DE3900629A1 - Verfahren zur reinigung von rohphenol - Google Patents
Verfahren zur reinigung von rohphenolInfo
- Publication number
- DE3900629A1 DE3900629A1 DE19893900629 DE3900629A DE3900629A1 DE 3900629 A1 DE3900629 A1 DE 3900629A1 DE 19893900629 DE19893900629 DE 19893900629 DE 3900629 A DE3900629 A DE 3900629A DE 3900629 A1 DE3900629 A1 DE 3900629A1
- Authority
- DE
- Germany
- Prior art keywords
- isophorone
- phenol
- phenols
- purification
- fractions
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 title claims abstract description 13
- 238000000034 method Methods 0.000 title claims abstract description 10
- 238000000746 purification Methods 0.000 title claims abstract 3
- HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 claims abstract description 22
- 150000002989 phenols Chemical class 0.000 claims abstract description 13
- 239000003245 coal Substances 0.000 claims abstract description 3
- 239000011269 tar Substances 0.000 claims abstract description 3
- 238000004821 distillation Methods 0.000 claims description 5
- 238000007669 thermal treatment Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 2
- QWVGKYWNOKOFNN-UHFFFAOYSA-N o-cresol Chemical compound CC1=CC=CC=C1O QWVGKYWNOKOFNN-UHFFFAOYSA-N 0.000 description 6
- NKTOLZVEWDHZMU-UHFFFAOYSA-N 2,5-xylenol Chemical compound CC1=CC=C(C)C(O)=C1 NKTOLZVEWDHZMU-UHFFFAOYSA-N 0.000 description 2
- NXXYKOUNUYWIHA-UHFFFAOYSA-N 2,6-Dimethylphenol Chemical compound CC1=CC=CC(C)=C1O NXXYKOUNUYWIHA-UHFFFAOYSA-N 0.000 description 2
- KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 125000000468 ketone group Chemical group 0.000 description 2
- 150000002576 ketones Chemical class 0.000 description 2
- RLSSMJSEOOYNOY-UHFFFAOYSA-N m-cresol Chemical compound CC1=CC=CC(O)=C1 RLSSMJSEOOYNOY-UHFFFAOYSA-N 0.000 description 2
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 2
- IWDCLRJOBJJRNH-UHFFFAOYSA-N p-cresol Chemical compound CC1=CC=C(O)C=C1 IWDCLRJOBJJRNH-UHFFFAOYSA-N 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 description 1
- LCZUOKDVTBMCMX-UHFFFAOYSA-N 2,5-dimethyl pyrazine Natural products CC1=CN=C(C)C=N1 LCZUOKDVTBMCMX-UHFFFAOYSA-N 0.000 description 1
- HJFZAYHYIWGLNL-UHFFFAOYSA-N 2,6-DiMepyz Natural products CC1=CN=CC(C)=N1 HJFZAYHYIWGLNL-UHFFFAOYSA-N 0.000 description 1
- IXQGCWUGDFDQMF-UHFFFAOYSA-N 2-Ethylphenol Chemical compound CCC1=CC=CC=C1O IXQGCWUGDFDQMF-UHFFFAOYSA-N 0.000 description 1
- SYTQFBVTZCYXOV-UHFFFAOYSA-N 3,5,5-trimethylcyclohex-2-en-1-one Chemical compound CC1=CC(=O)CC(C)(C)C1.CC1=CC(=O)CC(C)(C)C1 SYTQFBVTZCYXOV-UHFFFAOYSA-N 0.000 description 1
- 241000723346 Cinnamomum camphora Species 0.000 description 1
- HDELZEHCSGXWFK-UHFFFAOYSA-N [N].OC1=CC=CC=C1 Chemical compound [N].OC1=CC=CC=C1 HDELZEHCSGXWFK-UHFFFAOYSA-N 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- RWCCWEUUXYIKHB-UHFFFAOYSA-N benzophenone Chemical compound C=1C=CC=CC=1C(=O)C1=CC=CC=C1 RWCCWEUUXYIKHB-UHFFFAOYSA-N 0.000 description 1
- 239000012965 benzophenone Substances 0.000 description 1
- 229960000846 camphor Drugs 0.000 description 1
- 229930008380 camphor Natural products 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 230000000887 hydrating effect Effects 0.000 description 1
- 150000004658 ketimines Chemical class 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- KLIDCXVFHGNTTM-UHFFFAOYSA-N syringol Natural products COC1=CC=CC(OC)=C1O KLIDCXVFHGNTTM-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/005—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by obtaining phenols from products, waste products or side-products of processes, not directed to the production of phenols, by conversion or working-up
- C07C37/007—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by obtaining phenols from products, waste products or side-products of processes, not directed to the production of phenols, by conversion or working-up from the tar industry
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/86—Purification; separation; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19893900629 DE3900629A1 (de) | 1989-01-11 | 1989-01-11 | Verfahren zur reinigung von rohphenol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19893900629 DE3900629A1 (de) | 1989-01-11 | 1989-01-11 | Verfahren zur reinigung von rohphenol |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3900629A1 true DE3900629A1 (de) | 1990-07-12 |
| DE3900629C2 DE3900629C2 (enrdf_load_stackoverflow) | 1990-10-11 |
Family
ID=6371876
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19893900629 Granted DE3900629A1 (de) | 1989-01-11 | 1989-01-11 | Verfahren zur reinigung von rohphenol |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE3900629A1 (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105949037A (zh) * | 2016-03-23 | 2016-09-21 | 中国科学院过程工程研究所 | 一种焦化粗酚精制方法 |
| CN108440302A (zh) * | 2018-03-21 | 2018-08-24 | 司华山 | 一种4,6-二硝基邻甲酚制备工艺 |
-
1989
- 1989-01-11 DE DE19893900629 patent/DE3900629A1/de active Granted
Non-Patent Citations (1)
| Title |
|---|
| DIERICHS/KUBICKA: Phenole und Basen, Akademie- Verlag, 1958, S. 344-350 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105949037A (zh) * | 2016-03-23 | 2016-09-21 | 中国科学院过程工程研究所 | 一种焦化粗酚精制方法 |
| CN105949037B (zh) * | 2016-03-23 | 2019-01-25 | 中国科学院过程工程研究所 | 一种焦化粗酚精制方法 |
| CN108440302A (zh) * | 2018-03-21 | 2018-08-24 | 司华山 | 一种4,6-二硝基邻甲酚制备工艺 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3900629C2 (enrdf_load_stackoverflow) | 1990-10-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OP8 | Request for examination as to paragraph 44 patent law | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: VFT AG, 47138 DUISBURG, DE |
|
| 8327 | Change in the person/name/address of the patent owner |
Owner name: RUETGERS VFT AG, 44579 CASTROP-RAUXEL, DE |
|
| 8327 | Change in the person/name/address of the patent owner |
Owner name: RUTGERS CHEMICALS AG, 44579 CASTROP-RAUXEL, DE |
|
| 8339 | Ceased/non-payment of the annual fee |