DE69807224T2 - Lineare acetale und ketale als duftstoffvorläufer - Google Patents
Lineare acetale und ketale als duftstoffvorläuferInfo
- Publication number
- DE69807224T2 DE69807224T2 DE69807224T DE69807224T DE69807224T2 DE 69807224 T2 DE69807224 T2 DE 69807224T2 DE 69807224 T DE69807224 T DE 69807224T DE 69807224 T DE69807224 T DE 69807224T DE 69807224 T2 DE69807224 T2 DE 69807224T2
- Authority
- DE
- Germany
- Prior art keywords
- ketals
- perfume
- performance
- linear acetals
- acetals
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 150000001241 acetals Chemical class 0.000 title 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/04—Detergent materials or soaps characterised by their shape or physical properties combined with or containing other objects
- C11D17/041—Compositions releasably affixed on a substrate or incorporated into a dispensing means
- C11D17/047—Arrangements specially adapted for dry cleaning or laundry dryer related applications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/70—Fixation, conservation, or encapsulation of flavouring agents
- A23L27/75—Fixation, conservation, or encapsulation of flavouring agents the flavouring agents being bound to a host by chemical, electrical or like forces, e.g. use of precursors
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C43/00—Ethers; Compounds having groups, groups or groups
- C07C43/30—Compounds having groups
- C07C43/303—Compounds having groups having acetal carbon atoms bound to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C43/00—Ethers; Compounds having groups, groups or groups
- C07C43/30—Compounds having groups
- C07C43/305—Compounds having groups having acetal carbon atoms as rings members or bound to carbon atoms of rings other than six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C47/00—Compounds having —CHO groups
- C07C47/02—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen
- C07C47/198—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen containing ether groups, groups, groups, or groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
- C07F9/09—Esters of phosphoric acids
- C07F9/091—Esters of phosphoric acids with hydroxyalkyl compounds with further substituents on alkyl
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3723—Polyamines or polyalkyleneimines
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
- C11D3/502—Protected perfumes
- C11D3/507—Compounds releasing perfumes by thermal or chemical activation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Emergency Medicine (AREA)
- Nutrition Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Detergent Compositions (AREA)
- Fats And Perfumes (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US5110497P | 1997-06-27 | 1997-06-27 | |
PCT/US1998/013281 WO1999000347A1 (en) | 1997-06-27 | 1998-06-26 | Pro-fragrance linear acetals and ketals |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69807224D1 DE69807224D1 (de) | 2002-09-19 |
DE69807224T2 true DE69807224T2 (de) | 2003-04-17 |
Family
ID=21969370
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69807224T Expired - Lifetime DE69807224T2 (de) | 1997-06-27 | 1998-06-26 | Lineare acetale und ketale als duftstoffvorläufer |
Country Status (10)
Country | Link |
---|---|
US (3) | US6316397B1 (de) |
EP (1) | EP0991615B1 (de) |
JP (1) | JP2002510323A (de) |
CN (1) | CN1268107A (de) |
AR (1) | AR016292A1 (de) |
BR (1) | BR9810630B1 (de) |
CA (1) | CA2295114A1 (de) |
DE (1) | DE69807224T2 (de) |
ES (1) | ES2182333T3 (de) |
WO (1) | WO1999000347A1 (de) |
Families Citing this family (56)
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JP2002542382A (ja) * | 1999-04-20 | 2002-12-10 | ザ、プロクター、エンド、ギャンブル、カンパニー | 前芳香剤 |
AU2001264965A1 (en) * | 2000-05-26 | 2001-12-11 | Exitexchange Corporation | Post-session internet advertising system |
US7503127B2 (en) * | 2002-04-22 | 2009-03-17 | The Procter And Gamble Company | Electrically charged volatile material delivery method |
US7066412B2 (en) * | 2002-05-28 | 2006-06-27 | Johnsondiversey, Inc. | Apparatus, methods, and compositions for adding fragrance to laundry |
US7109157B2 (en) * | 2003-02-27 | 2006-09-19 | Lawnie Taylor | Methods and equipment for removing stains from fabrics using a composition comprising hydroxide and hypochlorite |
US8592361B2 (en) * | 2002-11-25 | 2013-11-26 | Colgate-Palmolive Company | Functional fragrance precursor |
AU2003271194A1 (en) | 2003-10-09 | 2005-04-21 | Daewoong Co., Ltd. | Process for purifying human thrombopoietin with high content of sialic acid |
US20050192205A1 (en) * | 2004-02-27 | 2005-09-01 | Toan Trinh | Multiple use fabric conditioning article with replacement indicium |
US7723285B2 (en) * | 2004-07-20 | 2010-05-25 | Michigan Molecular Institute | Beneficial agent delivery systems |
US7569529B2 (en) * | 2005-09-07 | 2009-08-04 | The Procter & Gamble Company | Method of using fabric care compositions to achieve a synergistic odor benefit |
DE102005058339A1 (de) * | 2005-12-06 | 2007-06-28 | Henkel Kgaa | Stabilitätsverbesserung flüssiger hypochlorithaltiger Wasch- und Reinigungsmittel |
DE102005058642B3 (de) * | 2005-12-07 | 2007-07-26 | Henkel Kgaa | Erhöhung der Stabilität flüssiger hypochlorithaltiger Wasch- und Reinigungsmittel |
DE102005062008B3 (de) * | 2005-12-22 | 2007-08-30 | Henkel Kgaa | Geruchsreduktion hypochlorithaltiger Mittel |
DE102005063065A1 (de) * | 2005-12-29 | 2007-07-12 | Henkel Kgaa | Korrosionsinhibierung flüssiger hypochlorithaltiger Reinigungsmittel |
DE102005063177A1 (de) | 2005-12-30 | 2007-07-05 | Henkel Kgaa | Erhöhung der Stabilität hypochlorihaltiger Waschmittel |
EP1857436A1 (de) * | 2006-05-19 | 2007-11-21 | Kao Corporation, S.A. | Vorläuferverbindungen für Riechstoffe |
US20070275866A1 (en) * | 2006-05-23 | 2007-11-29 | Robert Richard Dykstra | Perfume delivery systems for consumer goods |
WO2008134212A1 (en) * | 2007-04-27 | 2008-11-06 | The Dial Company | Methods for treating fabric in a dryer |
EP1992606A1 (de) * | 2007-05-15 | 2008-11-19 | Symrise GmbH & Co. KG | Alkenacetale und ihre Verwendung als Riechstoffe |
US20090312223A1 (en) * | 2008-06-13 | 2009-12-17 | Conopco, Inc., D/B/A Unilever | Method of Controlling Structure and Rheology of Low Active Liquid Cleansers by Selecting Perfume Components |
US20090312224A1 (en) * | 2008-06-13 | 2009-12-17 | Conopco, Inc., D/B/A Unilever | Method of Reducing Viscosity of Concentrated Liquid Cleansers by Selection of Perfume Components |
US20110150803A1 (en) * | 2008-08-22 | 2011-06-23 | Jean-Marie Lehn | Equilibrated dynamic mixtures containing stabilized hemiacetals for the controlled release of active alcohols |
JP5567029B2 (ja) | 2008-12-01 | 2014-08-06 | ザ プロクター アンド ギャンブル カンパニー | 香料システム |
US8754028B2 (en) * | 2008-12-16 | 2014-06-17 | The Procter & Gamble Company | Perfume systems |
EP2270124A1 (de) | 2009-06-30 | 2011-01-05 | The Procter & Gamble Company | Bleichzusammensetzungen mit Parfümliefersystem |
EP3434764A3 (de) | 2009-12-09 | 2019-04-03 | The Procter & Gamble Company | Stoff- und heimpflegeprodukte |
EP2512527A1 (de) | 2009-12-17 | 2012-10-24 | The Procter & Gamble Company | Auffrischungszusammensetzungen mit geruchsbindenden polymeren und geruchsbekämpfenden bestandteilen |
CA2900812C (en) | 2010-06-22 | 2017-07-04 | Johan Smets | Perfume systems |
MX2012015201A (es) | 2010-06-22 | 2013-01-24 | Procter & Gamble | Sistemas de perfumeria. |
WO2012003319A2 (en) | 2010-07-02 | 2012-01-05 | The Procter & Gamble Company | Filaments comprising an active agent nonwoven webs and methods for making same |
MX345026B (es) | 2010-07-02 | 2017-01-12 | Procter & Gamble | Material de trama y método para su elaboración. |
JP5770280B2 (ja) | 2010-07-02 | 2015-08-26 | ザ プロクター アンド ギャンブルカンパニー | 非香料系活性剤を含むフィラメントの不織布ウェブ及びその作製方法 |
EP2723841B1 (de) | 2011-06-23 | 2017-01-04 | The Procter and Gamble Company | Duftstoffsysteme |
US20140141126A1 (en) | 2011-06-29 | 2014-05-22 | Solae Llc | Baked food compositions comprising soy whey proteins that have been isolated from processing streams |
FR2985272B1 (fr) | 2012-01-04 | 2021-10-22 | Procter & Gamble | Structures fibreuses contenant des actifs et ayant des regions multiples aux caracteristiques distinctes |
CN106968050B (zh) | 2012-01-04 | 2019-08-27 | 宝洁公司 | 具有多个区域的含活性物质纤维结构 |
RU2605065C2 (ru) | 2012-01-04 | 2016-12-20 | Дзе Проктер Энд Гэмбл Компани | Волокнистые структуры, содержащие частицы. |
EP3572572B1 (de) | 2013-12-09 | 2021-01-20 | The Procter & Gamble Company | Verfahren zum drucken einer grafik auf eine faserstruktur |
EP3094615A4 (de) | 2014-01-13 | 2017-11-08 | P2 Science, Inc. | Säuren aus terpen und ester sowie verfahren zur herstellung und verwendung davon |
US20150238394A1 (en) * | 2014-02-27 | 2015-08-27 | Kimberly-Clark Worldwide, Inc. | Triggerable Compositions For Two-Stage, Controlled Release of Proactive Chemistry Using Aldehydes |
WO2015191706A1 (en) * | 2014-06-10 | 2015-12-17 | P2 Science, Inc. | Terpene-derived compounds and methods for preparing and using same |
US10071944B2 (en) | 2014-06-20 | 2018-09-11 | P2 Science, Inc. | Film ozonolysis in a tubular or multitubular reactor |
KR20180069915A (ko) * | 2015-11-25 | 2018-06-25 | 킴벌리-클라크 월드와이드, 인크. | 물- 또는 산-유발 방향제 방출 기능성 단량체 및 중합체 시스템 |
CN108697591B (zh) | 2016-02-18 | 2022-06-17 | 国际香料和香精公司 | 聚脲胶囊组合物 |
WO2017223220A1 (en) | 2016-06-21 | 2017-12-28 | P2 Science, Inc. | Flow-through reactors for the continuous quenching of peroxide mixtures and methods comprising the same |
WO2018053289A1 (en) | 2016-09-16 | 2018-03-22 | P2 Science, Inc. | Uses of vanadium to oxidize aldehydes and ozonides |
ES2950434T3 (es) | 2016-09-16 | 2023-10-10 | Int Flavors & Fragrances Inc | Composiciones de microcápsula estabilizadas con agentes de control de la viscosidad |
US11697905B2 (en) | 2017-01-27 | 2023-07-11 | The Procter & Gamble Company | Active agent-containing articles that exhibit consumer acceptable article in-use properties |
US11697906B2 (en) | 2017-01-27 | 2023-07-11 | The Procter & Gamble Company | Active agent-containing articles and product-shipping assemblies for containing the same |
US11697904B2 (en) | 2017-01-27 | 2023-07-11 | The Procter & Gamble Company | Active agent-containing articles that exhibit consumer acceptable article in-use properties |
EP3573721B1 (de) | 2017-01-27 | 2021-08-11 | The Procter & Gamble Company | Wirkstoffhaltige artikel die für den verbraucher akzeptable eigenschaften aufweisen |
CN107325273B (zh) * | 2017-06-22 | 2019-09-20 | 温州大学 | 高分子聚合物及其制备方法和在酸敏感型两亲性纳米胶束的应用 |
WO2020082007A1 (en) | 2018-10-19 | 2020-04-23 | P2 Science, Inc. | New methods for disproportionation quenching of ozonides |
EP4069811A1 (de) | 2019-12-05 | 2022-10-12 | The Procter & Gamble Company | Verfahren zur herstellung einer reinigungszusammensetzung |
US20210171866A1 (en) | 2019-12-05 | 2021-06-10 | The Procter & Gamble Company | Cleaning composition |
IT202200003008A1 (it) | 2022-02-17 | 2023-08-17 | Andrea Macchia | Sistema pulente per la pulitura delle superfici dipinte di arte pubblica vandalizzate |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2206883A (en) * | 1936-03-07 | 1940-07-09 | Ig Farbenindustrie Ag | Aromatic-aliphatic acetals |
GB1365062A (en) | 1970-07-01 | 1974-08-29 | Bush Boake Allen Ltd | Compounded perfumery compositions containing organic titanates or zirconates |
DE2132898A1 (de) * | 1971-07-02 | 1973-01-18 | Henkel & Cie Gmbh | Schwachschaeumendes wasch-, reinigungsund enthaertungsmittel |
CH628516A5 (en) | 1977-07-25 | 1982-03-15 | Bush Boake Allen Ltd | Perfumery compositions |
US4424146A (en) | 1981-10-07 | 1984-01-03 | Fritzsche Dodge & Olcott Inc. | Acetaldehyde ethyl 6-dihydrolinalyl acetal perfume compositions |
JPS58208211A (ja) | 1982-05-28 | 1983-12-03 | Chisso Corp | 徐分解性香料を使用した芳香剤 |
JPH0644927B2 (ja) | 1987-03-14 | 1994-06-15 | 日本油脂株式会社 | 徐放性活性成分放出剤 |
GB8816209D0 (en) | 1988-07-07 | 1988-08-10 | Bush Boake Allen Ltd | Perfumery compositions |
DE4110973A1 (de) | 1991-04-05 | 1992-10-08 | Haarmann & Reimer Gmbh | Mittel mit physiologischem kuehleffekt und fuer diese mittel geeignete wirksame verbindungen |
US5232612A (en) | 1991-08-28 | 1993-08-03 | The Procter & Gamble Company | Solid, particulate fabric softener with protected, dryer-activated, cyclodextrin/perfume complex |
JPH05230496A (ja) | 1992-02-24 | 1993-09-07 | Nippon Fine Chem Co Ltd | 調合香料及び該調合香料を含有する芳香性組成物 |
US5378468A (en) | 1992-09-22 | 1995-01-03 | The Mennen Company | Composition containing body activated fragrance for contacting the skin and method of use |
DE69428978T2 (de) | 1993-08-09 | 2002-07-18 | Firmenich & Cie | Parfümierungsverfahren von geweben |
WO1995016660A1 (fr) | 1993-12-17 | 1995-06-22 | Nippon Zeon Co., Ltd. | Compose d'acetal de cis-3-hexenal cis-3-hexenyle, son procede de production, aromatisant, exhausteur de gout, et composition parfumee le contenant |
US5506201A (en) | 1994-04-29 | 1996-04-09 | International Flavors & Fragrances Inc. | Formulation of a fat surfactant vehicle containing a fragrance |
US5500138A (en) * | 1994-10-20 | 1996-03-19 | The Procter & Gamble Company | Fabric softener compositions with improved environmental impact |
US6576247B1 (en) | 1994-11-10 | 2003-06-10 | Kanebo Ltd. And T. Hasegawa Co. Ltd. | Sustained-release aromatic and method of detecting micro-organism by using the same |
WO1997034986A1 (en) | 1996-03-22 | 1997-09-25 | The Procter & Gamble Company | Detergent compositions containing fragrance precursors and the fragrance precursors themselves |
US5968893A (en) * | 1996-05-03 | 1999-10-19 | The Procter & Gamble Company | Laundry detergent compositions and methods for providing soil release to cotton fabric |
WO1998006803A1 (en) * | 1996-08-12 | 1998-02-19 | The Procter & Gamble Company | Rinse added fabric softening compositions and method of use for the delivery of fragrance precursors |
ZA9711272B (en) | 1996-12-19 | 1998-06-23 | Procter & Gamble | Dryer-activated fabric conditioning and antistatic compositions with improved perfume longevity. |
-
1998
- 1998-06-26 CA CA002295114A patent/CA2295114A1/en not_active Abandoned
- 1998-06-26 AR ARP980103108A patent/AR016292A1/es active IP Right Grant
- 1998-06-26 BR BRPI9810630-9A patent/BR9810630B1/pt not_active IP Right Cessation
- 1998-06-26 US US09/445,325 patent/US6316397B1/en not_active Expired - Fee Related
- 1998-06-26 CN CN98808558A patent/CN1268107A/zh active Pending
- 1998-06-26 JP JP50787399A patent/JP2002510323A/ja not_active Ceased
- 1998-06-26 EP EP98931620A patent/EP0991615B1/de not_active Expired - Lifetime
- 1998-06-26 DE DE69807224T patent/DE69807224T2/de not_active Expired - Lifetime
- 1998-06-26 ES ES98931620T patent/ES2182333T3/es not_active Expired - Lifetime
- 1998-06-26 WO PCT/US1998/013281 patent/WO1999000347A1/en active IP Right Grant
-
2001
- 2001-07-27 US US09/917,542 patent/US6395695B1/en not_active Expired - Fee Related
-
2002
- 2002-05-09 US US10/142,039 patent/US6677491B2/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
ES2182333T3 (es) | 2003-03-01 |
DE69807224D1 (de) | 2002-09-19 |
WO1999000347A1 (en) | 1999-01-07 |
US6677491B2 (en) | 2004-01-13 |
CN1268107A (zh) | 2000-09-27 |
EP0991615B1 (de) | 2002-08-14 |
US6316397B1 (en) | 2001-11-13 |
AR016292A1 (es) | 2001-07-04 |
CA2295114A1 (en) | 1999-01-07 |
US6395695B1 (en) | 2002-05-28 |
BR9810630A (pt) | 2000-10-03 |
US20030032565A1 (en) | 2003-02-13 |
EP0991615A1 (de) | 2000-04-12 |
BR9810630B1 (pt) | 2010-10-05 |
JP2002510323A (ja) | 2002-04-02 |
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