EG25565A - Reactor for preparing hydrogen cyanide by the andrussow process - Google Patents

Reactor for preparing hydrogen cyanide by the andrussow process

Info

Publication number
EG25565A
EG25565A EG2010010113A EG2010010113A EG25565A EG 25565 A EG25565 A EG 25565A EG 2010010113 A EG2010010113 A EG 2010010113A EG 2010010113 A EG2010010113 A EG 2010010113A EG 25565 A EG25565 A EG 25565A
Authority
EG
Egypt
Prior art keywords
reactor
hydrogen cyanide
preparing hydrogen
andrussow process
andrussow
Prior art date
Application number
EG2010010113A
Other languages
English (en)
Inventor
Thomas Schafer
Robert Weber
Udo Gropp
Thomas Mertz
Original Assignee
Evonik Roehm Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Roehm Gmbh filed Critical Evonik Roehm Gmbh
Application granted granted Critical
Publication of EG25565A publication Critical patent/EG25565A/xx

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J12/00Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
    • B01J12/007Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor in the presence of catalytically active bodies, e.g. porous plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B01J8/009Membranes, e.g. feeding or removing reactants or products to or from the catalyst bed through a membrane
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0242Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly vertical
    • B01J8/025Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly vertical in a cylindrical shaped bed
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0285Heating or cooling the reactor
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00Cyanogen; Compounds thereof
    • C01C3/02Preparation, separation or purification of hydrogen cyanide
    • C01C3/0208Preparation in gaseous phase
    • C01C3/0212Preparation in gaseous phase from hydrocarbons and ammonia in the presence of oxygen, e.g. the Andrussow-process
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00Cyanogen; Compounds thereof
    • C01C3/02Preparation, separation or purification of hydrogen cyanide
    • C01C3/0208Preparation in gaseous phase
    • C01C3/0212Preparation in gaseous phase from hydrocarbons and ammonia in the presence of oxygen, e.g. the Andrussow-process
    • C01C3/022Apparatus therefor
    • C01C3/0225Apparatus therefor characterised by the synthesis reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00106Controlling the temperature by indirect heat exchange
    • B01J2208/00168Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00194Tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/0053Controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796Details of the reactor or of the particulate material
    • B01J2208/00823Mixing elements
    • B01J2208/00831Stationary elements
    • B01J2208/00849Stationary elements outside the bed, e.g. baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796Details of the reactor or of the particulate material
    • B01J2208/00884Means for supporting the bed of particles, e.g. grids, bars, perforated plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081Tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00159Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Toxicology (AREA)
  • Inorganic Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Catalysts (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Hydrogen, Water And Hydrids (AREA)
EG2010010113A 2007-07-23 2010-01-21 Reactor for preparing hydrogen cyanide by the andrussow process EG25565A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102007034715A DE102007034715A1 (de) 2007-07-23 2007-07-23 Reaktor zur Herstellung von Cyanwasserstoff nach dem Andrussow-Verfahren
PCT/EP2008/055730 WO2009013035A1 (de) 2007-07-23 2008-05-09 Reaktor zur herstellung von cyanwasserstoff nach dem andrussow-verfahren

Publications (1)

Publication Number Publication Date
EG25565A true EG25565A (en) 2012-02-27

Family

ID=39596817

Family Applications (1)

Application Number Title Priority Date Filing Date
EG2010010113A EG25565A (en) 2007-07-23 2010-01-21 Reactor for preparing hydrogen cyanide by the andrussow process

Country Status (16)

Country Link
US (1) US8802020B2 (ru)
EP (1) EP2170499B1 (ru)
JP (1) JP5656631B2 (ru)
KR (1) KR101527240B1 (ru)
CN (1) CN101353173B (ru)
AU (1) AU2008280378B2 (ru)
BR (1) BRPI0703617B1 (ru)
CA (1) CA2694236C (ru)
DE (1) DE102007034715A1 (ru)
EG (1) EG25565A (ru)
ES (1) ES2614277T3 (ru)
MY (1) MY154793A (ru)
RU (1) RU2470860C2 (ru)
TW (1) TWI505991B (ru)
WO (1) WO2009013035A1 (ru)
ZA (1) ZA201000527B (ru)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5656872B2 (ja) * 2009-01-21 2015-01-21 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 非触媒作用又は均一系触媒作用反応のための管束反応器
ES2526165T3 (es) 2011-02-23 2015-01-07 Evonik Degussa Gmbh Nitrilo del ácido 2-hidroxi-4-(metiltio)butírico estable al almacenamiento
SG192565A1 (en) 2011-02-23 2013-09-30 Evonik Degussa Gmbh Method for producing 2-hydroxy-4-(methylthio)butanenitrile from 3-(methylthio)propanal and hydrogen cyanide
EP2644263A1 (de) 2012-03-28 2013-10-02 Aurotec GmbH Druckgeregelter Reaktor
EP2644264A1 (de) 2012-03-28 2013-10-02 Aurotec GmbH Druckreguliertes Mehrreaktorsystem
EP2703076B1 (de) * 2012-08-29 2016-04-27 Wolfgang Gerlinger Reaktor mit einer oder mehreren zuführleitungen und einer gleichverteilungseinrichtung für einen oder mehrere fluidströme
TWI519480B (zh) * 2012-12-18 2016-02-01 英威達技術有限公司 使用整流器之製造氰化氫的方法
WO2014099563A1 (en) * 2012-12-18 2014-06-26 Invista North America S.A R.L. Reactor scheme in andrussow process
RU2015128903A (ru) * 2012-12-18 2017-01-25 Инвиста Текнолоджиз С.А.Р.Л. Устройство и способ регенерации водорода в процессе андрусова
US20150353371A1 (en) 2012-12-18 2015-12-10 Invista North America S.A R.L. Processes for producing hydrogen cyanide using static mixer
CN113603115A (zh) * 2012-12-18 2021-11-05 英威达纺织(英国)有限公司 采用催化剂床层生产氰化氢的方法
CN113816398B (zh) * 2012-12-18 2023-11-10 英威达纺织(英国)有限公司 安德卢梭法中氨比例的变化
WO2014099572A1 (en) * 2012-12-18 2014-06-26 Invista Technologies S.A R.L. Process for producing hydrogen cyanide using a distributor plate
TW201441157A (zh) * 2012-12-18 2014-11-01 Invista Tech Sarl 在安德盧梭(andrussow)法中用於回收之系統及方法
WO2014099568A1 (en) * 2012-12-18 2014-06-26 Invista Technologies S.A.R.L. Enhanced methane control for andrussow process
WO2014099601A1 (en) * 2012-12-18 2014-06-26 Invista Technologies S.A.R.L. Process for stabilizing heat exchanger tubes in andrussow process
FR3008692B1 (fr) * 2013-07-19 2016-12-23 Arkema France Installation et procede pour la preparation de cyanure d'hydrogene
FR3008626B1 (fr) * 2013-07-19 2015-08-07 Arkema France Reacteur pour preparer du cyanure d'hydrogene par le procede d'andrussow, equipement comprenant ledit reacteur et procede utilisant un tel equipement
EP3475248B1 (de) 2016-06-27 2020-08-05 Evonik Operations GmbH Dipeptidhaltige granulate
EP3339289A1 (de) 2016-12-21 2018-06-27 Evonik Degussa GmbH Verfahren zur herstellung von methionin
WO2019020705A1 (en) * 2017-07-27 2019-01-31 Haldor Topsøe A/S CATALYTIC REACTOR COMPRISING A FIBROUS CATALYST PARTICLE CARRIER
EP3461803A1 (de) 2017-10-02 2019-04-03 Evonik Degussa GmbH Herstellverfahren für dipeptidhaltige granulate
ES2930162T3 (es) 2018-12-14 2022-12-07 Evonik Operations Gmbh Método para producir metionina
CN111533136A (zh) * 2020-07-03 2020-08-14 重庆奕翔化工有限公司 一种氢氰酸的生产系统及工艺
CN115371047A (zh) * 2021-05-19 2022-11-22 武汉氢阳能源有限公司 一种新型防回火氢气催化燃烧反应器
CN113267076B (zh) * 2021-06-04 2022-08-23 四川能投建工集团设计研究院有限公司 一种氢氰酸氧化反应器及其管板冷却结构
CN117205848A (zh) * 2023-11-07 2023-12-12 上海氢田新材料科技有限公司 一种基于气相分解法制备纳米硅的系统及方法

Family Cites Families (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2011A (en) * 1841-03-18 Appabatxts for piling saws
US4015A (en) * 1845-04-26 Hand-loom for weaving figured fabrics
US1934838A (en) 1930-04-14 1933-11-14 Ig Farbenindustrie Ag Production of hydrocyanic acid
DE549055C (de) 1930-04-15 1932-04-22 I G Farbenindustrie Akt Ges Verfahren zur Herstellung von Cyanwasserstoff
US2387577A (en) * 1943-09-20 1945-10-23 Du Pont Production of hydrocyanic acid
US2404574A (en) * 1943-11-30 1946-07-23 Us Ind Chemicals Inc Apparatus for catalytic operations
US2782107A (en) * 1953-01-14 1957-02-19 Du Pont Reactor for making hydrogen cyanide
US2750266A (en) * 1954-06-25 1956-06-12 Chemical Construction Corp Catalytic reactor for hydrocyanic acid production
US2906604A (en) * 1955-08-01 1959-09-29 Sueddeutsche Kalkstickstoff Method of producing hydrogen cyanide
US2893852A (en) * 1956-04-16 1959-07-07 American Oil Co Fixed bed reformer vapor distributor
US3073685A (en) * 1960-06-15 1963-01-15 Monsanto Chemicals Gauze catalyst support
US3215495A (en) * 1962-01-23 1965-11-02 Du Pont Apparatus and process for preparing hydrogen cyanide
US3505030A (en) * 1965-11-16 1970-04-07 Du Pont Composite articles of manufacture and apparatus for their use
US3545939A (en) * 1968-11-08 1970-12-08 Union Carbide Corp Catalyst system for making hydrogen cyanide
US4128622A (en) 1976-08-27 1978-12-05 E. I. Du Pont De Nemours And Company Process for producing hydrogen cyanide
DE2913925C2 (de) * 1979-04-06 1982-06-03 Degussa Ag, 6000 Frankfurt Verfahren zur Herstellung von Cyanwasserstoff
US5431984A (en) 1990-12-11 1995-07-11 Avco Corporation Composite preforms with groves for fibers and groves for off-gassing
US5242882A (en) * 1992-05-11 1993-09-07 Scientific Design Company, Inc. Catalyst for the production of nitric acid by oxidation of ammonia
DE4411774C1 (de) 1994-04-06 1995-08-17 Degussa Katalysatornetze für Gasreaktionen
US6073467A (en) * 1994-04-06 2000-06-13 Degussa Aktiengesellschaft Catalyst gauzes for gaseous reactions
EP0680767A1 (en) 1994-05-06 1995-11-08 Nardino Righi Non-reusable safety syringe
US6491876B2 (en) * 1995-09-01 2002-12-10 Imperial Chemical Industries Plc Hydrogen cyanide process and apparatus therefor
CN1112961C (zh) * 1997-07-03 2003-07-02 纳幕尔杜邦公司 感应加热的催化反应器
KR100474613B1 (ko) 1997-07-03 2005-03-08 이 아이 듀폰 디 네모아 앤드 캄파니 화학 반응의 유도 점화 방법
AU1842899A (en) * 1998-02-25 1999-09-09 African Oxygen Limited Reactor for hydrogen cyanide gas production
US6221327B1 (en) * 1998-05-15 2001-04-24 Rohm And Haas Company Catalyst system using flow-through radiation shielding and a process for producing hydrogen cyanide using the same
AU4090600A (en) * 1999-06-30 2001-01-04 Rohm And Haas Company High performance heat exchangers
US6579510B2 (en) * 1999-07-30 2003-06-17 Alfred E. Keller SPOX-enhanced process for production of synthesis gas
RU2191746C2 (ru) * 2000-01-27 2002-10-27 Открытое акционерное общество "Волжский Оргсинтез" Способ получения цианистого водорода
AU2001255670A1 (en) 2000-04-25 2001-11-07 E.I. Du Pont De Nemours And Company Catalyst and process for gas phase reactions
FR2812221B1 (fr) 2000-07-28 2003-04-04 Butachimie Nouveau dispositif catalytique pour la mise en oeuvre d'une reaction en milieu gazeux a haute temperature
JP3913469B2 (ja) 2000-12-27 2007-05-09 株式会社コロナ ふろ装置のリモコン装置
RU2298433C2 (ru) 2001-02-08 2007-05-10 Умикор АГ энд Ко. КГ. Трехмерные каталитические сетки, сплетенные в два или более слоев
AU2003277837A1 (en) 2002-11-08 2004-06-07 Morten Muller Ltd., Aps Mixing device for two-phase concurrent vessels
FR2850372B1 (fr) * 2003-01-23 2006-06-09 Inst Francais Du Petrole Nouveau reacteur d'oxydation partielle
WO2008105669A1 (en) * 2007-03-01 2008-09-04 Eicproc As A process for the production of cyanides

Also Published As

Publication number Publication date
CN101353173A (zh) 2009-01-28
AU2008280378B2 (en) 2013-11-28
JP2010534182A (ja) 2010-11-04
TW200922874A (en) 2009-06-01
JP5656631B2 (ja) 2015-01-21
CN101353173B (zh) 2014-08-13
DE102007034715A1 (de) 2009-01-29
WO2009013035A1 (de) 2009-01-29
BRPI0703617B1 (pt) 2017-06-13
CA2694236A1 (en) 2009-01-29
KR20100051622A (ko) 2010-05-17
ES2614277T3 (es) 2017-05-30
RU2010105920A (ru) 2011-08-27
KR101527240B1 (ko) 2015-06-09
EP2170499A1 (de) 2010-04-07
US20110171101A1 (en) 2011-07-14
EP2170499B1 (de) 2016-11-16
CA2694236C (en) 2015-11-10
TWI505991B (zh) 2015-11-01
RU2470860C2 (ru) 2012-12-27
BRPI0703617A2 (pt) 2009-03-10
MY154793A (en) 2015-07-31
AU2008280378A1 (en) 2009-01-29
ZA201000527B (en) 2010-10-27
US8802020B2 (en) 2014-08-12

Similar Documents

Publication Publication Date Title
EG25565A (en) Reactor for preparing hydrogen cyanide by the andrussow process
EP2294002A4 (en) IMPROVED METHOD FOR THE PRODUCTION OF HYDROGEN
IL202140A0 (en) Method for the production of hydrogen from ammonia borane
EP2341040A4 (en) PROCESS FOR PRODUCING 1,3,3,3-TETRAFLUOROPROPENE
HK1211280A1 (en) Process for the praparation of 2,3,3,3-tetrafluoropropene 2333-
PL2583959T3 (pl) Zintegrowany sposób wytwarzania 2,3,3,3-tetrafluoropropenu
ZA201007557B (en) Process for producing an organo-mineral fertilizer
EG26693A (en) Low-energy process to produce ammonia or methanol
EG25746A (en) Process for producing ammonia synthesis gas
EG25151A (en) Process for hydrogen production.
PL2292574T3 (pl) Proces wytwarzania 2,3,3,3-tetrafluoropropenu
HK1160097A1 (en) Process for the production of ammonia
HK1142055A1 (en) Hydrogen catalyst reactor
ZA201104061B (en) Reactor for preparing syngas
EP2510020A4 (en) MULTI-REACTOR PROCESS
PL2438033T3 (pl) Proces wytwarzania 2,3,3,3 - tetrafluoropropenu
IL217610A (en) A process for preparing 2,2-diplooroethylamine
IL202831A0 (en) Process for performing an endothermic reaction
EP2586759A4 (en) PROCESS FOR PRODUCING 2,3,3,3-TETRAFLUOROPROPENE
PL2417086T3 (pl) Sposób wytwarzania 3,3,3-trifluoropropenu
EP2132138A4 (en) PROCESS FOR THE PRODUCTION OF CYANIDES
ZA201004142B (en) Improved process for preparing hydrogen cyanide by catalytic dehydration of gaseous formamide
EP2586760A4 (en) PROCESS FOR THE PREPARATION OF 2,3,3,3-TETRAFLUOROPROPES
IL211307A0 (en) Process for preparing cinacalcet
SI2281801T1 (sl) Postopek za pridobivanje 3,3-diphenilpropilamina