EA028106B1 - Полые микросферы и способ получения полых микросфер - Google Patents
Полые микросферы и способ получения полых микросфер Download PDFInfo
- Publication number
- EA028106B1 EA028106B1 EA201300432A EA201300432A EA028106B1 EA 028106 B1 EA028106 B1 EA 028106B1 EA 201300432 A EA201300432 A EA 201300432A EA 201300432 A EA201300432 A EA 201300432A EA 028106 B1 EA028106 B1 EA 028106B1
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- hollow microspheres
- heating system
- grinding
- glass
- oxides
- Prior art date
Links
- 239000004005 microsphere Substances 0.000 title claims abstract description 95
- 238000004519 manufacturing process Methods 0.000 title description 16
- 238000000034 method Methods 0.000 claims abstract description 47
- 239000000463 material Substances 0.000 claims description 101
- 238000010438 heat treatment Methods 0.000 claims description 68
- 239000011521 glass Substances 0.000 claims description 41
- 238000000227 grinding Methods 0.000 claims description 27
- 229910052751 metal Inorganic materials 0.000 claims description 17
- 239000002184 metal Substances 0.000 claims description 17
- 150000002739 metals Chemical class 0.000 claims description 13
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims description 12
- 229910052753 mercury Inorganic materials 0.000 claims description 12
- 239000012159 carrier gas Substances 0.000 claims description 10
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 9
- 239000002356 single layer Substances 0.000 claims description 9
- 229910052717 sulfur Inorganic materials 0.000 claims description 9
- 239000011593 sulfur Substances 0.000 claims description 9
- 229910000272 alkali metal oxide Inorganic materials 0.000 claims description 5
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims description 4
- 239000011737 fluorine Substances 0.000 claims description 4
- 229910052731 fluorine Inorganic materials 0.000 claims description 4
- 229910052738 indium Inorganic materials 0.000 claims description 4
- 239000004615 ingredient Substances 0.000 claims description 4
- 239000010451 perlite Substances 0.000 claims description 4
- 235000019362 perlite Nutrition 0.000 claims description 4
- 238000012546 transfer Methods 0.000 claims description 2
- 239000002245 particle Substances 0.000 description 21
- 239000004604 Blowing Agent Substances 0.000 description 15
- 238000002844 melting Methods 0.000 description 11
- 230000008018 melting Effects 0.000 description 11
- 239000000203 mixture Substances 0.000 description 11
- 210000003739 neck Anatomy 0.000 description 10
- 230000015572 biosynthetic process Effects 0.000 description 8
- 239000007788 liquid Substances 0.000 description 8
- 230000008569 process Effects 0.000 description 8
- 238000005755 formation reaction Methods 0.000 description 7
- 239000002131 composite material Substances 0.000 description 6
- 238000001816 cooling Methods 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 239000003570 air Substances 0.000 description 5
- 239000004568 cement Substances 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 5
- 239000004567 concrete Substances 0.000 description 5
- 239000000945 filler Substances 0.000 description 5
- 229920000642 polymer Polymers 0.000 description 5
- 239000002360 explosive Substances 0.000 description 4
- 230000003287 optical effect Effects 0.000 description 4
- 239000012080 ambient air Substances 0.000 description 3
- 238000013461 design Methods 0.000 description 3
- 229910044991 metal oxide Inorganic materials 0.000 description 3
- 150000004706 metal oxides Chemical class 0.000 description 3
- 239000003607 modifier Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000007789 sealing Methods 0.000 description 3
- 239000005368 silicate glass Substances 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 239000000758 substrate Substances 0.000 description 3
- 230000007704 transition Effects 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000005553 drilling Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000012634 fragment Substances 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 230000035515 penetration Effects 0.000 description 2
- 239000005060 rubber Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000006557 surface reaction Methods 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 239000002023 wood Substances 0.000 description 2
- 235000019738 Limestone Nutrition 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 239000011398 Portland cement Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 230000002238 attenuated effect Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000005524 ceramic coating Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000011231 conductive filler Substances 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 229910001882 dioxygen Inorganic materials 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- VJYFKVYYMZPMAB-UHFFFAOYSA-N ethoprophos Chemical compound CCCSP(=O)(OCC)SCCC VJYFKVYYMZPMAB-UHFFFAOYSA-N 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 229920000876 geopolymer Polymers 0.000 description 1
- -1 heat-shrinkable Polymers 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000001746 injection moulding Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 239000006028 limestone Substances 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000003129 oil well Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 150000002927 oxygen compounds Chemical class 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 239000011505 plaster Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000002285 radioactive effect Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000005488 sandblasting Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- 230000001755 vocal effect Effects 0.000 description 1
- 239000011800 void material Substances 0.000 description 1
- 239000013585 weight reducing agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/10—Forming beads
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/10—Forming beads
- C03B19/107—Forming hollow beads
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C11/00—Multi-cellular glass ; Porous or hollow glass or glass particles
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C11/00—Multi-cellular glass ; Porous or hollow glass or glass particles
- C03C11/002—Hollow glass particles
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C12/00—Powdered glass; Bead compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacturing & Machinery (AREA)
- Glass Compositions (AREA)
- Manufacturing Of Micro-Capsules (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201061424960P | 2010-12-20 | 2010-12-20 | |
| US61/424,960 | 2010-12-20 | ||
| PCT/US2011/064581 WO2012087656A2 (en) | 2010-12-20 | 2011-12-13 | Hollow microspheres and method of making hollow microspheres |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EA201300432A1 EA201300432A1 (ru) | 2013-09-30 |
| EA028106B1 true EA028106B1 (ru) | 2017-10-31 |
Family
ID=45476605
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EA201300432A EA028106B1 (ru) | 2010-12-20 | 2011-12-13 | Полые микросферы и способ получения полых микросфер |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US9266764B2 (enExample) |
| EP (1) | EP2655273A2 (enExample) |
| JP (1) | JP5824069B2 (enExample) |
| KR (1) | KR20140000302A (enExample) |
| CN (1) | CN103249684B (enExample) |
| BR (1) | BR112013013237A2 (enExample) |
| EA (1) | EA028106B1 (enExample) |
| WO (1) | WO2012087656A2 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2749769C1 (ru) * | 2020-12-25 | 2021-06-16 | Автономная некоммерческая организация высшего образования «Белгородский университет кооперации, экономики и права» | Способ получения стеклянных светоотражающих сферических материалов |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10053387B2 (en) | 2013-07-18 | 2018-08-21 | 3M Innovative Properties Company | Glass microbubbles, raw product, and methods of making the same |
| CN103755146A (zh) * | 2013-12-14 | 2014-04-30 | 蚌埠玻璃工业设计研究院 | 一种固体浮体材料空心玻璃微珠及其制备方法 |
| CN104276745B (zh) * | 2014-10-30 | 2022-09-09 | 中国建材国际工程集团有限公司 | 空心玻璃微珠的强化方法 |
| US9809493B2 (en) * | 2015-04-27 | 2017-11-07 | Ford Global Technologies, Llc | Surface treatment of glass bubbles |
| CN105036555A (zh) * | 2015-07-13 | 2015-11-11 | 安徽天堂唯高塑业科技有限公司 | 一种用于汽车车牌级反光膜的玻璃微珠及其制备方法 |
| EP3344589A1 (en) * | 2015-09-04 | 2018-07-11 | 3M Innovative Properties Company | Method of making hollow glass microspheres |
| KR101715180B1 (ko) * | 2015-10-22 | 2017-03-10 | 주식회사 케이알 | 화장품 용기 |
| EP3826969B1 (en) * | 2018-07-26 | 2024-05-22 | Basf Se | Hollow spherical glass particles |
| CN108191250A (zh) * | 2018-03-30 | 2018-06-22 | 山东德润机电设备制造有限公司 | 空心玻璃微珠及其制备方法 |
| CN111362582B (zh) * | 2020-04-09 | 2021-01-19 | 浙江大学 | 真空发泡低温泡沫玻璃材料及其制备方法和应用 |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2838881A (en) * | 1953-07-18 | 1958-06-17 | Union Des Verreries Mecaniques | Apparatus for the manufacture of glass beads |
| US3838998A (en) * | 1971-01-07 | 1974-10-01 | R Carson | Process for forming hollow glass micro-spheres from admixed high and low temperature glass formers |
| US4163637A (en) * | 1977-06-16 | 1979-08-07 | The United States Of America As Represented By The United States Department Of Energy | Method and apparatus for producing small hollow spheres |
| US4257798A (en) * | 1979-07-26 | 1981-03-24 | The United States Of America As Represented By The United States Department Of Energy | Method for introduction of gases into microspheres |
| US4391646A (en) * | 1982-02-25 | 1983-07-05 | Minnesota Mining And Manufacturing Company | Glass bubbles of increased collapse strength |
| EP0801037A1 (en) * | 1996-04-09 | 1997-10-15 | Asahi Glass Company Ltd. | Process for producing inorganic microspheres and glass microballoons |
| JP2002037636A (ja) * | 2000-07-26 | 2002-02-06 | Toshiba Eng Co Ltd | 微小中空球体の製造方法、その製造装置および廃棄物リサイクル方法 |
| US20060122049A1 (en) * | 2004-12-03 | 2006-06-08 | 3M Innovative Properties Company | Method of making glass microbubbles and raw product |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL232500A (enExample) | 1957-10-22 | |||
| US3230064A (en) | 1960-10-21 | 1966-01-18 | Standard Oil Co | Apparatus for spherulization of fusible particles |
| US3365315A (en) * | 1963-08-23 | 1968-01-23 | Minnesota Mining & Mfg | Glass bubbles prepared by reheating solid glass partiles |
| ZA831343B (en) | 1982-04-08 | 1983-11-30 | Pq Corp | Hollow microspheres with organosilicon-silicate surfaces |
| FR2566384B1 (fr) * | 1984-06-21 | 1986-09-05 | Saint Gobain Vitrage | Perfectionnements aux techniques de production de microspheres en verre |
| US4767726A (en) * | 1987-01-12 | 1988-08-30 | Minnesota Mining And Manufacturing Company | Glass microbubbles |
| US4935387A (en) * | 1988-10-24 | 1990-06-19 | Corning Incorporated | Fiber-reinforced composite comprising mica matrix or interlayer |
| EP1156021A1 (en) | 2000-05-19 | 2001-11-21 | Asahi Glass Co., Ltd. | Hollow aluminosilicate glass microspheres and process for their production |
| WO2007050062A1 (en) | 2005-10-26 | 2007-05-03 | University Of North Dakota | Methods for the production of low-density microspheres |
| GB0609409D0 (en) * | 2006-05-12 | 2006-06-21 | Ici Plc | Plaster levelling compositions |
| CN101439935B (zh) * | 2008-12-22 | 2011-04-13 | 北京航空航天大学 | 一种中空玻璃微球/铁氧体复合材料的制备方法 |
| US20110152057A1 (en) * | 2009-12-21 | 2011-06-23 | Gang Qi | Hollow microspheres |
| US8261577B2 (en) * | 2009-12-21 | 2012-09-11 | 3M Innovative Properties Company | Method for making hollow microspheres |
| EP2683668A4 (en) * | 2011-03-07 | 2015-06-03 | 3M Innovative Properties Co | HOLLOW MICROSPHERES |
-
2011
- 2011-12-13 US US13/996,182 patent/US9266764B2/en not_active Expired - Fee Related
- 2011-12-13 EP EP11808033.2A patent/EP2655273A2/en not_active Withdrawn
- 2011-12-13 CN CN201180058604.6A patent/CN103249684B/zh not_active Expired - Fee Related
- 2011-12-13 JP JP2013546204A patent/JP5824069B2/ja not_active Expired - Fee Related
- 2011-12-13 EA EA201300432A patent/EA028106B1/ru not_active IP Right Cessation
- 2011-12-13 KR KR1020137018570A patent/KR20140000302A/ko not_active Abandoned
- 2011-12-13 BR BR112013013237A patent/BR112013013237A2/pt not_active Application Discontinuation
- 2011-12-13 WO PCT/US2011/064581 patent/WO2012087656A2/en not_active Ceased
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2838881A (en) * | 1953-07-18 | 1958-06-17 | Union Des Verreries Mecaniques | Apparatus for the manufacture of glass beads |
| US3838998A (en) * | 1971-01-07 | 1974-10-01 | R Carson | Process for forming hollow glass micro-spheres from admixed high and low temperature glass formers |
| US4163637A (en) * | 1977-06-16 | 1979-08-07 | The United States Of America As Represented By The United States Department Of Energy | Method and apparatus for producing small hollow spheres |
| US4257798A (en) * | 1979-07-26 | 1981-03-24 | The United States Of America As Represented By The United States Department Of Energy | Method for introduction of gases into microspheres |
| US4391646A (en) * | 1982-02-25 | 1983-07-05 | Minnesota Mining And Manufacturing Company | Glass bubbles of increased collapse strength |
| EP0801037A1 (en) * | 1996-04-09 | 1997-10-15 | Asahi Glass Company Ltd. | Process for producing inorganic microspheres and glass microballoons |
| JP2002037636A (ja) * | 2000-07-26 | 2002-02-06 | Toshiba Eng Co Ltd | 微小中空球体の製造方法、その製造装置および廃棄物リサイクル方法 |
| US20060122049A1 (en) * | 2004-12-03 | 2006-06-08 | 3M Innovative Properties Company | Method of making glass microbubbles and raw product |
Non-Patent Citations (2)
| Title |
|---|
| BUDOV V. V.: "HOLLOW GLASS MICROSPHERES. ÖUSE, PROPERTIES, AND TECHNOLOGY (REVIEW).", GLASS AND CERAMICS., SPRINGER, NEW YORK, NY., US, vol. 51., no. 07/08., 1 July 1994 (1994-07-01), US, pages 230 - 235., XP000496884, ISSN: 0361-7610, DOI: 10.1007/BF00680655 * |
| K. SODEYAMA ; Y. SAKKA ; Y. KAMINO ; H. SEKI: "Preparation of fine expanded perlite", JOURNAL OF MATERIALS SCIENCE, KLUWER ACADEMIC PUBLISHERS, BO, vol. 34, no. 10, 1 May 1999 (1999-05-01), Bo, pages 2461 - 2468, XP019209350, ISSN: 1573-4803, DOI: 10.1023/A:1004579120164 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2749769C1 (ru) * | 2020-12-25 | 2021-06-16 | Автономная некоммерческая организация высшего образования «Белгородский университет кооперации, экономики и права» | Способ получения стеклянных светоотражающих сферических материалов |
Also Published As
| Publication number | Publication date |
|---|---|
| JP5824069B2 (ja) | 2015-11-25 |
| JP2014501693A (ja) | 2014-01-23 |
| CN103249684B (zh) | 2016-03-30 |
| CN103249684A (zh) | 2013-08-14 |
| EP2655273A2 (en) | 2013-10-30 |
| KR20140000302A (ko) | 2014-01-02 |
| EA201300432A1 (ru) | 2013-09-30 |
| US20130291590A1 (en) | 2013-11-07 |
| BR112013013237A2 (pt) | 2016-09-06 |
| WO2012087656A3 (en) | 2012-11-15 |
| US9266764B2 (en) | 2016-02-23 |
| WO2012087656A2 (en) | 2012-06-28 |
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