DE69535355D1 - Verfahren zur trennung von optischen isomeren - Google Patents

Verfahren zur trennung von optischen isomeren

Info

Publication number
DE69535355D1
DE69535355D1 DE69535355T DE69535355T DE69535355D1 DE 69535355 D1 DE69535355 D1 DE 69535355D1 DE 69535355 T DE69535355 T DE 69535355T DE 69535355 T DE69535355 T DE 69535355T DE 69535355 D1 DE69535355 D1 DE 69535355D1
Authority
DE
Germany
Prior art keywords
optical isomers
separating optical
separating
isomers
optical
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69535355T
Other languages
English (en)
Other versions
DE69535355T2 (de
Inventor
Hirokazu Ikeda
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Daicel Corp
Original Assignee
Daicel Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Daicel Chemical Industries Ltd filed Critical Daicel Chemical Industries Ltd
Application granted granted Critical
Publication of DE69535355D1 publication Critical patent/DE69535355D1/de
Publication of DE69535355T2 publication Critical patent/DE69535355T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B01D15/185—Simulated moving beds characterized by the components to be separated
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B57/00—Separation of optically-active compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2215/00—Separating processes involving the treatment of liquids with adsorbents
    • B01D2215/02—Separating processes involving the treatment of liquids with adsorbents with moving adsorbents
    • B01D2215/023—Simulated moving beds
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
    • G01N2030/8809—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
    • G01N2030/8877—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample optical isomers
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G01N30/6004—Construction of the column end pieces

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
DE69535355T 1994-04-20 1995-04-19 Verfahren zur trennung von optischen isomeren Expired - Lifetime DE69535355T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP8147994 1994-04-20
JP6081479A JPH07285889A (ja) 1994-04-20 1994-04-20 光学異性体の分離方法
PCT/JP1995/000768 WO1995029142A1 (fr) 1994-04-20 1995-04-19 Procede de separation d'isomeres optiques

Publications (2)

Publication Number Publication Date
DE69535355D1 true DE69535355D1 (de) 2007-02-15
DE69535355T2 DE69535355T2 (de) 2007-08-16

Family

ID=13747547

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69535355T Expired - Lifetime DE69535355T2 (de) 1994-04-20 1995-04-19 Verfahren zur trennung von optischen isomeren

Country Status (5)

Country Link
US (1) US6533936B1 (de)
EP (1) EP0706982B1 (de)
JP (1) JPH07285889A (de)
DE (1) DE69535355T2 (de)
WO (1) WO1995029142A1 (de)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10249191A (ja) * 1997-03-17 1998-09-22 Daicel Chem Ind Ltd 分離剤
US6107492A (en) * 1998-05-08 2000-08-22 Ucb, S.A. Process for the preparation of levetiracetam
US6124473A (en) * 1998-05-08 2000-09-26 Ucb, S.A. Process for preparing (s)- and (R)-α-ethyl-2-oxo-1-pyrrolidineacetamide
WO2002088048A1 (fr) * 2001-04-27 2002-11-07 Daicel Chemical Industries, Ltd. Agent de separation comprenant un derive de polysaccharide a structure polycyclique
US7199241B1 (en) 2001-05-29 2007-04-03 Ucb, S.A. Process for preparing (S) and (R)-2-[4-(4-chlorobenzhydryl)piperazin-1-yl]-ethoxyacetamide
US6977301B1 (en) 2001-05-29 2005-12-20 Ucb, S.A. Process for preparing (S) and (R)—2-[4-(4-chlorobenzhydryl)piperazin-1-yl]-ethoxyacetamide
SE0102369D0 (sv) * 2001-07-03 2001-07-03 Monocell Ab New method
EP1623978B1 (de) * 2003-04-24 2010-08-11 Daicel Chemical Industries, Ltd. Verfahren zur herstellung von (3r,5s,6e)-7-[2-cyclopropyl-4-(4-fluorphenyl)chinolin-3-yl] -3,5-dihydroxy-6-heptensäureethylester
US20060086667A1 (en) * 2004-09-13 2006-04-27 Cephalon, Inc., U.S. Corporation Methods for the separation of enantiomeric sulfinylacetamides
JP5224264B2 (ja) * 2006-05-09 2013-07-03 株式会社ダイセル キトサン誘導体の製造方法
CN101535345B (zh) 2006-09-04 2013-09-11 大赛璐化学工业株式会社 多糖衍生物和含有该多糖衍生物的光学异构体用分离剂
WO2008088830A2 (en) * 2007-01-16 2008-07-24 Evolved Nanomaterial Sciences, Inc. Chiral separating agents with active support
US7618539B2 (en) 2008-03-31 2009-11-17 Ampac Fine Chemicals Llc Simulated moving bed chromatography for strongly retained compounds
US7906046B2 (en) * 2008-04-04 2011-03-15 Panduit Corp. Antioxidant joint compound and method for forming an electrical connection
CN102311504B (zh) 2010-07-09 2017-05-10 株式会社大赛璐 多糖衍生物及其制备方法以及分离剂

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60216842A (ja) * 1984-04-11 1985-10-30 Daicel Chem Ind Ltd 多糖誘導体よりなる分離剤
JPS60226831A (ja) * 1984-04-02 1985-11-12 Daicel Chem Ind Ltd 分離剤
JPS60226832A (ja) * 1984-04-02 1985-11-12 Daicel Chem Ind Ltd 多糖の脂肪族エステルを含む分離剤
US4861872A (en) * 1986-03-20 1989-08-29 Daicel Chemical Industries, Ltd. Alkyl-phenylcarbamate derivative of polysaccharide
US5066793A (en) 1987-10-26 1991-11-19 Ciba-Geigy Corporation Finely particulate cellulose esters of aromatic or aromatic-aliphatic carboxylic acids, process for their preparation, and the use thereof
JPH03100459A (ja) * 1989-09-14 1991-04-25 Sumitomo Heavy Ind Ltd 擬似移動床式クロマト分離法
JP2834225B2 (ja) * 1989-10-20 1998-12-09 オルガノ株式会社 擬似移動層式クロマト分離装置
JP2925753B2 (ja) * 1990-02-23 1999-07-28 ダイセル化学工業株式会社 光学異性体の分離方法
JP2828770B2 (ja) * 1990-10-23 1998-11-25 ダイセル化学工業株式会社 多糖のフェニルアルキルカルバメート誘導体及び分離剤
US5354852A (en) * 1991-03-04 1994-10-11 Daicel Chemical Industries, Ltd. Polysaccharide derivative, process for producing the same, and separating agent
ATE144909T1 (de) * 1991-03-14 1996-11-15 Bayer Ag Verfahren zur trennung von enantiomeren an chiralen trennphasen mit hilfe eines kontinuierlichen gegenstrom- chromatographieverfahrens
JP3010816B2 (ja) * 1991-08-22 2000-02-21 ダイセル化学工業株式会社 光学分割における光学異性体と溶媒との回収方法、溶媒の循環使用方法、および光学異性体の再利用方法
US5498752A (en) * 1991-08-22 1996-03-12 Daicel Chemical Industries, Ltd. Process for recovering optical isomers and solvent, process for using solvent by circulation and process for reusing optical isomers in optical resolution
EP0577079B1 (de) * 1992-06-30 1999-12-01 Daicel Chemical Industries, Ltd. Trennsystem mit simuliertem Fliessbett
US5518625A (en) * 1995-02-13 1996-05-21 Uop Chiral separations by simulated moving bed chromatography operating at low k' values

Also Published As

Publication number Publication date
EP0706982A1 (de) 1996-04-17
EP0706982B1 (de) 2007-01-03
WO1995029142A1 (fr) 1995-11-02
US6533936B1 (en) 2003-03-18
DE69535355T2 (de) 2007-08-16
JPH07285889A (ja) 1995-10-31
EP0706982A4 (de) 1997-05-02

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Legal Events

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