large length of the pressure vessel in relation to its diameter in some types, the stretching, for example, has a considerable weight-reducing effect on 75% of the original wall thickness.
  • a further measure with regard to saving weight is the reinforcement of the cylindrical part of the pressure vessel with a fiber winding covered by a plastic, which is applied without tension or under tension. Depending on the thickness and preload, part of the tension caused by the internal pressure is reduced via this winding, so that the wall thickness of the metallic body in the cylindrical region can be reduced.
  • the effect of saving weight is exacerbated when the proposal of a fiber winding is combined with a strain-hardened cylindrical jacket.
  • the pressure vessel can be manufactured in a seamless one-part or in a multi-part welded version.
  • the advantage of the multi-part welded design is that the individual parts can be easily machined so that the inner surfaces can be smoothed accordingly before electropolishing.
  • the small surface cracks that occur during hot forming of the top or bottom part of a one-piece bottle, which are usually unavoidable, can only be eliminated with great effort and only partially by electropolishing.
  • the effect of electropolishing is greater and the effort required for this is reduced, the smoother the surface is mechanically prepared.
  • Such a smooth surface can also be achieved by way of a one-piece pressure vessel produced by cold forming.
  • the neck area of the pressure vessel must be electropolished and the connection of the valve to the pressure vessel must not lead to material abrasion.
  • This arrangement has the advantage that the seal is only stressed by the non-rotatable adapter piece and therefore no abrasion is generated.
  • There are several options for securing the adapter against rotation e.g. B. to arrange an even polygonal profile in the form of secants for receiving an open-end wrench or a corresponding tool at the valve-side end of the adapter piece or to provide two blind holes extending in the axial direction in order to attach a hook wrench or a corresponding tool.
  • the adapter piece can be connected to the valve in such a way that the adapter piece is welded or soldered to the connecting body of the valve and then the entire device is electropolished in the immersion process.
  • a modification of this connection consists in arranging the connecting body of the valve in the bore of the adapter piece and providing a seam on the outside and / or inside at the transition point.
  • the adapter piece is provided with a standardized internal thread in the bore area and that the entire device is also electropolished after the connection body of the valve has been screwed on.
  • a sealing seam can also be attached to the transition point outside and / or inside. The screw connection without a sealing seam would have the advantage that the valve can be replaced at any time if the adapter piece is reusable.
  • the adapter piece is formed as an integral unit of the connecting body of the valve, then this unit can be screwed to the neck of the pressure vessel directly after the electropolishing and without a further connecting seam. It is also possible to design the adapter piece and the neck as an integral unit and the valve body with a corresponding collar on the neck to screw tight. As an alternative to the exemplary embodiment described, there is also the possibility of connecting the adapter piece directly to the neck of the pressure vessel via a seam. With this type of design, the sealing ring and the union nut would be omitted.
  • the connection options of the adapter piece with the valve correspond to those which have already been explained for the other exemplary embodiment.
  • the protective cap is screwed onto a section of the head part that carries an external thread, this section can be an integral part of the head part or is designed as a shrunk-on ring. This separation of the fastening of the protective cap and the valve ensures that the valve connection is not affected in the event of the bottle accidentally falling over or in the event of an unintended external impact on the protective cap.
  • the material used to make the adapter, union nut and valve body need not be identical to that of the pressure vessel, except that the adapter is an integral part of the neck. With regard to good machinability and shaping possibilities, it can be chosen accordingly, but must also meet the requirements of corrosion resistance and strength.
  • Figure 1 shows a longitudinal section (right half) and a plan view (left half) of a pressure vessel according to the invention.
  • the pressure vessel 1 is a multi-part welded design made of corrosion-resistant stainless steel, which is particularly suitable for storing and removing noble, special gases or gas mixtures of high purity and consists of a base part 2 welded to one another, a cylindrical jacket 3 and a head part 4 with a molded part Neck 5 is made.
  • the cylindrical jacket 3 is a longitudinally welded tube with a weld seam 7 running parallel to the container axis 6, but a seamless tube can also be used for this.
  • Bottom 2 and head part 4 are connected to the cylindrical jacket 3 by means of circular welds 8, 9, the three parts 2, 3, 4 of the pressure vessel 1 having been subjected to a heat treatment after being shaped, before being welded to one another.
  • the entire inner surface 10, 11, 12 of the pressure vessel 1, including the neck 5, is electropolished after the welding in order to reduce the roughness to a great extent and to reduce the remaining stresses.
  • the inner surfaces 10, 11, 12 can also be electropolished before welding, with post-treatment of the circular weld seams 8, 9 being necessary, depending on the requirements.
  • FIG. 2 the connection according to the invention is shown on an enlarged scale in longitudinal section.
  • An adapter piece 14 which is designed as an essentially cylindrical hollow body, is connected to the neck 5 of the pressure vessel 1 by means of a union nut 15.
  • the left half of the adapter piece 14 graphically represents the variant that the adapter piece 14 forms an integral unit with the connecting body 26 of the valve 25.
  • the adapter piece 14 has Region of the container-side end on an outwardly extending collar 16 which, like the cylindrical part 17, is surrounded by the union nut 15.
  • Connected to the bore part 18 of the union nut 15 is a part 19 which is provided with an internal thread and which is screwed to a neck 5 which carries an external thread 20 (FIG. 1).
  • a recess 22 is provided, into which a corrosion-resistant metallic seal 32 is arranged.
  • the seal 32 is pressed onto the end face 21 by the rotation of the union nut 15.
  • a central shoulder 23 is provided at the end on the container side, which is slightly smaller in diameter than the bore 13 of the neck 5. So that during the rotation of the union nut 15 no abrasion of the seal 32 producing rotation of the adapter piece 14 is possible , a cross-sectional shape 24 deviating from the circular shape is provided at the valve-side end.
  • two opposing secants are produced mechanically in a simple manner in order to be able to hold an open-end wrench or a comparable tool.
  • Other cross-sectional profiles that enable the adapter piece 14 to be held may just as well be.
  • Another possibility is to make two axially extending, mutually opposite blind holes in this valve-side end in order to insert a hook wrench.
  • a standard valve 25 is screwed into the adapter piece 14 with its connecting body 26 carrying a thread 33.
  • the adapter piece 14 can be welded to the connector body 26 and then electropolished without the sensitive mechanical valve parts (not shown here).
  • the known protective cap 27 is screwed onto an element 28 of the head part 4 which has an external thread. This element 28 can also be a ring shrunk onto the head part 4 (not shown here).

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Filling Or Discharging Of Gas Storage Vessels (AREA)
  • Testing, Inspecting, Measuring Of Stereoscopic Televisions And Televisions (AREA)
  • Stereoscopic And Panoramic Photography (AREA)
  • Projection Apparatus (AREA)
EP88730233A 1987-10-26 1988-10-25 Druckbehälter zur Speicherung von Gasen hoher Reinheit Expired - Lifetime EP0314609B1 (de)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AT88730233T ATE89904T1 (de) 1987-10-26 1988-10-25 Druckbehaelter zur speicherung von gasen hoher reinheit.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE3736579A DE3736579C3 (de) 1987-10-26 1987-10-26 Druckbehälter zur Speicherung von Gasen hoher Reinheit
DE3736579 1987-10-26

Publications (3)

Publication Number Publication Date
EP0314609A2 EP0314609A2 (en) 1989-05-03
EP0314609A3 EP0314609A3 (en) 1989-11-29
EP0314609B1 true EP0314609B1 (de) 1993-05-26

Family

ID=6339296

Family Applications (1)

Application Number Title Priority Date Filing Date
EP88730233A Expired - Lifetime EP0314609B1 (de) 1987-10-26 1988-10-25 Druckbehälter zur Speicherung von Gasen hoher Reinheit

Country Status (5)

Country Link
US (1) US4884708A (enrdf_load_stackoverflow)
EP (1) EP0314609B1 (enrdf_load_stackoverflow)
AT (1) ATE89904T1 (enrdf_load_stackoverflow)
DE (1) DE3736579C3 (enrdf_load_stackoverflow)
ES (1) ES2041333T3 (enrdf_load_stackoverflow)

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WO2022218672A1 (en) * 2021-04-12 2022-10-20 Carbon Cylinder S.R.L. Nozzle for high-pressure cylinders

Also Published As

Publication number Publication date
DE3736579A1 (de) 1989-05-03
ES2041333T3 (es) 1993-11-16
EP0314609A3 (en) 1989-11-29
ATE89904T1 (de) 1993-06-15
EP0314609A2 (en) 1989-05-03
US4884708A (en) 1989-12-05
DE3736579C2 (enrdf_load_stackoverflow) 1991-05-23
DE3736579C3 (de) 1996-10-17

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