DK138655C - - Google Patents

Info

Publication number
DK138655C
DK138655C DK188175A DK188175A DK138655C DK 138655 C DK138655 C DK 138655C DK 188175 A DK188175 A DK 188175A DK 188175 A DK188175 A DK 188175A DK 138655 C DK138655 C DK 138655C
Authority
DK
Denmark
Application number
DK188175A
Other languages
Danish (da)
Other versions
DK138655B (da
DK188175A (nl
Inventor
A Hershman
Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Co filed Critical Monsanto Co
Publication of DK188175A publication Critical patent/DK188175A/da
Publication of DK138655B publication Critical patent/DK138655B/da
Application granted granted Critical
Publication of DK138655C publication Critical patent/DK138655C/da

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
    • C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DK188175AA 1974-05-01 1975-04-30 Fremgangsmåde til fremstilling af N-phosphonomethyl-glycin. DK138655B (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US05/465,976 US3969398A (en) 1974-05-01 1974-05-01 Process for producing N-phosphonomethyl glycine
KR7500924A KR790000297B1 (en) 1974-05-01 1975-04-30 Process for producing n-phosphono methyl gylcine

Publications (3)

Publication Number Publication Date
DK188175A DK188175A (nl) 1975-11-02
DK138655B DK138655B (da) 1978-10-09
DK138655C true DK138655C (nl) 1979-02-26

Family

ID=26625851

Family Applications (1)

Application Number Title Priority Date Filing Date
DK188175AA DK138655B (da) 1974-05-01 1975-04-30 Fremgangsmåde til fremstilling af N-phosphonomethyl-glycin.

Country Status (27)

Country Link
US (1) US3969398A (nl)
JP (1) JPS5330690B2 (nl)
KR (1) KR790000297B1 (nl)
AR (1) AR215840A1 (nl)
AT (1) AT336637B (nl)
BE (1) BE828599A (nl)
BG (1) BG26398A3 (nl)
BR (1) BR7502651A (nl)
CA (1) CA1030157A (nl)
CH (1) CH613210A5 (nl)
CS (1) CS179938B2 (nl)
DD (1) DD119241A5 (nl)
DE (1) DE2519388C3 (nl)
DK (1) DK138655B (nl)
EG (1) EG11700A (nl)
ES (1) ES437154A1 (nl)
FR (1) FR2269533B1 (nl)
GB (1) GB1467778A (nl)
IE (1) IE41118B1 (nl)
IT (1) IT1037766B (nl)
MY (1) MY7800280A (nl)
NL (1) NL161763C (nl)
PH (1) PH12324A (nl)
RO (1) RO70907A (nl)
SE (1) SE427752B (nl)
YU (1) YU40117B (nl)
ZA (1) ZA752792B (nl)

Families Citing this family (93)

* Cited by examiner, † Cited by third party
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US4100275A (en) * 1975-01-27 1978-07-11 Hoffmann-La Roche Inc. Compositions having antibiotic properties
US4127649A (en) * 1975-01-27 1978-11-28 Hoffmann-La Roche Inc. Compositions having antibiotic properties
IL48835A (en) * 1975-01-27 1979-05-31 Sparamedica Ag Amino acyl and peptidyl derivatives of phophonic acids, their preparation and pharmaceutical compositions containingthem
US4134972A (en) * 1976-07-21 1979-01-16 Hoffmann-La Roche Inc. Compositions having antibiotic properties
MX4703E (es) * 1976-12-20 1982-08-04 Monsanto Co Procedimiento mejorado para la preparacion de mono y disales de n-fosfonometilglicina
HU184168B (en) * 1979-05-11 1984-07-30 Mta Koezponti Kemiai Kutato In Process for producing n-bracket-phosphono-methyl-bracket closed-glycine
US4454043A (en) * 1980-11-17 1984-06-12 Monsanto Company Column switching procedure
IL65187A (en) * 1982-03-08 1985-03-31 Geshuri Lab Ltd N-phosphonomethylglycine derivatives,processes for their preparation and herbicidal compositions containing them
IL66824A0 (en) * 1982-06-25 1982-12-31 Geshuri Lab Ltd Process for producing n-phosphonomethylglycine derivatives and herbicidal compounds and compositions prepared thereby
US4442041A (en) * 1982-06-30 1984-04-10 Stauffer Chemical Company Method for preparation of N-phosphonomethylglycine
IL68716A (en) * 1983-05-17 1987-03-31 Geshuri Lab Ltd Process for producing n-phosphonomethylglycine
US4654429A (en) * 1983-12-02 1987-03-31 Monsanto Company Process for the preparation of a glyphosate product
US4617415A (en) * 1983-12-02 1986-10-14 Monsanto Company α-Substituted N-phosphonomethyliminodiacetic acid
US4624937A (en) * 1984-05-10 1986-11-25 Monsanto Company Process for removing surface oxides from activated carbon catalyst
US5068404A (en) * 1984-12-28 1991-11-26 Monsanto Company Thermal dealkylation of N-alkyl N-phosphonomethylglycine
US5874612A (en) * 1984-12-28 1999-02-23 Baysdon; Sherrol L. Process for the preparation of glyphosate and glyphosate derivatives
US4579689A (en) * 1985-02-11 1986-04-01 Monsanto Company Oxidation with coated catalyst
US4582650A (en) * 1985-02-11 1986-04-15 Monsanto Company Oxidation with encapsulated co-catalyst
US4696772A (en) * 1985-02-28 1987-09-29 Monsanto Company Amine oxidation using carbon catalyst having oxides removed from surface
DE3532344A1 (de) * 1985-09-11 1987-03-19 Hoechst Ag Verfahren zur herstellung von n-phosphonomethylglycin
US4684483A (en) * 1985-09-23 1987-08-04 Monsanto Company Preparation of N-substituted amino acids
US4657705A (en) * 1985-09-23 1987-04-14 Monsanto Company Process for the preparation of N-substituted aminomethylphosphonic acids
US4694082A (en) * 1985-09-23 1987-09-15 Monsanto Company Compound 1,4-diisopropyl-2,5-diketopiperazine
US4740608A (en) * 1985-10-09 1988-04-26 Monsanto Company (Phosphonomethyl)trifluoromethyl sulfonates
US4853159A (en) * 1987-10-26 1989-08-01 Monsanto Company Process for producing N-phosphonomethylglycine
US4898972A (en) * 1988-09-26 1990-02-06 Monsanto Company Process for producing N-phosphonomethylglycine
US4965403A (en) * 1988-11-07 1990-10-23 Monsanto Company Oxidation/dealkylation process
US4937376A (en) * 1989-05-25 1990-06-26 Monsanto Company Process for producing N-phosphonomethylglycine
US4952723A (en) * 1989-07-31 1990-08-28 Monsanto Company Process for producing N-phosphonomethylglycine
US5095140A (en) * 1990-06-25 1992-03-10 Monsanto Company Peroxide process for producing N-phosphonomethylglycine
US5312973A (en) * 1993-03-25 1994-05-17 Finchimica S.P.A. Process for producing n-phosphono-methyl-imino-diacetic acid
GB9410524D0 (en) * 1993-06-21 1994-07-13 Zeneca Ltd Manufacture of n- phosphonomethylglycine and its salts
SI9400449A (en) * 1994-12-20 1996-06-30 Pinus D D Process for preparing N-phosphonomethyl glycin
DE19500121A1 (de) * 1995-01-04 1996-07-11 Bayer Ag Verfahren zur Herstellung von N-Phosphonomethylglycin
TW322481B (nl) * 1995-03-07 1997-12-11 Sankyo Co
AU699417B2 (en) * 1995-03-14 1998-12-03 Monsanto Company Treatment of a formaldehyde-containing waste stream
US6365772B1 (en) 1995-05-30 2002-04-02 Hampshire Chemical Corp. Facile synthesis of phosphonomethylglycine from phosphonomethyliminodiacetic acid
US6054608A (en) 1997-05-05 2000-04-25 Monsanto Company Method for preparing formylphosphonic acid
WO1999041260A1 (en) * 1998-02-12 1999-08-19 Monsanto Company Process for making glyphosate by oxidizing n-substituted glyphosates
US6232494B1 (en) * 1998-02-12 2001-05-15 Monsanto Company Process for the preparation of N-(phosphonomethyl)glycine by oxidizing N-substituted N-(phosphonomethyl)glycine
US6417133B1 (en) 1998-02-25 2002-07-09 Monsanto Technology Llc Deeply reduced oxidation catalyst and its use for catalyzing liquid phase oxidation reactions
ES2200509T3 (es) 1998-03-09 2004-03-01 Monsanto Technology Llc Mezclas para el control de las malas hierbas en cultivos de soja tolerantes a glifosato.
US5962729A (en) * 1998-05-14 1999-10-05 Calgon Carbon Corporation Method for the manufacture of N-phosphonomethylglycine from N-phosphonomethyliminodiacetic acid using a catalytic carbon
US5942643A (en) * 1998-05-14 1999-08-24 Calgon Carbon Corporation Method for the manufacture of N-phosphonomethylglycine from N-phosphonomethyliminodiacetic acid using a low temperature catalytic carbon
IES980552A2 (en) 1998-07-09 1999-08-11 Agritech Chemical Ltd Improved process for preparing N-phosphonomethyl iminodiacetic acid
WO2000009520A1 (en) * 1998-08-12 2000-02-24 Monsanto Company Continuous process for the preparation of n-(phosphonomethyl) iminodiacetic acid
BR9907000A (pt) * 1998-09-08 2000-09-26 Hampshire Chemical Corp Sìntese de ácido fosfonometiliminodiacético com efluente reduzido
US6194604B1 (en) 1998-12-10 2001-02-27 Monsanto Company Process for producing phosphorous acid
AU6826400A (en) 1999-07-23 2001-02-13 Basf Aktiengesellschaft Method of producing glyphosate or a salt thereof
EP1242433B1 (en) 1999-12-21 2004-06-02 Monsanto Technology LLC Use of a supplemental promoter in conjunction with a carbon-supported, noble-metal-containing catalyst in liquid phase oxidation reactions
DE10007702A1 (de) * 2000-02-19 2001-08-23 Sueddeutsche Kalkstickstoff Verfahren zur Herstellung von N-(Phosphonomethyl)glycin
US6274760B1 (en) 2000-03-14 2001-08-14 Monsanto Co. Preparation of formylphosphonic acid from tertiary aminomethylphosphonic acid N-oxides
US6376708B1 (en) * 2000-04-11 2002-04-23 Monsanto Technology Llc Process and catalyst for dehydrogenating primary alcohols to make carboxylic acid salts
CN100354256C (zh) * 2000-05-15 2007-12-12 孟山都技术有限责任公司 以单乙醇胺为原料制备亚氨基二乙酸化合物
US6927304B2 (en) 2000-05-22 2005-08-09 Monsanto Technology Llc De-oxygenation treatment for noble metal on carbon catalysts used in liquid phase oxidation reactions
CN101311183B (zh) * 2000-05-22 2011-08-31 孟山都技术有限责任公司 制备n-(膦酰基甲基)甘氨酸化合物的反应系统
CN102250141B (zh) * 2000-05-22 2014-10-01 孟山都技术有限责任公司 制备n－(膦酰基甲基)甘氨酸化合物的反应系统
US6441223B1 (en) 2000-11-30 2002-08-27 Monsanto Technology Llc Method of making phosphorus-containing compounds and products thereof
WO2002095373A1 (en) 2001-05-22 2002-11-28 Monsanto Technology Llc Use of infrared spectroscopy for on-line process control and endpoint detection
DE10130136A1 (de) * 2001-06-22 2003-01-02 Basf Ag Verfahren zur Gewinnung von N-Phosphonomethylglycin
MX244781B (es) 2001-10-18 2007-04-03 Monsanto Technology Llc Procedimiento y catalizador para la deshidrogenacion de alcoholes primarios en la elaboracion de sales de acido carboxilico.
AU2003215241B2 (en) * 2002-02-14 2008-07-31 Monsanto Technology Llc Oxidation catalyst and process for its preparation and process for oxidation using it
US7390920B2 (en) * 2002-02-14 2008-06-24 Monsanto Technology Llc Oxidation catalyst and process
US7932419B2 (en) 2003-08-14 2011-04-26 Monsanto Technology Llc Transition metal-containing catalysts and processes for their preparation and use as oxidation and dehydrogenation catalysts
US6921834B2 (en) * 2002-05-22 2005-07-26 Dow Agrosciences Llc Continuous process for preparing N-phosphonomethyl glycine
JP4202047B2 (ja) * 2002-05-24 2008-12-24 富士通株式会社 ヘッド位置制御方法及びデイスク記憶装置
US6956005B2 (en) * 2002-06-28 2005-10-18 Monsanto Technology Llc Use of tellurium in carbon-supported, noble metal-containing catalysts for liquid phase oxidation reactions
MXPA06003149A (es) * 2003-09-17 2006-06-05 Monsanto Technology Llc Procedimiento para la recuperacion de un producto cristalino de una solucion.
FR2865468B1 (fr) * 2004-01-22 2006-04-28 Ceca Sa Charbon actif a resistance mecanique amelioree, ses utilisations, notamment comme support de catalyseur.
AR048411A1 (es) 2004-03-30 2006-04-26 Monsanto Technology Llc Metodos para controlar patogenos de plantas que utilizan n-fosfonometilglicina
CN100372857C (zh) * 2004-05-12 2008-03-05 江苏好收成韦恩农药化工有限公司 N-膦酰基甲基甘氨酸的生产方法
US7893004B2 (en) * 2004-09-06 2011-02-22 Japan Envirochemicals, Ltd. Oxidation reaction catalyst and process for producing a compound using the same
AR051926A1 (es) * 2004-09-15 2007-02-21 Monsanto Technology Llc Catalizadores de oxidacion, procedimientos de preparacion de dichos catalizadores y proceso para la elaboracion de n-( fosfonometil)glicina o una sal de la misma
AR054096A1 (es) * 2004-11-12 2007-06-06 Monsanto Technology Llc Recuperacion de metales nobles de corrientes de proceso acuosas y proceso de preparacion de n-(fosfonometil)-glicina
BRPI0608355B1 (pt) * 2005-02-17 2016-05-24 Monsanto Technology Llc processo para oxidação de ácido n-(fosfonometil) iminodiacético ou seu sal e catalisador de oxidação
BRPI0609260B1 (pt) 2005-03-04 2020-11-03 Monsanto Technology Llc composição de glifosato herbicida útil para matar ou controlar o crescimento de ervas daninhas em um campo contendo uma cultura de plantas transgênicas de algodão tolerantes ao glifosato
EP1989749A2 (en) * 2006-02-17 2008-11-12 Monsanto Technology, LLC Transition metal-containing catalysts and processes for their preparation and use as fuel cell catalysts
CN100460408C (zh) * 2007-01-26 2009-02-11 捷马化工股份有限公司 资源再利用的催化氧化制备草甘膦方法
US7771494B2 (en) * 2007-01-31 2010-08-10 Monsanto Technology Llc Process for selective removal of water and impurities from N-(phosphonomethyl)glycine
US8252953B2 (en) 2008-05-01 2012-08-28 Monsanto Technology Llc Metal utilization in supported, metal-containing catalysts
CN101337978B (zh) * 2008-05-13 2011-06-29 浙江新安化工集团股份有限公司 一种利用富氧气体催化氧化双甘膦制取草甘膦的方法
CN101481387B (zh) * 2008-11-27 2012-02-01 浙江新安化工集团股份有限公司 一种催化氧化合成草甘膦的制备方法
CN101508701B (zh) * 2008-12-10 2012-09-05 上海泰禾(集团)有限公司 一种活性碳作催化剂氧气氧化双甘膦制备草甘膦的方法
US8669396B2 (en) 2009-05-18 2014-03-11 Monsanto Technology Llc Recovery of phosphorus values and salt impurities from aqueous waste streams
CN101781332B (zh) * 2010-03-02 2012-10-24 广西壮族自治区化工研究院 活性炭催化空气氧化双甘膦制备草甘膦的方法
CN102241703B (zh) * 2011-05-07 2014-05-07 安徽国星生物化学有限公司 一种改进的双甘膦制备草甘膦的方法
WO2014012987A1 (en) 2012-07-17 2014-01-23 Straitmark Holding Ag Method for the synthesis of aminoalkylenephosphonic acid
US10364262B2 (en) 2012-07-17 2019-07-30 Monsanto Technology Llc Method for the synthesis of N-phosphonomethyliminodiacetic acid
RU2674023C9 (ru) 2012-07-17 2019-01-24 МОНСАНТО ТЕКНОЛОДЖИ ЭлЭлСи Способ синтеза n-(фосфонометил)глицина
BR112015000995B1 (pt) 2012-07-17 2020-04-28 Monsanto Technology Llc método para a síntese de n-(fosfonometil)glicina ou um de seus derivados selecionados a partir do grupo que consiste em seus sais, seus ésteres de fosfonato e seus sais de éster de fosfonato
WO2014012990A1 (en) 2012-07-17 2014-01-23 Straitmark Holding Ag Method for the synthesis of alpha-aminoalkylenephosphonic acid
BR112019027682A2 (pt) 2017-06-26 2020-09-15 Monsanto Technology Llc controle de fósforo para fluxos de resíduos provenientes de processos de produção de glifosato
CN115215900A (zh) * 2022-07-01 2022-10-21 安徽东至广信农化有限公司 一种草甘膦的节能生产方法

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DE1217950B (de) * 1965-02-25 1966-06-02 Henkel & Cie Gmbh Verfahren zur Herstellung neuer Perhydrate von Aminoalkylphosphonsaeuren
DE2013371B1 (de) * 1970-03-20 1971-11-04 Joh A , Benckiser GmbH, Chemische Fabrik, 6700 Ludwigshafen Verfahren zur Herstellung von Amino methylenphosphonsauren
US3799758A (en) * 1971-08-09 1974-03-26 Monsanto Co N-phosphonomethyl-glycine phytotoxicant compositions

Also Published As

Publication number Publication date
AT336637B (de) 1977-05-10
IE41118B1 (en) 1979-10-24
BR7502651A (pt) 1976-03-16
FR2269533B1 (nl) 1978-02-24
ATA333975A (de) 1976-09-15
AR215840A1 (es) 1979-11-15
GB1467778A (en) 1977-03-23
DK138655B (da) 1978-10-09
DE2519388C3 (de) 1978-03-09
MY7800280A (en) 1978-12-31
AU8070175A (en) 1976-11-04
YU111575A (en) 1982-06-30
ZA752792B (en) 1976-04-28
PH12324A (en) 1979-01-16
SE427752B (sv) 1983-05-02
DK188175A (nl) 1975-11-02
NL161763B (nl) 1979-10-15
EG11700A (en) 1977-10-31
FR2269533A1 (nl) 1975-11-28
NL161763C (nl) 1980-03-17
BG26398A3 (bg) 1979-03-15
CA1030157A (en) 1978-04-25
JPS50160222A (nl) 1975-12-25
JPS5330690B2 (nl) 1978-08-29
YU40117B (en) 1985-08-31
IE41118L (en) 1975-11-01
NL7505071A (nl) 1975-11-04
CH613210A5 (nl) 1979-09-14
DE2519388B2 (de) 1977-07-14
DD119241A5 (nl) 1976-04-12
BE828599A (fr) 1975-10-30
ES437154A1 (es) 1977-01-16
RO70907A (ro) 1980-04-15
SE7505040L (sv) 1975-11-03
IT1037766B (it) 1979-11-20
DE2519388A1 (de) 1975-11-13
CS179938B2 (en) 1977-12-30
US3969398A (en) 1976-07-13
KR790000297B1 (en) 1979-04-23

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