DK138655B - Fremgangsmåde til fremstilling af N-phosphonomethyl-glycin. - Google Patents

Fremgangsmåde til fremstilling af N-phosphonomethyl-glycin.

Info

Publication number
DK138655B
DK138655B DK188175AA DK188175A DK138655B DK 138655 B DK138655 B DK 138655B DK 188175A A DK188175A A DK 188175AA DK 188175 A DK188175 A DK 188175A DK 138655 B DK138655 B DK 138655B
Authority
DK
Denmark
Prior art keywords
phosphonomethyl
glycine
preparation
Prior art date
Application number
DK188175AA
Other languages
Danish (da)
English (en)
Other versions
DK188175A (OSRAM
DK138655C (OSRAM
Inventor
Arnold Hershman
Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Co filed Critical Monsanto Co
Publication of DK188175A publication Critical patent/DK188175A/da
Publication of DK138655B publication Critical patent/DK138655B/da
Application granted granted Critical
Publication of DK138655C publication Critical patent/DK138655C/da

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
    • C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DK188175AA 1974-05-01 1975-04-30 Fremgangsmåde til fremstilling af N-phosphonomethyl-glycin. DK138655B (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US05/465,976 US3969398A (en) 1974-05-01 1974-05-01 Process for producing N-phosphonomethyl glycine
KR7500924A KR790000297B1 (en) 1974-05-01 1975-04-30 Process for producing n-phosphono methyl gylcine

Publications (3)

Publication Number Publication Date
DK188175A DK188175A (OSRAM) 1975-11-02
DK138655B true DK138655B (da) 1978-10-09
DK138655C DK138655C (OSRAM) 1979-02-26

Family

ID=26625851

Family Applications (1)

Application Number Title Priority Date Filing Date
DK188175AA DK138655B (da) 1974-05-01 1975-04-30 Fremgangsmåde til fremstilling af N-phosphonomethyl-glycin.

Country Status (27)

Country Link
US (1) US3969398A (OSRAM)
JP (1) JPS5330690B2 (OSRAM)
KR (1) KR790000297B1 (OSRAM)
AR (1) AR215840A1 (OSRAM)
AT (1) AT336637B (OSRAM)
BE (1) BE828599A (OSRAM)
BG (1) BG26398A3 (OSRAM)
BR (1) BR7502651A (OSRAM)
CA (1) CA1030157A (OSRAM)
CH (1) CH613210A5 (OSRAM)
CS (1) CS179938B2 (OSRAM)
DD (1) DD119241A5 (OSRAM)
DE (1) DE2519388C3 (OSRAM)
DK (1) DK138655B (OSRAM)
EG (1) EG11700A (OSRAM)
ES (1) ES437154A1 (OSRAM)
FR (1) FR2269533B1 (OSRAM)
GB (1) GB1467778A (OSRAM)
IE (1) IE41118B1 (OSRAM)
IT (1) IT1037766B (OSRAM)
MY (1) MY7800280A (OSRAM)
NL (1) NL161763C (OSRAM)
PH (1) PH12324A (OSRAM)
RO (1) RO70907A (OSRAM)
SE (1) SE427752B (OSRAM)
YU (1) YU40117B (OSRAM)
ZA (1) ZA752792B (OSRAM)

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US4134972A (en) * 1976-07-21 1979-01-16 Hoffmann-La Roche Inc. Compositions having antibiotic properties
ES465139A1 (es) * 1976-12-20 1978-10-01 Monsanto Co Un procedimiento para preparar una mono-o disal de n-fosfo- nometilglicina.
HU184168B (en) * 1979-05-11 1984-07-30 Mta Koezponti Kemiai Kutato In Process for producing n-bracket-phosphono-methyl-bracket closed-glycine
US4454043A (en) * 1980-11-17 1984-06-12 Monsanto Company Column switching procedure
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IL66824A0 (en) * 1982-06-25 1982-12-31 Geshuri Lab Ltd Process for producing n-phosphonomethylglycine derivatives and herbicidal compounds and compositions prepared thereby
US4442041A (en) * 1982-06-30 1984-04-10 Stauffer Chemical Company Method for preparation of N-phosphonomethylglycine
IL68716A (en) * 1983-05-17 1987-03-31 Geshuri Lab Ltd Process for producing n-phosphonomethylglycine
US4617415A (en) * 1983-12-02 1986-10-14 Monsanto Company α-Substituted N-phosphonomethyliminodiacetic acid
US4654429A (en) * 1983-12-02 1987-03-31 Monsanto Company Process for the preparation of a glyphosate product
US4624937A (en) * 1984-05-10 1986-11-25 Monsanto Company Process for removing surface oxides from activated carbon catalyst
US5068404A (en) * 1984-12-28 1991-11-26 Monsanto Company Thermal dealkylation of N-alkyl N-phosphonomethylglycine
US5874612A (en) * 1984-12-28 1999-02-23 Baysdon; Sherrol L. Process for the preparation of glyphosate and glyphosate derivatives
US4582650A (en) * 1985-02-11 1986-04-15 Monsanto Company Oxidation with encapsulated co-catalyst
US4579689A (en) * 1985-02-11 1986-04-01 Monsanto Company Oxidation with coated catalyst
US4696772A (en) * 1985-02-28 1987-09-29 Monsanto Company Amine oxidation using carbon catalyst having oxides removed from surface
DE3532344A1 (de) * 1985-09-11 1987-03-19 Hoechst Ag Verfahren zur herstellung von n-phosphonomethylglycin
US4694082A (en) * 1985-09-23 1987-09-15 Monsanto Company Compound 1,4-diisopropyl-2,5-diketopiperazine
US4657705A (en) * 1985-09-23 1987-04-14 Monsanto Company Process for the preparation of N-substituted aminomethylphosphonic acids
US4684483A (en) * 1985-09-23 1987-08-04 Monsanto Company Preparation of N-substituted amino acids
US4740608A (en) * 1985-10-09 1988-04-26 Monsanto Company (Phosphonomethyl)trifluoromethyl sulfonates
US4853159A (en) * 1987-10-26 1989-08-01 Monsanto Company Process for producing N-phosphonomethylglycine
US4898972A (en) * 1988-09-26 1990-02-06 Monsanto Company Process for producing N-phosphonomethylglycine
US4965403A (en) * 1988-11-07 1990-10-23 Monsanto Company Oxidation/dealkylation process
US4937376A (en) * 1989-05-25 1990-06-26 Monsanto Company Process for producing N-phosphonomethylglycine
US4952723A (en) * 1989-07-31 1990-08-28 Monsanto Company Process for producing N-phosphonomethylglycine
US5095140A (en) * 1990-06-25 1992-03-10 Monsanto Company Peroxide process for producing N-phosphonomethylglycine
US5312973A (en) * 1993-03-25 1994-05-17 Finchimica S.P.A. Process for producing n-phosphono-methyl-imino-diacetic acid
GB9410524D0 (en) * 1993-06-21 1994-07-13 Zeneca Ltd Manufacture of n- phosphonomethylglycine and its salts
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DE19500121A1 (de) * 1995-01-04 1996-07-11 Bayer Ag Verfahren zur Herstellung von N-Phosphonomethylglycin
TW322481B (OSRAM) * 1995-03-07 1997-12-11 Sankyo Co
WO1996028391A1 (en) * 1995-03-14 1996-09-19 Monsanto Company Treatment of a formaldehyde-containing waste stream
US6365772B1 (en) 1995-05-30 2002-04-02 Hampshire Chemical Corp. Facile synthesis of phosphonomethylglycine from phosphonomethyliminodiacetic acid
US6054608A (en) * 1997-05-05 2000-04-25 Monsanto Company Method for preparing formylphosphonic acid
BR9806202B1 (pt) * 1998-02-12 2009-12-01 processo para fabricação de glifosato, um sal de glifosato, ou um éster de glifosato e catalisador de oxidação.
US6232494B1 (en) 1998-02-12 2001-05-15 Monsanto Company Process for the preparation of N-(phosphonomethyl)glycine by oxidizing N-substituted N-(phosphonomethyl)glycine
US6417133B1 (en) * 1998-02-25 2002-07-09 Monsanto Technology Llc Deeply reduced oxidation catalyst and its use for catalyzing liquid phase oxidation reactions
AU754918C (en) 1998-03-09 2007-05-31 Monsanto Technology Llc Mixtures for weed control in glyphosate tolerant soybeans
US5962729A (en) * 1998-05-14 1999-10-05 Calgon Carbon Corporation Method for the manufacture of N-phosphonomethylglycine from N-phosphonomethyliminodiacetic acid using a catalytic carbon
US5942643A (en) * 1998-05-14 1999-08-24 Calgon Carbon Corporation Method for the manufacture of N-phosphonomethylglycine from N-phosphonomethyliminodiacetic acid using a low temperature catalytic carbon
IES980552A2 (en) 1998-07-09 1999-08-11 Agritech Chemical Ltd Improved process for preparing N-phosphonomethyl iminodiacetic acid
CA2339839A1 (en) 1998-08-12 2000-02-24 Monsanto Company Continuous process for the preparation of n-(phosphonomethyl) iminodiacetic acid
US6118022A (en) * 1998-09-08 2000-09-12 Hampshire Chemical Corp. Synthesis of phosphonomethyliminodiacetic acid with reduced effluent
US6194604B1 (en) 1998-12-10 2001-02-27 Monsanto Company Process for producing phosphorous acid
PL364748A1 (en) 1999-07-23 2004-12-13 Basf Aktiengesellschaft Method of producing glyphosate or a salt thereof
EP1923395A1 (en) * 1999-12-21 2008-05-21 Monsanto Technology, LLC Use of supplemental promoter in conjuction with a carbon-supported, noble-metal-containing catalyst in liquid phase oxidation reactions
DE10007702A1 (de) * 2000-02-19 2001-08-23 Sueddeutsche Kalkstickstoff Verfahren zur Herstellung von N-(Phosphonomethyl)glycin
US6274760B1 (en) 2000-03-14 2001-08-14 Monsanto Co. Preparation of formylphosphonic acid from tertiary aminomethylphosphonic acid N-oxides
US6376708B1 (en) 2000-04-11 2002-04-23 Monsanto Technology Llc Process and catalyst for dehydrogenating primary alcohols to make carboxylic acid salts
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CN100393733C (zh) * 2000-05-22 2008-06-11 孟山都技术有限责任公司 制备n-(膦酰基甲基)甘氨酸化合物的反应系统
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US6441223B1 (en) 2000-11-30 2002-08-27 Monsanto Technology Llc Method of making phosphorus-containing compounds and products thereof
WO2002095373A1 (en) 2001-05-22 2002-11-28 Monsanto Technology Llc Use of infrared spectroscopy for on-line process control and endpoint detection
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AU2002362929B2 (en) 2001-10-18 2007-08-09 Monsanto Technology Llc Process and catalyst for dehydrogenating primary alcohols to make carboxylic acid salts
US7390920B2 (en) * 2002-02-14 2008-06-24 Monsanto Technology Llc Oxidation catalyst and process
MX284594B (es) * 2002-02-14 2011-03-10 Monsanto Technology Llc Catalizador de oxidacion y procedimiento para su preparacion y procedimiento para oxidacion mediante el uso del mismo.
US6921834B2 (en) * 2002-05-22 2005-07-26 Dow Agrosciences Llc Continuous process for preparing N-phosphonomethyl glycine
JP4202047B2 (ja) * 2002-05-24 2008-12-24 富士通株式会社 ヘッド位置制御方法及びデイスク記憶装置
AR040319A1 (es) * 2002-06-28 2005-03-23 Monsanto Technology Llc Uso de telurio en catalizadores con contenido de metales nobles y con soporte de carbon para reacciones de oxidacion en fase liquida
BRPI0413586A (pt) 2003-08-14 2006-10-17 Monsanto Technology Llc catalisadores contendo metal de transição e processo para a preparação dos mesmos e uso como catalisadores de oxidação e de desidrogenação
US7179936B2 (en) * 2003-09-17 2007-02-20 Monsanto Technology Llc Process for recovering a crystalline product from solution
FR2865468B1 (fr) * 2004-01-22 2006-04-28 Ceca Sa Charbon actif a resistance mecanique amelioree, ses utilisations, notamment comme support de catalyseur.
AR048411A1 (es) 2004-03-30 2006-04-26 Monsanto Technology Llc Metodos para controlar patogenos de plantas que utilizan n-fosfonometilglicina
CN100372857C (zh) * 2004-05-12 2008-03-05 江苏好收成韦恩农药化工有限公司 N-膦酰基甲基甘氨酸的生产方法
EP1806177A4 (en) * 2004-09-06 2009-09-16 Japan Enviro Chemicals Ltd OXIDATION REACTION CATALYST AND PROCESS FOR PRODUCING COMPOUND USING THE SAME
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BRPI0608355B1 (pt) 2005-02-17 2016-05-24 Monsanto Technology Llc processo para oxidação de ácido n-(fosfonometil) iminodiacético ou seu sal e catalisador de oxidação
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CN101427406A (zh) * 2006-02-17 2009-05-06 孟山都技术公司 含过渡金属的催化剂、其制备方法及其作为燃料电池催化剂的用途
CN100460408C (zh) * 2007-01-26 2009-02-11 捷马化工股份有限公司 资源再利用的催化氧化制备草甘膦方法
US7771494B2 (en) * 2007-01-31 2010-08-10 Monsanto Technology Llc Process for selective removal of water and impurities from N-(phosphonomethyl)glycine
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CN101481387B (zh) * 2008-11-27 2012-02-01 浙江新安化工集团股份有限公司 一种催化氧化合成草甘膦的制备方法
CN101508701B (zh) * 2008-12-10 2012-09-05 上海泰禾(集团)有限公司 一种活性碳作催化剂氧气氧化双甘膦制备草甘膦的方法
CN104058495B (zh) 2009-05-18 2016-04-20 孟山都技术公司 含水废物流中磷有用成分和盐杂质的回收
CN101781332B (zh) * 2010-03-02 2012-10-24 广西壮族自治区化工研究院 活性炭催化空气氧化双甘膦制备草甘膦的方法
CN102241703B (zh) * 2011-05-07 2014-05-07 安徽国星生物化学有限公司 一种改进的双甘膦制备草甘膦的方法
RU2015103314A (ru) 2012-07-17 2016-09-10 Страйтмарк Холдинг Аг Способ синтеза N-фосфонометилиминодиуксусной кислоты
BR112015000990B1 (pt) 2012-07-17 2020-04-28 Monsanto Technology Llc Método para a síntese de um ácido aminoalquilenofosfônico ouseus ésteres fosfatos
BR112015000966B1 (pt) 2012-07-17 2020-04-28 Monsanto Technology Llc método para a síntese de n-(fosfonometil)glicina ou um de seus derivados selecionados a partir do grupo que consiste em seus sais, seus ésteres de fosfonato e seus sais de éster de fosfonato
WO2014012991A1 (en) 2012-07-17 2014-01-23 Straitmark Holding Ag Method for the synthesis of n-(phosphonomethyl)glycine
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WO2019005718A1 (en) 2017-06-26 2019-01-03 Monsanto Technology Llc PHOSPHORUS CONTROL FOR WASTE FLOWS FROM GLYPHOSATE MANUFACTURING PROCESSES
CN115215900A (zh) * 2022-07-01 2022-10-21 安徽东至广信农化有限公司 一种草甘膦的节能生产方法

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Also Published As

Publication number Publication date
SE427752B (sv) 1983-05-02
DE2519388B2 (de) 1977-07-14
ATA333975A (de) 1976-09-15
BG26398A3 (bg) 1979-03-15
IT1037766B (it) 1979-11-20
AU8070175A (en) 1976-11-04
YU111575A (en) 1982-06-30
DK188175A (OSRAM) 1975-11-02
DE2519388C3 (de) 1978-03-09
SE7505040L (sv) 1975-11-03
IE41118B1 (en) 1979-10-24
PH12324A (en) 1979-01-16
JPS5330690B2 (OSRAM) 1978-08-29
AT336637B (de) 1977-05-10
FR2269533A1 (OSRAM) 1975-11-28
CH613210A5 (OSRAM) 1979-09-14
DK138655C (OSRAM) 1979-02-26
NL7505071A (nl) 1975-11-04
ES437154A1 (es) 1977-01-16
ZA752792B (en) 1976-04-28
DE2519388A1 (de) 1975-11-13
KR790000297B1 (en) 1979-04-23
DD119241A5 (OSRAM) 1976-04-12
CA1030157A (en) 1978-04-25
BR7502651A (pt) 1976-03-16
US3969398A (en) 1976-07-13
MY7800280A (en) 1978-12-31
JPS50160222A (OSRAM) 1975-12-25
AR215840A1 (es) 1979-11-15
EG11700A (en) 1977-10-31
IE41118L (en) 1975-11-01
NL161763B (nl) 1979-10-15
FR2269533B1 (OSRAM) 1978-02-24
YU40117B (en) 1985-08-31
RO70907A (ro) 1980-04-15
GB1467778A (en) 1977-03-23
NL161763C (nl) 1980-03-17
BE828599A (fr) 1975-10-30
CS179938B2 (en) 1977-12-30

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