DE3763072D1 - Katalytisches verfahren zur herstellung von oximen. - Google Patents
Katalytisches verfahren zur herstellung von oximen.Info
- Publication number
- DE3763072D1 DE3763072D1 DE8787108577T DE3763072T DE3763072D1 DE 3763072 D1 DE3763072 D1 DE 3763072D1 DE 8787108577 T DE8787108577 T DE 8787108577T DE 3763072 T DE3763072 T DE 3763072T DE 3763072 D1 DE3763072 D1 DE 3763072D1
- Authority
- DE
- Germany
- Prior art keywords
- catalytic method
- producing oximes
- oximes
- producing
- catalytic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IT22346/86A IT1198283B (it) | 1986-11-14 | 1986-11-14 | Processo catalitico per la produzione di cicloesanon ossima |
IT19607/87A IT1202643B (it) | 1987-03-06 | 1987-03-06 | Processo catalitico per la produzione di ossime |
Publications (1)
Publication Number | Publication Date |
---|---|
DE3763072D1 true DE3763072D1 (de) | 1990-07-12 |
Family
ID=26327230
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE8787108577T Expired - Lifetime DE3763072D1 (de) | 1986-11-14 | 1987-06-12 | Katalytisches verfahren zur herstellung von oximen. |
Country Status (6)
Country | Link |
---|---|
US (1) | US4794198A (de) |
EP (1) | EP0267362B1 (de) |
JP (1) | JPH0610181B2 (de) |
CA (1) | CA1279068C (de) |
DE (1) | DE3763072D1 (de) |
ES (1) | ES2015287B3 (de) |
Families Citing this family (61)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT1222022B (it) * | 1987-07-14 | 1990-08-31 | Montedipe Spa | Metodo per la preparazione di un catalizzatore per l' ammossimazione di composti carbonilici |
IT1222171B (it) * | 1987-07-29 | 1990-09-05 | Montedipe Spa | Processo per la produzione di chetossime |
IT1223330B (it) * | 1987-10-29 | 1990-09-19 | Montedipe Spa | Processo per la sintesi di una n n dialchil idrossilammina |
IT1217899B (it) * | 1988-06-23 | 1990-03-30 | Montedipe Spa | Processo catalitico per la produzione di ossime |
IT1230769B (it) * | 1989-02-21 | 1991-10-29 | Montedipe Spa | Processo catalitico per la produzione di ossime. |
IT1230096B (it) * | 1989-04-27 | 1991-10-05 | Donegani Guido Ist | Processo per l'ossidazione di ammine sature primarie ad ossime. |
IT1244680B (it) * | 1991-01-23 | 1994-08-08 | Montedipe Srl | Processo a piu' stadi per l'ammossimazione in fase liquida dei composti carbonilici |
DE4138155A1 (de) * | 1991-11-21 | 1993-05-27 | Basf Ag | Verfahren zur herstellung von im wesentlichen alkalifreien titansilikat-kristallen mit zeolithstruktur |
IT1255745B (it) * | 1992-04-01 | 1995-11-15 | Enichem Anic Srl | Processo in due stadi per la produzione in fase liquida di ossime |
CA2149894C (en) * | 1992-12-03 | 1999-04-27 | Rainer Schodel | Titanium silicalite oxidation catalysts |
US5451701A (en) * | 1994-03-11 | 1995-09-19 | Arco Chemical Technology, L.P. | Integrated process for cyclohexanone oxime production |
IT1270196B (it) * | 1994-06-09 | 1997-04-29 | Enichem Spa | Procedimento catalitico per la produzione di ossime |
DE4421928A1 (de) * | 1994-06-23 | 1996-01-04 | Basf Ag | Verfahren zur Herstellung von aliphatischen und cycloaliphatischen Oximen |
US5466869A (en) * | 1994-10-31 | 1995-11-14 | Hoechst Celanese Corporation | Process for perparing 4-hydroxyacetophenone oxime |
US5599987A (en) * | 1995-03-31 | 1997-02-04 | Arco Chemical Technology, L.P. | Integrated process for cyclohexanone oxime production |
BE1010717A3 (fr) * | 1996-10-25 | 1998-12-01 | Solvay | Procede de regeneration de catalyseurs. |
GB2331071A (en) * | 1997-11-11 | 1999-05-12 | Solvay | Manufacture of micro spherical zeolite containing catalyst particles |
DE69901654T2 (de) | 1998-05-19 | 2003-02-06 | Eni S.P.A., Rom/Roma | Aktivierungsmethode für Titansilikalit und dessen Verwendung in Oxidationsverfahren mit Wasserstoffperoxid |
WO2000039084A1 (en) * | 1998-12-25 | 2000-07-06 | Mitsubishi Chemical Corporation | OXIDE CATALYSTS AND PROCESS FOR PRODUCING ε-CAPROLACTAM BY USING THE SAME |
DE19939416A1 (de) | 1999-08-20 | 2001-02-22 | Basf Ag | Verfahren zur Herstellung eines kristallinen, zeolithischen Feststoffs |
IT1314189B1 (it) * | 1999-10-18 | 2002-12-06 | Enichem Spa | Procedimento per la rigenerazione di catalizzatori zeoliticicontenenti titanio |
IT1314001B1 (it) * | 1999-11-19 | 2002-12-03 | Enichem Spa | Metodo per la rimozione del templante da zeoliti sintetiche |
EP1138387A1 (de) * | 2000-03-29 | 2001-10-04 | Degussa AG | Verfahren zur Herstellung eines Titansilicalitformkörpers |
DE10047435A1 (de) * | 2000-09-26 | 2002-04-11 | Degussa | Verfahren zur Herstellung von Oximen |
DE10103581A1 (de) | 2001-01-26 | 2002-08-01 | Degussa | Durch Ammoniumsalze oder substituierte Ammoniumsalze cokatalysiertes Verfahren zur Herstellung von Oximen |
FR2825362B1 (fr) * | 2001-06-01 | 2003-08-15 | Jean Pierre Schirmann | Procede de fabrication de l'oxime de la 2,2,4,4-tetramethyl- 3-pentanone et de sels d'hydroxylammonium |
ITMI20011363A1 (it) * | 2001-06-28 | 2002-12-28 | Enichem Spa | Procedimento per l'attivazione di catalizzatori zeolitici contenenti titanio e loro impiego nelle reazioni di ossidazione |
DE10142621A1 (de) | 2001-08-31 | 2003-03-20 | Degussa | Aufarbeitung der Ammoximationsprodukte von Ketonen durch Flüssig-Flüssig-Extraktion in einem ternären Lösemittelsystem |
DE10142620A1 (de) | 2001-08-31 | 2003-03-20 | Degussa | Ammoximation von Ketonen und Aufarbeitung durch Pervaporation/Dampfpermeation |
DE10158352A1 (de) | 2001-11-28 | 2003-06-12 | Degussa | Zweiphasige Ammoximierung |
AU2003246098A1 (en) | 2002-05-31 | 2003-12-19 | China Petroleum And Chemical Corporation | Oxamidination process of carbonyl compounds |
US7384882B2 (en) * | 2002-05-31 | 2008-06-10 | China Petroleum & Chemical Corporation | Process for regenerating titanium-containing catalysts |
DE10260717A1 (de) | 2002-12-23 | 2004-07-01 | Degussa Ag | Verfahren zur Herstellung von Oximen |
JP4534428B2 (ja) * | 2003-04-09 | 2010-09-01 | 住友化学株式会社 | シクロヘキサノンオキシムの製造方法 |
FR2856400A1 (fr) * | 2003-06-18 | 2004-12-24 | Jean Pierre Schirmann | Procede de fabrication de l'oxime de la methyl ethyl cetone et de l'hydroxylamine base |
JP4552435B2 (ja) * | 2003-12-22 | 2010-09-29 | 住友化学株式会社 | オキシムの製造方法 |
ITMI20032553A1 (it) * | 2003-12-22 | 2005-06-23 | Polimeri Europa Spa | Procedimento per la rimozione degli acidi inorganici e delle impurezze metalliche presenti in soluzioni essenzialmente alcoliche di h202 proveniente da sintesi iretta |
JP4577003B2 (ja) * | 2004-12-16 | 2010-11-10 | 住友化学株式会社 | オキシムの製造方法 |
JP4595804B2 (ja) * | 2004-12-22 | 2010-12-08 | 住友化学株式会社 | シクロヘキサノンオキシムの製造方法 |
SG123723A1 (en) | 2004-12-22 | 2006-07-26 | Sumitomo Chemical Co | Process for producing cyclohexanone oxime |
JP4577205B2 (ja) * | 2004-12-22 | 2010-11-10 | 住友化学株式会社 | シクロヘキサノンオキシムの製造方法 |
JP4577025B2 (ja) * | 2005-01-27 | 2010-11-10 | 住友化学株式会社 | シクロアルカノンオキシムの製造方法 |
JP4635644B2 (ja) * | 2005-02-28 | 2011-02-23 | 住友化学株式会社 | シクロヘキサノンオキシムの製造方法 |
JP4577077B2 (ja) * | 2005-04-25 | 2010-11-10 | 住友化学株式会社 | シクロヘキサノンオキシムの製造方法 |
JP2008088106A (ja) * | 2006-10-02 | 2008-04-17 | Sumitomo Chemical Co Ltd | エポキシ化合物の製造方法 |
EP2098506B1 (de) | 2008-02-22 | 2010-07-28 | Uhde Inventa-Fischer GmbH | Herstellung von Lactamen durch Ammoximierung zyklischer Ketone |
CN101544582B (zh) * | 2008-03-27 | 2012-06-27 | 中国石油化工股份有限公司 | 一种丁酮肟的合成方法 |
DE102008041870A1 (de) * | 2008-09-08 | 2010-03-11 | Evonik Degussa Gmbh | Reaktor mit Titansilikat-Rezyklierung |
CN101486667B (zh) * | 2009-02-13 | 2012-06-20 | 中国天辰工程有限公司 | 采用流化床反应器制备环己酮肟的方法 |
TW201114729A (en) * | 2009-06-18 | 2011-05-01 | Sumitomo Chemical Co | Process for producing oxime |
JP2012067044A (ja) | 2010-09-27 | 2012-04-05 | Sumitomo Chemical Co Ltd | シクロヘキサノンオキシムの製造方法 |
TWI426050B (zh) * | 2011-04-19 | 2014-02-11 | China Petrochemical Dev Corp Taipei Taiwan | A method for preparing titanium-silicon molecular sieve and method for producing cyclohexanone oxime using the molecular sieve |
TWI480100B (zh) * | 2011-04-27 | 2015-04-11 | China Petrochemical Dev Corp Taipei Taiwan | Titanium-silicon molecular sieve and its preparation method and method for producing cyclohexanone oxime using the molecular sieve |
CN102502690A (zh) | 2011-10-31 | 2012-06-20 | 大连理工大学 | 一种基于季铵盐和无机碱混合液的ts-1改性方法 |
CN102584624A (zh) * | 2012-01-19 | 2012-07-18 | 湖南兴鹏化工科技有限公司 | 环己酮氨肟化制备环己酮肟的方法 |
JP2013170153A (ja) * | 2012-02-22 | 2013-09-02 | Sumitomo Chemical Co Ltd | オキシムの製造方法 |
CN105800637B (zh) * | 2016-03-18 | 2018-03-13 | 大连理工大学 | 一种快速合成高骨架钛含量钛硅分子筛的免除醇制备方法 |
CN107539998B (zh) * | 2016-06-27 | 2019-12-27 | 中国石油化工股份有限公司 | 一种钛硅分子筛及其合成方法和应用以及一种环酮氧化的方法 |
CN108002404B (zh) * | 2016-10-27 | 2019-11-15 | 中国石油化工股份有限公司 | 一种含贵金属钛硅分子筛及其合成方法和应用 |
CN108002986B (zh) * | 2016-10-27 | 2021-03-12 | 中国石油化工股份有限公司 | 一种由丙烯制备丙二醇单甲醚的方法 |
WO2020078884A1 (en) | 2018-10-17 | 2020-04-23 | Cap Iii B.V. | An improved process and plant for the production of oximes |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1245371B (de) * | 1966-02-07 | 1967-07-27 | Toa Gosei Chem Ind | Verfahren zur Herstellung von Cyclohexanonoxim |
US3960954A (en) * | 1968-05-27 | 1976-06-01 | Halcon International, Inc. | Process for preparing oximes and hydroxylamines |
US4163756A (en) * | 1978-04-11 | 1979-08-07 | Allied Chemical Corporation | Direct oximation of ketones |
IT1127311B (it) * | 1979-12-21 | 1986-05-21 | Anic Spa | Materiale sintetico,cristallino,poroso costituito da ossidi di silicio e titanio,metodo per la sua preparazione e suoi usi |
US4281194A (en) * | 1980-02-28 | 1981-07-28 | Allied Chemical Corporation | Process for ammoximation of cyclohexanone |
US4560797A (en) * | 1982-12-20 | 1985-12-24 | Allied Corporation | Oxidation of primary amines to oximes by elemental oxygen with catalyst regeneration |
US4504681A (en) * | 1982-12-20 | 1985-03-12 | Allied Corporation | Catalytic oxidation of primary amines to oximes by elemental oxygen |
EP0132550A1 (de) * | 1983-06-27 | 1985-02-13 | Norton Company | Zeolith und Verfahren zu seiner Herstellung |
IT1214622B (it) * | 1985-07-10 | 1990-01-18 | Montedipe Spa | Processo catalitico per laproduzione di cicloesanonossima. |
-
1987
- 1987-06-08 JP JP62141638A patent/JPH0610181B2/ja not_active Expired - Lifetime
- 1987-06-08 US US07/059,536 patent/US4794198A/en not_active Expired - Lifetime
- 1987-06-09 CA CA000539254A patent/CA1279068C/en not_active Expired - Lifetime
- 1987-06-12 EP EP87108577A patent/EP0267362B1/de not_active Expired - Lifetime
- 1987-06-12 ES ES87108577T patent/ES2015287B3/es not_active Expired - Lifetime
- 1987-06-12 DE DE8787108577T patent/DE3763072D1/de not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
JPH0610181B2 (ja) | 1994-02-09 |
EP0267362A1 (de) | 1988-05-18 |
CA1279068C (en) | 1991-01-15 |
US4794198A (en) | 1988-12-27 |
JPS63130575A (ja) | 1988-06-02 |
ES2015287B3 (es) | 1990-08-16 |
EP0267362B1 (de) | 1990-06-06 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition |