DE602006011286D1 - Herstellungsverfahren für caprolactam - Google Patents
Herstellungsverfahren für caprolactamInfo
- Publication number
- DE602006011286D1 DE602006011286D1 DE602006011286T DE602006011286T DE602006011286D1 DE 602006011286 D1 DE602006011286 D1 DE 602006011286D1 DE 602006011286 T DE602006011286 T DE 602006011286T DE 602006011286 T DE602006011286 T DE 602006011286T DE 602006011286 D1 DE602006011286 D1 DE 602006011286D1
- Authority
- DE
- Germany
- Prior art keywords
- reaction
- caprolactam
- manufacturing process
- reaction zones
- aminocapronitrile
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000006243 chemical reaction Methods 0.000 abstract 5
- KBMSFJFLSXLIDJ-UHFFFAOYSA-N 6-aminohexanenitrile Chemical compound NCCCCCC#N KBMSFJFLSXLIDJ-UHFFFAOYSA-N 0.000 abstract 1
- 125000005219 aminonitrile group Chemical group 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 150000003951 lactams Chemical class 0.000 abstract 1
- 238000007363 ring formation reaction Methods 0.000 abstract 1
- 239000012808 vapor phase Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/02—Preparation of lactams
- C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
- C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
- C07D223/06—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D223/08—Oxygen atoms
- C07D223/10—Oxygen atoms attached in position 2
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Cable Accessories (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
- Sealing Battery Cases Or Jackets (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/083,728 US7060820B1 (en) | 2005-03-18 | 2005-03-18 | Process for making caprolactam |
| PCT/US2006/009232 WO2006101871A1 (en) | 2005-03-18 | 2006-03-15 | Process for making caprolactam |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE602006011286D1 true DE602006011286D1 (de) | 2010-02-04 |
Family
ID=36576434
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE602006011286T Active DE602006011286D1 (de) | 2005-03-18 | 2006-03-15 | Herstellungsverfahren für caprolactam |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US7060820B1 (enExample) |
| EP (1) | EP1858843B1 (enExample) |
| JP (1) | JP5302672B2 (enExample) |
| KR (1) | KR101141912B1 (enExample) |
| CN (1) | CN101142179B (enExample) |
| AT (1) | ATE452878T1 (enExample) |
| BR (1) | BRPI0609846A2 (enExample) |
| CA (1) | CA2600770A1 (enExample) |
| CZ (1) | CZ2007622A3 (enExample) |
| DE (1) | DE602006011286D1 (enExample) |
| MX (1) | MX2007011228A (enExample) |
| MY (1) | MY142413A (enExample) |
| PL (1) | PL383762A1 (enExample) |
| SK (1) | SK51082007A3 (enExample) |
| TW (1) | TW200643010A (enExample) |
| WO (1) | WO2006101871A1 (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8167490B2 (en) | 2009-04-22 | 2012-05-01 | Reynolds Consumer Products Inc. | Multilayer stretchy drawstring |
| FR2944791B1 (fr) * | 2009-04-27 | 2012-02-10 | Rhodia Operations | Procede de preparation de lactames. |
| CN102952075A (zh) * | 2011-08-30 | 2013-03-06 | 中国科学院大连化学物理研究所 | 一种己内酰胺的合成方法 |
| CN102399363B (zh) * | 2011-10-11 | 2013-11-06 | 上海焦耳蜡业有限公司 | 一种利用回收尼龙生产热熔胶的方法 |
| CN113087641B (zh) * | 2021-04-14 | 2023-10-24 | 江苏扬农化工集团有限公司 | 一种由环己酮肟制备6-氨基己腈的方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2301964A (en) | 1941-09-12 | 1942-11-17 | Du Pont | Method of preparing lactams |
| US2357484A (en) | 1941-09-12 | 1944-09-05 | Du Pont | Process for producing compounds containing an n-substituted amide group |
| US4625023A (en) * | 1985-09-03 | 1986-11-25 | Allied Corporation | Selective conversion of aliphatic and aromatic aminonitriles and/or dinitriles into lactams |
| FR2751962B1 (fr) * | 1996-08-02 | 1998-09-11 | Rhone Poulenc Fibres | Procede de purification de lactames |
| FR2755132B1 (fr) | 1996-10-24 | 1998-11-27 | Rhone Poulenc Fibres | Procede de traitement de lactames |
| DE19753301A1 (de) * | 1997-12-01 | 1999-06-02 | Basf Ag | Verfahren zur Herstellung von Lactamen |
| FR2781393B1 (fr) * | 1998-07-22 | 2000-08-25 | Rhone Poulenc Fibres | Procede de regeneration d'un catalyseur d'hydrolyse cyclisante d'un aminonitrile en lactame et utilisation du catalyseur regenere pour la fabrication de lactames |
| US6686465B2 (en) * | 2000-05-03 | 2004-02-03 | Basf Aktiengesellschaft | Preparation of cyclic lactams |
| JP2004298768A (ja) * | 2003-03-31 | 2004-10-28 | Jgc Corp | 気相反応装置の運転方法 |
| US6716977B1 (en) * | 2003-06-17 | 2004-04-06 | E. I. Du Pont De Nemours And Company | Method for making caprolactam from impure ACN wherein ammonia and water are removed from crude caprolactam in a simple separation step and then THA is removed from the resulting caprolactam melt |
-
2005
- 2005-03-18 US US11/083,728 patent/US7060820B1/en not_active Expired - Fee Related
-
2006
- 2006-03-15 CN CN2006800087225A patent/CN101142179B/zh not_active Expired - Fee Related
- 2006-03-15 SK SK5108-2007A patent/SK51082007A3/sk unknown
- 2006-03-15 BR BRPI0609846-0A patent/BRPI0609846A2/pt not_active IP Right Cessation
- 2006-03-15 CA CA002600770A patent/CA2600770A1/en not_active Abandoned
- 2006-03-15 DE DE602006011286T patent/DE602006011286D1/de active Active
- 2006-03-15 PL PL383762A patent/PL383762A1/pl unknown
- 2006-03-15 CZ CZ20070622A patent/CZ2007622A3/cs unknown
- 2006-03-15 EP EP06738306A patent/EP1858843B1/en not_active Not-in-force
- 2006-03-15 JP JP2008501986A patent/JP5302672B2/ja not_active Expired - Fee Related
- 2006-03-15 MX MX2007011228A patent/MX2007011228A/es active IP Right Grant
- 2006-03-15 AT AT06738306T patent/ATE452878T1/de not_active IP Right Cessation
- 2006-03-15 WO PCT/US2006/009232 patent/WO2006101871A1/en not_active Ceased
- 2006-03-15 KR KR1020077021278A patent/KR101141912B1/ko not_active Expired - Fee Related
- 2006-03-17 TW TW095109264A patent/TW200643010A/zh unknown
- 2006-03-17 MY MYPI20061186A patent/MY142413A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| MY142413A (en) | 2010-11-30 |
| TW200643010A (en) | 2006-12-16 |
| EP1858843B1 (en) | 2009-12-23 |
| SK51082007A3 (sk) | 2008-10-07 |
| CN101142179A (zh) | 2008-03-12 |
| MX2007011228A (es) | 2007-10-17 |
| WO2006101871A1 (en) | 2006-09-28 |
| EP1858843A1 (en) | 2007-11-28 |
| JP5302672B2 (ja) | 2013-10-02 |
| BRPI0609846A2 (pt) | 2010-05-04 |
| CN101142179B (zh) | 2012-05-30 |
| KR20080016530A (ko) | 2008-02-21 |
| PL383762A1 (pl) | 2008-05-12 |
| US7060820B1 (en) | 2006-06-13 |
| CA2600770A1 (en) | 2006-09-28 |
| CZ2007622A3 (cs) | 2008-07-02 |
| ATE452878T1 (de) | 2010-01-15 |
| KR101141912B1 (ko) | 2012-05-03 |
| JP2008533160A (ja) | 2008-08-21 |
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| TH129011A (th) | กระบวนการสำหรับการผลิตคาโปแลคแตม (Caprolactam) และ สารอนุพันธ์ของสิ่งนั้นจากน้ำหมักที่ประกอบด้วย ไดแอมโมเนียม อะดิเพต (diammonium adipate) โมโนแอมโมเนียม อะดิเพต (monoammonium adipate) และ/หรือ กรดอะดิพิก (adipic acid) |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition |