DE804511T1 - Neue farbstoffe und farbstoffmodifizierungsmittel - Google Patents

Neue farbstoffe und farbstoffmodifizierungsmittel

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Publication number
DE804511T1
DE804511T1 DE0804511T DE96902719T DE804511T1 DE 804511 T1 DE804511 T1 DE 804511T1 DE 0804511 T DE0804511 T DE 0804511T DE 96902719 T DE96902719 T DE 96902719T DE 804511 T1 DE804511 T1 DE 804511T1
Authority
DE
Germany
Prior art keywords
group
aryl
alkyl
stabilizing
heterocycloalkyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DE0804511T
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English (en)
Inventor
John Macdonald
Ronald Nohr
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kimberly Clark Corp
Original Assignee
Kimberly Clark Corp
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Filing date
Publication date
Application filed by Kimberly Clark Corp filed Critical Kimberly Clark Corp
Publication of DE804511T1 publication Critical patent/DE804511T1/de
Pending legal-status Critical Current

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Claims (1)

  1. KIMBERLY-CLARK WORLDWIDE, INC.
    PATENTANSPRÜCHE
    Stabilisierungszusammensetzung umfassend eine Verbindung mit der Formel:
    ^XR,
    R,
    wonn
    Ri Wasserstoff, eine Alkyl-, Alkenyl-, Cycloalkyl-, Heterocycloalkyl-, heterocyclische, Aryl-, substituierte Aryl- oder eine Heteroarylgruppe bedeutet;
    R2 Wasserstoff, eine Alkyl-, Alkenyl-, Cycloalkyl-, Heterocycloalkyl-, heterocyclische, Aryl-, substituierte Aryl- oder eine Heteroarylgruppe bedeutet;
    R3 Wasserstoff, eine Alkyl-, Alkenyl-, Cycloalkyl-, Heterocycloalkyl-, Aryl-, substituierte Aryl- oder eine Heteroarylgruppe bedeutet; und
    R4 Wasserstoff, eine Alkyl-, Alkenyl-, Cycloalkyl-, Heterocycloalkyl-, heterocyclische, Aryl-, substituierte Aryl- oder eine Heteroarylgruppe bedeutet; und
    worin R1, R2 oder R4 eine Aryl- oder substituierte Arylgruppe bedeutet.
    2. Stabilisierungszusammensetzung nach Anspruch 1, worin die Verbindung die folgende Formel aufweist:
    ff
    R4-C-CH=CH-R2
    worin, wenn R4 eine Arylgruppe ist, R2 Wasserstoff, eine Alkyl-, Aryl-, heterocyclische oder Phenylgruppe ist, wobei die Phenylgruppe gegebenenfalls mit einer Alkyl-, Halogen-, Amino- oder Thiolgruppe substituiert ist; und
    worin, wenn R2 eine Arylgruppe ist, R4 ein Wasserstoff, eine Alkyl-, Aryl-, heterocyclische oder Phenylgruppe ist, wobei die Phenylgruppe gegebenenfalls mit einer Alkyl-, Halogen-, Amino- oder Thiolgruppe substituiert ist.
    3. Stabilisierungszusammensetzung nach Anspruch 1, worin die Zusammensetzung femer ein Färbemittel umfaßt.
    4. Stabilisierungszusammensetzung nach Anspruch 1, worin die Zusammensetzung femer eine Moleküleinschlußverbindung umfaßt.
    5. Stabilisierungszusammensetzung nach Anspruch 4, worin die Moleküleinschiußverbindung an die Verbindung kovalent gebunden ist.
    6. Stabilisierungszusammensetzung nach Anspruch 1, worin die Verbindung die folgende Formel aufweist:
    HO(CH2)2—O·
    DE/EP
    oder
    H=CH—C-CH3
    Stabilisierungszusammensetzung nach Anspruch 1, worin R1 oder R2 oder R4 eine Arylgruppe bedeutet, an die eine Carbonsäuregruppe, eine Aldehydgruppe, eine Aminogaippe, eine Halogenalkylgruppe, eine Hydroxylgruppe, oder eine Thioalkylgruppe gebunden ist.
    Stabilisierungszusammensetzung nach Anspruch 7, worin die Verbindung die folgende Formel aufweist:
    HOOC
    HOOC
    H=CH-C-CH3
    oder
    0OH
    9. Stabilisierungszusammensetzung nach Anspruch 1, welche ferner ein wellenlängenselektives Sensibilisierungsmittel umfaßt.
    10. Stabilisierungszusammensetzung nach Anspruch 9, worin die Verbindung an das wellenlängenselektive Sensibiiisierungsmittel kovalent gebunden ist.
    11. Stabilisierungszusammensetzung nach Anspruch 10, worin die Verbindung, die an das wellenlängenselektive Sensibilisierungsmittel kovalent gebunden ist, durch die folgende Formel dargestellt ist:
    O ,
    &Pgr; //
    N-CH2-C-O(CHa)2O-\
    12. Verfahren zum Lichtstabilisieren eines Färbemittels umfassend das Assoziieren des Färbemittels mit einem Stabilisierungsmolekül , wobei das Stabilisierungsmolekül durch die Formel dargestellt ist:
    wonn
    R1 Wasserstoff, eine Alkyl-, Alkenyl-, Cycloalkyl-, Heterocycloalkyl-, heterocyclische, Aryl-, substituierte Aryl- oder eine Heteroarylgruppe bedeutet;
    R2 Wasserstoff, eine Alkyl-, Alkenyl-, Cycloalkyl-, Heterocycloalkyl-, heterocyclische, Aryl-, substituierte Aryl- oder eine Heteroarylgruppe bedeutet;
    R3 Wasserstoff, eine Alkyl-, Alkenyl-, Cycloalkyl-, Heterocycloalkyl-, Aryl-, substituierte Aryl- oder eine Heteroarylgruppe bedeutet; und
    R4 Wasserstoff, eine Alkyl-, Alkenyl-, Cycloalkyl-, Heterocycloalkyl-, heterocyclische, Aryl-, substituierte Aryl- oder eine Heteroarylgruppe bedeutet; und
    worin Ri, R2 oder R4 eine Aryl- oder substituierte Arylgruppe bedeutet.
    13. Verfahren nach Anspruch 12, worin das Stabilisierungsmolekül durch die folgende Formel dargestellt ist:
    R1-C-CH=CH-R2
    worin, wenn R4 eine Arylgruppe ist, R2 Wasserstoff, eine Alkyl-, Aryl-, heterocyclische oder Phenyigruppe ist, wobei die Phenyigruppe gegebenenfalls mit einer Alkyl-, Halogen-, Amino- oder Thiolgruppe substituiert ist; und
    worin, wenn R2 eine Arylgruppe ist, R4 Wasserstoff, eine Alkyl-, Aryl-, heterocyclische oder Phenyigruppe ist, wobei die Phenyigruppe gegebenenfalls mit einer Alkyl-, Halogen-, Amino- oder Thiolgruppe substituiert ist.
    14. Verfahren nach Anspruch 12, worin das Stabilisierungsmolekül femer mit einer Moleküleinschlußverbindung assoziiert ist.
    15. Verfahren nach Anspruch 14, worin die Moleküleinschlußverbindung an das Stabilisierungsmolekül kovalent gebunden ist.
    16. Verfahren nach Anspruch 12, worin das Stabilisierungsmolekül durch die folgende Formel dargestellt ist:
    HO(CH2)2—O—«
    H=CH-C
    oder
    17. Verfahren nach Anspruch 12, worin das Stabilisierungsmolekül ferner mit einem wellenlängenselektiven Sensibilisienjngsmittel assoziiert ist.
    18. Verfahren nach Anspruch 17, worin das Stabilisierungsmolekül an das wellenlängenselektive Sensibilisienjngsmittel kovalent gebunden ist.
    19. Verfahren nach Anspruch 18, worin das Stabilisierungsmolekül, das an das wellenlängenselektive Sensibilisienjngsmittel kovalent gebunden ist, durch die folgende Formel dargestellt ist:
    N-CH2-C-O(CH2J2O.
    20. Verfahren nach Anspruch 12, worin Ri oder R2 oder R4 eine Arylgruppe bedeutet, an die eine Carbonsäuregruppe, eine Aldehydgruppe, eine Aminogruppe, eine Halogenalkylgruppe, eine Hydroxylgruppe oder eine Thioalkylgruppe gebunden ist.
    21. Verfahren nach Anspruch 20, worin das Stabilisierungsmolekül durch die folgende Formel dargestellt ist:
    HOOC-YQ)-CH=CH—C
    HOOC
    H—CH C—CH3
    0OH
    22. Verfahren zum Dehydratisieren eines tertiären Alkohols, umfassend das Umsetzen des tertiären Alkohols in einem nichtwäßrigen nichtpolaren Lösungsmittel in Gegenwart einer wirksamen Menge eines Übergangsmetallsalzes, so daß der tertiäre Alkohol dehydratisiert wird, worin der tertiäre Alkohol durch die Formel dargestellt ist:
    R3-C-C-OH
    R1 Wasserstoff, eine Alkyl-, Alkenyl-, Cycloalkyl-, Heterocycloalkyl-, Aryl- oder eine Heteroarylgruppe bedeutet;
    R2 Wasserstoff, eine Alkyl-, Alkenyl-, Cycloalkyl-, Heterocycloalkyl-, Aryl- oder eine Heteroarylgruppe bedeutet;
    R3 eine Aryl- oder substituierte Arylgruppe bedeutet.
    23. Verfahren nach Anspruch 22, worin das nichtpolare Lösungsmittel aus der Gruppe ausgewählt ist, die aus Xylol, Benzol, Toluol, Cumol, Mesitylen, p-Cymol, Butylbenzol, Styrol und Divinylbenzol besteht.
    24. Verfahren nach Anspruch 23, worin das nichtpolare Lösungsmittel p-Xylol ist.
    25. Verfahren nach Anspruch 22, worin das Übergangsmetallsalz ZnCI2 ist.
    26. Verfahren nach Anspruch 22, worin die Reaktion bei einer Temperatur zwischen ungefähr 80eC und 150X durchgeführt wird.
    27. Verfahren nach Anspruch 22, worin der tertiäre Alkohol 2-[p-(2-Methyllactoyl)-phenoxy]ethyl-1,3-dioxo-2-isoindolinacetat ist.
DE0804511T 1995-01-17 1996-01-16 Neue farbstoffe und farbstoffmodifizierungsmittel Pending DE804511T1 (de)

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