EP0022739B1 - Procédé et dispositif pour la mesure du niveau de la scorie dans un récipient métallurgique et pour l'appréciation de son état physique - Google Patents
Procédé et dispositif pour la mesure du niveau de la scorie dans un récipient métallurgique et pour l'appréciation de son état physique Download PDFInfo
- Publication number
- EP0022739B1 EP0022739B1 EP80630021A EP80630021A EP0022739B1 EP 0022739 B1 EP0022739 B1 EP 0022739B1 EP 80630021 A EP80630021 A EP 80630021A EP 80630021 A EP80630021 A EP 80630021A EP 0022739 B1 EP0022739 B1 EP 0022739B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- crucible
- sensors
- level
- slag
- pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000002893 slag Substances 0.000 title claims abstract description 26
- 238000000034 method Methods 0.000 title claims abstract description 12
- 238000005259 measurement Methods 0.000 claims abstract description 9
- 239000011261 inert gas Substances 0.000 claims abstract description 6
- 230000002706 hydrostatic effect Effects 0.000 claims abstract description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 14
- 229910052757 nitrogen Inorganic materials 0.000 claims description 7
- 239000007789 gas Substances 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 2
- 229910052751 metal Inorganic materials 0.000 claims description 2
- 238000012856 packing Methods 0.000 claims description 2
- 238000010926 purge Methods 0.000 claims description 2
- 239000011819 refractory material Substances 0.000 claims description 2
- 229910000831 Steel Inorganic materials 0.000 claims 1
- 239000003870 refractory metal Substances 0.000 claims 1
- 239000010959 steel Substances 0.000 claims 1
- 239000000155 melt Substances 0.000 abstract 1
- 239000000161 steel melt Substances 0.000 abstract 1
- 238000011144 upstream manufacturing Methods 0.000 abstract 1
- 238000007664 blowing Methods 0.000 description 6
- 239000011449 brick Substances 0.000 description 4
- 238000010079 rubber tapping Methods 0.000 description 4
- 238000011161 development Methods 0.000 description 3
- 238000007670 refining Methods 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000005587 bubbling Effects 0.000 description 2
- 238000010411 cooking Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000006073 displacement reaction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005187 foaming Methods 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 238000010008 shearing Methods 0.000 description 2
- 238000010408 sweeping Methods 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
- 235000000396 iron Nutrition 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000009628 steelmaking Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21C—PROCESSING OF PIG-IRON, e.g. REFINING, MANUFACTURE OF WROUGHT-IRON OR STEEL; TREATMENT IN MOLTEN STATE OF FERROUS ALLOYS
- C21C5/00—Manufacture of carbon-steel, e.g. plain mild steel, medium carbon steel or cast steel or stainless steel
- C21C5/28—Manufacture of steel in the converter
- C21C5/42—Constructional features of converters
- C21C5/46—Details or accessories
- C21C5/4673—Measuring and sampling devices
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21C—PROCESSING OF PIG-IRON, e.g. REFINING, MANUFACTURE OF WROUGHT-IRON OR STEEL; TREATMENT IN MOLTEN STATE OF FERROUS ALLOYS
- C21C5/00—Manufacture of carbon-steel, e.g. plain mild steel, medium carbon steel or cast steel or stainless steel
- C21C5/28—Manufacture of steel in the converter
- C21C5/30—Regulating or controlling the blowing
Definitions
- the present invention relates to a method and a device for measuring the level and for assessing the physical state of the slag in a metallurgical vessel, in particular in a steelworks converter.
- Knowledge of the level of slag in a steelworks converter is important, both from the metallurgical point of view, as a parameter of the degree of refining progress, and from the point of view of safety, in order to prevent overflow .
- the applicant has developed a system for measuring the level of the slag which allows at the same time an evaluation of the consistency thereof, which constitutes important information, especially for the refining of phosphorous cast irons where a slag of a frothy consistency was considered desirable.
- This measurement system that the applicant has described in Luxembourg patent N ° 71,261, includes a thermostatically controlled acoustic duct which is placed above the converter and which picks up the noise emitted by the oxygen blowing lance. After filtering the frequencies whose origin is foreign to the parameters which are of interest for the measurement proper, we retain a signal whose interpretation allows us to conclude on the degree of the noise absorbed by the slag and thereby on the degree of the sparkling character present as well 'at its level in the crucible.
- the object of the invention therefore consisted in proposing a system for measuring the level of the slag and its physical state, this measurement system being largely independent of the degree of foaming of the slag and its performance being at least equivalent to that of the systems. known.
- the measuring method according to the invention which is characterized in that at least two hydrostatic pressure taps swept by gas jets are provided at different levels above the filling level of the crucible. inert with adjustable flow rate, that the pressures of said intakes are initially adjusted to equal values with each other, that the pressures existing at said intakes are then captured and that the level of slag in the crucible is determined by interpreting the deviations of the measured pressures from their initial values.
- the scanning of the intakes by means of the inert gas ensures that the mouth on the internal face of the refractory, in which the pressure intakes are housed, is always free and as little as possible affected by d '' possible splashes.
- the idea which is the basis of the invention therefore consists in measuring and interpreting the differences in hydrostatic pressure determined at several well defined levels above the level of the bath in the crucible.
- the operating principle of the method is as follows: Consider for example three pressure taps, of which 2 (A1 and A2) are at a same level and the 3rd (B) is placed at a higher level, the difference in levels being equal to H.
- the three intakes are swept by nitrogen flows such that the pressures P A1 , PA2 and P B are equal if the intakes freely open into the crucible cavity, in other words, in the absence of slag. This situation occurs between the development phases and we take advantage of this to align the three pressures to the same value before the start of blowing.
- the A1 socket is chosen as the reference socket. Its adjusted nitrogen flow determines the starting value of the pressure P Al . We then cancel the differences P A1 -PA2 resp. P A1 -P B.
- two sockets are therefore provided at the same level, which, in principle, provide identical results at all times. In other words, they allow a relative appreciation of their behavior. If after a few campaigns we find that the behavior of the 2 catches is satisfactory, that is to say reliable and reproducible, we can delete one of the sockets on level A, as well as the associated equipment.
- the device necessary for implementing the method according to the invention comprises at least two individual sensors, which are embedded at two different levels in the vertical wall of a crucible.
- Each sensor comprises a rigid pressure tapping tube housed in the crucible refractory, which tube is attached to a flexible tube which crosses the carcass of the crucible and establishes communication with a conventional pressure measuring instrument.
- FIG. 1 shows in a nonlimiting manner the diagram of a preferred embodiment of a pressure sensor according to the invention
- FIG. 2 shows a block diagram of a possible embodiment of the measuring assembly.
- the pressure tap brick (1) which can be the size of normal neighboring refractory bricks and which contains the pressure tap.
- This outlet is constituted by a tube made of a refractory material (11), preferably ceramic, which retains its shape, that is to say its cross section for the purging gas, at high temperatures.
- the tube (11) is housed in a metal tube (12) protecting it with respect to the mechanical forces arising especially during the cooking of the converter and at the start of the campaign until the cooking can be considered as finished.
- the combination of the two tubes, which wear in parallel with the refractory, must ensure a pressure drop - due to the sweeping gas - stable and reproducible during the whole crucible campaign.
- the pressure tapping brick On the side of the permanent lining (30), the pressure tapping brick is housed in a mattress of refractory fibers which aims to attenuate the shearing forces to which it risks being exposed at the level of the face separating the two layers of refractory.
- the pressure tapping brick (1) including the tubes (11), (12) and (13) are wear elements which are replaced each time the crucible is built.
- the work to be carried out during each replacement is to remove the plug (21), to insert the tube (13), to replace the plug (21), to tighten the packing (22) in order to make the plug watertight vis- opposite the carcass.
- the pressure is transmitted to the measuring instrument by a tube (41) with a diameter large enough so that there is no appreciable pressure drop due to the flow of the sweeping fluid, in particular the occurrence of nitrogen.
- the three intakes are swept by nitrogen flow rates such that the pressures P A1 , PA2 and P B are equal if the intakes freely open into the crucible cavity, which is the case in the absence of slag.
- the three pressures are therefore adjusted to the same value before the start of blowing and / or between the blowing phases.
- the socket (A1) is chosen as the reference socket.
- the nitrogen flow (N2) is adjusted manually using a pressure reducer (D).
- This flow rate determines the starting value of the pressure (P A1 ) '
- Two regulators (R) cancel the differences P AI -PA2 resp. P AL -P B by action on the valves (VA2) and V B ).
- This alignment accomplished - operation which takes a few seconds - the regulator inputs (R) are short-circuited which has the effect of freezing the control valves in their last position for example by means of position regulators. In the case of regulating valves controlled by an electric motor, it is sufficient to cut off the output of the regulators (R) in order to block the valves in their last position.
- the acquisition of A data can be centralized in a computer which is responsible for the transformation of the measurement results into meaningful information for the staff of the steelworks or in a computer which assumes the control of the steel making.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Carbon Steel Or Casting Steel Manufacturing (AREA)
- Waste-Gas Treatment And Other Accessory Devices For Furnaces (AREA)
- Treatment Of Steel In Its Molten State (AREA)
- Measurement Of Levels Of Liquids Or Fluent Solid Materials (AREA)
- Investigating And Analyzing Materials By Characteristic Methods (AREA)
- Testing Or Calibration Of Command Recording Devices (AREA)
- Medical Preparation Storing Or Oral Administration Devices (AREA)
- Mechanical Treatment Of Semiconductor (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT80630021T ATE756T1 (de) | 1979-07-16 | 1980-07-02 | Verfahren und vorrichtung zum messen des niveaus der schlacke in einem metallurgischen gefaess und zur beurteilung ihres physischen zustandes. |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
LU81512A LU81512A1 (fr) | 1979-07-16 | 1979-07-16 | Procede et dispositif pour la mesure du niveau de la scorie dans un recipient metallurgique et pour l'appreciation de son etat physique |
LU81512 | 1979-07-16 |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0022739A1 EP0022739A1 (fr) | 1981-01-21 |
EP0022739B1 true EP0022739B1 (fr) | 1982-03-17 |
Family
ID=19729200
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP80630021A Expired EP0022739B1 (fr) | 1979-07-16 | 1980-07-02 | Procédé et dispositif pour la mesure du niveau de la scorie dans un récipient métallurgique et pour l'appréciation de son état physique |
Country Status (12)
Country | Link |
---|---|
US (1) | US4359211A (pt) |
EP (1) | EP0022739B1 (pt) |
JP (1) | JPS5616614A (pt) |
AT (1) | ATE756T1 (pt) |
AU (1) | AU6041580A (pt) |
BR (1) | BR8004359A (pt) |
CA (1) | CA1159923A (pt) |
DE (1) | DE3060230D1 (pt) |
ES (1) | ES493399A0 (pt) |
LU (1) | LU81512A1 (pt) |
PT (1) | PT71535A (pt) |
ZA (1) | ZA804241B (pt) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19962632C2 (de) * | 1998-12-24 | 2002-05-16 | Woojin Inc | Verfahren zur Messung der Dicke einer Schlacke bei der Stahlherstellung |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5963520U (ja) * | 1982-10-21 | 1984-04-26 | 株式会社河合楽器製作所 | ミキサ |
JPS59114716U (ja) * | 1983-01-25 | 1984-08-02 | 古河電気工業株式会社 | ケ−ブル貫通部 |
JPH0688127B2 (ja) * | 1988-03-09 | 1994-11-09 | 川崎製鉄株式会社 | スラグ流出検知方法 |
US5289716A (en) * | 1992-08-21 | 1994-03-01 | The United States Of America As Represented By The United States Department Of Energy | Monitoring and analyzing waste glass compositions |
US5650117A (en) * | 1995-09-27 | 1997-07-22 | Vesuvius Crucible Company | Slag detecting apparatus and method |
US6130637A (en) * | 1998-08-18 | 2000-10-10 | Usx Corporation | Measuring the thickness of hot slag in steelmaking |
US6166681A (en) * | 1998-08-18 | 2000-12-26 | Usx Corporation | Measuring the thickness of materials |
JP2010090675A (ja) * | 2008-10-10 | 2010-04-22 | Daiwa Kiko Kk | 側壁撤去装置 |
US8482295B2 (en) * | 2009-02-23 | 2013-07-09 | Hatch Ltd. | Electromagnetic bath level measurement for pyrometallurgical furnaces |
AT514132B1 (de) | 2013-03-25 | 2015-11-15 | Voestalpine Stahl Gmbh | Verfahren zur Bestimmung von Reaktionsdaten eines Reaktionsablaufs |
TWI706124B (zh) | 2019-09-04 | 2020-10-01 | 國立中央大學 | 物性測量裝置及測量物性的方法 |
Citations (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1457406A (en) * | 1919-06-19 | 1923-06-05 | Pneumercator Company | Depth and specific-gravity measuring apparatus |
FR1481242A (fr) * | 1966-04-07 | 1967-05-19 | Gaz De France | Procédé et dispositif de mesure de la hauteur d'un liquide contenu dans une cuve ou analogue |
AT260962B (de) * | 1963-02-21 | 1968-04-10 | Waagner Biro Ag | Verfahren zur Steuerung des Verbrennungsvorganges von Gasen sowie Vorrichtung zur Durchführung dieses Verfahrens |
DE1274146B (de) * | 1965-08-26 | 1968-08-01 | Foerderung Der Eisenhuettentec | Vorrichtung zum kontinuierlichen Messen der Temperatur von Konverterschmelzen |
DE1508250B1 (de) * | 1966-10-27 | 1970-04-09 | Siemens Ag | Anordnung zur Messung der Temperatur von Metallschmelzen,vorzugsweise in Konvertergefaessen |
US3620085A (en) * | 1969-03-27 | 1971-11-16 | Cermat | Apparatus for measuring the level of liquid in a reservoir |
DE2239216A1 (de) * | 1971-08-18 | 1973-05-03 | Allegheny Ludlum Ind Inc | Anordnung und verfahren zum ermitteln der eintauchtiefe einer lanze |
DE2452655A1 (de) * | 1973-11-08 | 1975-06-12 | Cermat | Verfahren und vorrichtung zum messen des standes und des spezifischen gewichts einer in behaeltern grossen fassungsvermoegens enthaltenen fluessigkeit |
JPS5252108A (en) * | 1975-10-24 | 1977-04-26 | Nippon Steel Corp | Pocess for efining by converter |
DE2834737A1 (de) * | 1977-08-26 | 1979-03-08 | British Steel Corp | Stahlherstellungsverfahren |
LU81207A1 (fr) * | 1979-04-30 | 1980-12-16 | Arbed | Procede d'affinage d'un bain de metal contenant des matieres refroidissantes solides |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR481242A (fr) * | 1916-03-16 | 1916-11-14 | Secondo Torta & Cie Soc | Bougie d'allumage pour moteurs à explosions |
US3200971A (en) * | 1961-08-01 | 1965-08-17 | Owens Corning Fiberglass Corp | Apparatus and method for controlling liquid level |
FR1363687A (fr) * | 1963-07-17 | 1964-06-12 | Bot Brassert Oxygen Technik Ag | Procédé et dispositif de réglage de fonctionnement pour opérations de soufflage ou pour des méthodes analogues d'affinage métallurgique |
US3476538A (en) * | 1965-10-24 | 1969-11-04 | Owens Corning Fiberglass Corp | Process and apparatus for controlling the flow of molten glass |
FR1540757A (fr) * | 1967-10-12 | 1968-09-27 | Beteiligungs & Patentverw Gmbh | Procédé et dispositif pour déterminer l'état des scories dans un convertisseur |
CH475551A (de) * | 1968-05-31 | 1969-07-15 | Brehm Dr Ingbureau Ag | Füllstandsanzeiger an Behälter für flüssiges oder pulverförmiges Gut |
US3590843A (en) * | 1969-10-23 | 1971-07-06 | Gen Electric | Multiple-jet liquid level detector |
DE2354003C2 (de) * | 1973-10-27 | 1975-02-13 | Stahlwerke Peine-Salzgitter Ag, 3150 Peine | Verfahren und Vorrichtung zur Überwachung und Steuerung des Reaktionsablaufes beim Frischen von Roheisen Stahlwerke Peine-Salzgitter AG, 315OPeine |
US3850416A (en) * | 1974-01-04 | 1974-11-26 | Ford Motor Co | Slag depth indicator |
FR2340156A2 (fr) * | 1976-02-03 | 1977-09-02 | Pechiney Aluminium | Procede et dispositif de moulage sous basse pression |
DE2706558A1 (de) * | 1976-03-15 | 1977-09-22 | Erwin Buehrer | Verfahren und einrichtung zum abgiessen einer form mit einer waehlbaren menge von fluessigem metall |
US4102190A (en) * | 1977-04-07 | 1978-07-25 | Bethlehem Steel Corporation | Method and apparatus for determining the weight of slag on a bath of molten metal |
US4288062A (en) * | 1979-08-09 | 1981-09-08 | Holcroft | Apparatus for control and monitoring of the carbon potential of an atmosphere in a heat-processing furnace |
-
1979
- 1979-07-16 LU LU81512A patent/LU81512A1/fr unknown
-
1980
- 1980-07-02 EP EP80630021A patent/EP0022739B1/fr not_active Expired
- 1980-07-02 AT AT80630021T patent/ATE756T1/de not_active IP Right Cessation
- 1980-07-02 DE DE8080630021T patent/DE3060230D1/de not_active Expired
- 1980-07-11 PT PT71535A patent/PT71535A/pt unknown
- 1980-07-14 BR BR8004359A patent/BR8004359A/pt not_active IP Right Cessation
- 1980-07-14 ZA ZA00804241A patent/ZA804241B/xx unknown
- 1980-07-14 CA CA000356149A patent/CA1159923A/fr not_active Expired
- 1980-07-15 ES ES493399A patent/ES493399A0/es active Granted
- 1980-07-15 US US06/169,481 patent/US4359211A/en not_active Expired - Lifetime
- 1980-07-15 AU AU60415/80A patent/AU6041580A/en not_active Abandoned
- 1980-07-16 JP JP9742880A patent/JPS5616614A/ja active Pending
Patent Citations (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1457406A (en) * | 1919-06-19 | 1923-06-05 | Pneumercator Company | Depth and specific-gravity measuring apparatus |
AT260962B (de) * | 1963-02-21 | 1968-04-10 | Waagner Biro Ag | Verfahren zur Steuerung des Verbrennungsvorganges von Gasen sowie Vorrichtung zur Durchführung dieses Verfahrens |
DE1274146B (de) * | 1965-08-26 | 1968-08-01 | Foerderung Der Eisenhuettentec | Vorrichtung zum kontinuierlichen Messen der Temperatur von Konverterschmelzen |
FR1481242A (fr) * | 1966-04-07 | 1967-05-19 | Gaz De France | Procédé et dispositif de mesure de la hauteur d'un liquide contenu dans une cuve ou analogue |
DE1508250B1 (de) * | 1966-10-27 | 1970-04-09 | Siemens Ag | Anordnung zur Messung der Temperatur von Metallschmelzen,vorzugsweise in Konvertergefaessen |
US3620085A (en) * | 1969-03-27 | 1971-11-16 | Cermat | Apparatus for measuring the level of liquid in a reservoir |
DE2239216A1 (de) * | 1971-08-18 | 1973-05-03 | Allegheny Ludlum Ind Inc | Anordnung und verfahren zum ermitteln der eintauchtiefe einer lanze |
DE2452655A1 (de) * | 1973-11-08 | 1975-06-12 | Cermat | Verfahren und vorrichtung zum messen des standes und des spezifischen gewichts einer in behaeltern grossen fassungsvermoegens enthaltenen fluessigkeit |
JPS5252108A (en) * | 1975-10-24 | 1977-04-26 | Nippon Steel Corp | Pocess for efining by converter |
DE2834737A1 (de) * | 1977-08-26 | 1979-03-08 | British Steel Corp | Stahlherstellungsverfahren |
LU81207A1 (fr) * | 1979-04-30 | 1980-12-16 | Arbed | Procede d'affinage d'un bain de metal contenant des matieres refroidissantes solides |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19962632C2 (de) * | 1998-12-24 | 2002-05-16 | Woojin Inc | Verfahren zur Messung der Dicke einer Schlacke bei der Stahlherstellung |
Also Published As
Publication number | Publication date |
---|---|
CA1159923A (fr) | 1984-01-03 |
ATE756T1 (de) | 1982-04-15 |
ES8103179A1 (es) | 1981-02-16 |
EP0022739A1 (fr) | 1981-01-21 |
JPS5616614A (en) | 1981-02-17 |
ZA804241B (en) | 1981-07-29 |
DE3060230D1 (en) | 1982-04-15 |
AU6041580A (en) | 1981-01-22 |
BR8004359A (pt) | 1981-01-27 |
US4359211A (en) | 1982-11-16 |
PT71535A (fr) | 1980-08-01 |
ES493399A0 (es) | 1981-02-16 |
LU81512A1 (fr) | 1981-02-03 |
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