DE98321C - - Google Patents
Info
- Publication number
- DE98321C DE98321C DENDAT98321D DE98321DA DE98321C DE 98321 C DE98321 C DE 98321C DE NDAT98321 D DENDAT98321 D DE NDAT98321D DE 98321D A DE98321D A DE 98321DA DE 98321 C DE98321 C DE 98321C
- Authority
- DE
- Germany
- Prior art keywords
- acid
- benzaldehyde
- dyes
- ethylbenzylaniline
- acids
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000002253 acid Substances 0.000 claims description 15
- 239000000975 dye Substances 0.000 claims description 11
- HUMNYLRZRPPJDN-UHFFFAOYSA-N Benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 claims description 9
- HSZCJVZRHXPCIA-UHFFFAOYSA-N N-benzyl-N-ethylaniline Chemical compound C=1C=CC=CC=1N(CC)CC1=CC=CC=C1 HSZCJVZRHXPCIA-UHFFFAOYSA-N 0.000 claims description 4
- 150000007513 acids Chemical class 0.000 claims description 4
- 229940095076 benzaldehyde Drugs 0.000 claims description 4
- LXZGVFCKZRHKMU-UHFFFAOYSA-N N-benzyl-N-methylaniline Chemical compound C=1C=CC=CC=1N(C)CC1=CC=CC=C1 LXZGVFCKZRHKMU-UHFFFAOYSA-N 0.000 claims description 2
- 230000003647 oxidation Effects 0.000 claims 2
- 238000007254 oxidation reaction Methods 0.000 claims 2
- GGSUCNLOZRCGPQ-UHFFFAOYSA-N Diethylaniline Chemical compound CCN(CC)C1=CC=CC=C1 GGSUCNLOZRCGPQ-UHFFFAOYSA-N 0.000 claims 1
- JLTDJTHDQAWBAV-UHFFFAOYSA-N Dimethylaniline Chemical compound CN(C)C1=CC=CC=C1 JLTDJTHDQAWBAV-UHFFFAOYSA-N 0.000 claims 1
- QFRIIGBAHKSVIU-UHFFFAOYSA-N N-benzyl-2-methylaniline Chemical compound CC1=CC=CC=C1NCC1=CC=CC=C1 QFRIIGBAHKSVIU-UHFFFAOYSA-N 0.000 claims 1
- 150000004982 aromatic amines Chemical class 0.000 claims 1
- SLXZZXJPFRYIKN-UHFFFAOYSA-N benzyl-(2-ethylphenyl)sulfamic acid Chemical compound CCC1=CC=CC=C1N(S(O)(=O)=O)CC1=CC=CC=C1 SLXZZXJPFRYIKN-UHFFFAOYSA-N 0.000 claims 1
- JNACZTITPIYADC-UHFFFAOYSA-N benzyl-(2-methylphenyl)sulfamic acid Chemical compound CC1=CC=CC=C1N(S(O)(=O)=O)CC1=CC=CC=C1 JNACZTITPIYADC-UHFFFAOYSA-N 0.000 claims 1
- 238000009833 condensation Methods 0.000 claims 1
- 230000005494 condensation Effects 0.000 claims 1
- 230000000875 corresponding Effects 0.000 claims 1
- VFCNQNZNPKRXIT-UHFFFAOYSA-N malachite green cation Chemical class C1=CC(N(C)C)=CC=C1C(C=1C=CC=CC=1)=C1C=CC(=[N+](C)C)C=C1 VFCNQNZNPKRXIT-UHFFFAOYSA-N 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- -1 monoethyl-otoluidine Chemical compound 0.000 claims 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- HXCKBNWJXWNEMZ-UHFFFAOYSA-N 1,4-dichlorocyclohexa-2,4-diene-1-carbaldehyde Chemical compound ClC1=CCC(Cl)(C=O)C=C1 HXCKBNWJXWNEMZ-UHFFFAOYSA-N 0.000 description 2
- GEHJYWRUCIMESM-UHFFFAOYSA-L Sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- GDQLHKHFHWLXES-UHFFFAOYSA-N ClC1=CC=CC(Cl)(C=O)C1 Chemical compound ClC1=CC=CC(Cl)(C=O)C1 GDQLHKHFHWLXES-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- JOVOSQBPPZZESK-UHFFFAOYSA-N amino(phenyl)azanium;chloride Chemical compound Cl.NNC1=CC=CC=C1 JOVOSQBPPZZESK-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 125000001309 chloro group Chemical group Cl* 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- YADSGOSSYOOKMP-UHFFFAOYSA-N dioxolead Chemical compound O=[Pb]=O YADSGOSSYOOKMP-UHFFFAOYSA-N 0.000 description 1
- 230000036545 exercise Effects 0.000 description 1
- 239000001046 green dye Substances 0.000 description 1
- 150000007857 hydrazones Chemical class 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical group C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- DWAQJAXMDSEUJJ-UHFFFAOYSA-M sodium bisulfite Chemical compound [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 description 1
- 229940001607 sodium bisulfite Drugs 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 235000002639 sodium chloride Nutrition 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 235000010267 sodium hydrogen sulphite Nutrition 0.000 description 1
- 235000010265 sodium sulphite Nutrition 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N sulfonic acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- 238000005987 sulfurization reaction Methods 0.000 description 1
- 239000002966 varnish Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B11/00—Diaryl- or thriarylmethane dyes
- C09B11/04—Diaryl- or thriarylmethane dyes derived from triarylmethanes, i.e. central C-atom is substituted by amino, cyano, alkyl
- C09B11/10—Amino derivatives of triarylmethanes
- C09B11/12—Amino derivatives of triarylmethanes without any OH group bound to an aryl nucleus
- C09B11/14—Preparation from aromatic aldehydes, aromatic carboxylic acids or derivatives thereof and aromatic amines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE98321C true DE98321C (zh) |
Family
ID=369296
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT98321D Active DE98321C (zh) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE98321C (zh) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0175226A2 (de) * | 1984-09-17 | 1986-03-26 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von Alkali- und Erdalkalisalzen der Benzaldehyd-2,4-disulfonsäure |
| US4715995A (en) * | 1984-09-17 | 1987-12-29 | Hoechst Aktiengesellschaft | Process for the preparation of alkali metal and alkaline earth salts of benzaldehyde-2,4-disulfonic acid |
-
0
- DE DENDAT98321D patent/DE98321C/de active Active
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0175226A2 (de) * | 1984-09-17 | 1986-03-26 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von Alkali- und Erdalkalisalzen der Benzaldehyd-2,4-disulfonsäure |
| EP0175226A3 (en) * | 1984-09-17 | 1986-05-14 | Hoechst Aktiengesellschaft | Process for the preparation of salts of alkaline or earth-alkaline metals of benzaldehyde-2,4-disulfonic acid |
| US4710322A (en) * | 1984-09-17 | 1987-12-01 | Hoechst Aktiengesellschaft | Process for the preparation of alkali metal and alkaline earth salts of benzaldehyde-2,4-di-sulfonic acid |
| US4715995A (en) * | 1984-09-17 | 1987-12-29 | Hoechst Aktiengesellschaft | Process for the preparation of alkali metal and alkaline earth salts of benzaldehyde-2,4-disulfonic acid |
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