DE3620991A1 - Wasserloesliche alkenyl- oder alkylbernsteinsaeureester enthaltende celluloseether - Google Patents
Wasserloesliche alkenyl- oder alkylbernsteinsaeureester enthaltende celluloseetherInfo
- Publication number
- DE3620991A1 DE3620991A1 DE19863620991 DE3620991A DE3620991A1 DE 3620991 A1 DE3620991 A1 DE 3620991A1 DE 19863620991 DE19863620991 DE 19863620991 DE 3620991 A DE3620991 A DE 3620991A DE 3620991 A1 DE3620991 A1 DE 3620991A1
- Authority
- DE
- Germany
- Prior art keywords
- water
- cellulose
- weight
- cellulose ether
- cellulose ethers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 229920003086 cellulose ether Polymers 0.000 title claims abstract description 35
- 229920002678 cellulose Polymers 0.000 claims abstract description 13
- 239000001913 cellulose Substances 0.000 claims abstract description 13
- 229940014800 succinic anhydride Drugs 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000006243 chemical reaction Methods 0.000 claims abstract description 7
- 239000002253 acid Substances 0.000 claims abstract description 6
- 125000004432 carbon atom Chemical group C* 0.000 claims abstract description 5
- 239000003513 alkali Substances 0.000 claims abstract description 4
- 239000008346 aqueous phase Substances 0.000 claims abstract description 4
- 239000000084 colloidal system Substances 0.000 claims abstract description 3
- 239000006185 dispersion Substances 0.000 claims abstract description 3
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 3
- 239000000178 monomer Substances 0.000 claims abstract description 3
- 230000001681 protective effect Effects 0.000 claims abstract description 3
- 239000004094 surface-active agent Substances 0.000 claims abstract description 3
- 239000002562 thickening agent Substances 0.000 claims abstract description 3
- -1 alkyl succinic anhydride Chemical compound 0.000 claims description 20
- 238000000034 method Methods 0.000 claims description 9
- FALRKNHUBBKYCC-UHFFFAOYSA-N 2-(chloromethyl)pyridine-3-carbonitrile Chemical class ClCC1=NC=CC=C1C#N FALRKNHUBBKYCC-UHFFFAOYSA-N 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 3
- 239000004566 building material Substances 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 238000010557 suspension polymerization reaction Methods 0.000 claims description 2
- 239000001384 succinic acid Substances 0.000 claims 1
- 239000000725 suspension Substances 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 abstract 1
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 14
- 239000000243 solution Substances 0.000 description 12
- WVRNUXJQQFPNMN-VAWYXSNFSA-N 3-[(e)-dodec-1-enyl]oxolane-2,5-dione Chemical compound CCCCCCCCCC\C=C\C1CC(=O)OC1=O WVRNUXJQQFPNMN-VAWYXSNFSA-N 0.000 description 9
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- 239000007864 aqueous solution Substances 0.000 description 7
- 239000002904 solvent Substances 0.000 description 7
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- QDCPNGVVOWVKJG-VAWYXSNFSA-N 2-[(e)-dodec-1-enyl]butanedioic acid Chemical group CCCCCCCCCC\C=C\C(C(O)=O)CC(O)=O QDCPNGVVOWVKJG-VAWYXSNFSA-N 0.000 description 5
- 125000003342 alkenyl group Chemical group 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 229920002153 Hydroxypropyl cellulose Polymers 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000000010 aprotic solvent Substances 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 150000002170 ethers Chemical class 0.000 description 3
- 239000001863 hydroxypropyl cellulose Substances 0.000 description 3
- 235000010977 hydroxypropyl cellulose Nutrition 0.000 description 3
- RINCXYDBBGOEEQ-UHFFFAOYSA-N succinic anhydride Chemical class O=C1CCC(=O)O1 RINCXYDBBGOEEQ-UHFFFAOYSA-N 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 125000004185 ester group Chemical group 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- LEQAOMBKQFMDFZ-UHFFFAOYSA-N glyoxal Chemical compound O=CC=O LEQAOMBKQFMDFZ-UHFFFAOYSA-N 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- YAXXOCZAXKLLCV-UHFFFAOYSA-N 3-dodecyloxolane-2,5-dione Chemical class CCCCCCCCCCCCC1CC(=O)OC1=O YAXXOCZAXKLLCV-UHFFFAOYSA-N 0.000 description 1
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 description 1
- GAWIXWVDTYZWAW-UHFFFAOYSA-N C[CH]O Chemical group C[CH]O GAWIXWVDTYZWAW-UHFFFAOYSA-N 0.000 description 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 125000001033 ether group Chemical group 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229940015043 glyoxal Drugs 0.000 description 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 235000010981 methylcellulose Nutrition 0.000 description 1
- GRVDJDISBSALJP-UHFFFAOYSA-N methyloxidanyl Chemical group [O]C GRVDJDISBSALJP-UHFFFAOYSA-N 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
- C04B24/24—Macromolecular compounds
- C04B24/38—Polysaccharides or derivatives thereof
- C04B24/383—Cellulose or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B13/00—Preparation of cellulose ether-esters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/12—Polymerisation in non-solvents
- C08F2/16—Aqueous medium
- C08F2/22—Emulsion polymerisation
- C08F2/24—Emulsion polymerisation with the aid of emulsifying agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/43—Thickening agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L1/00—Compositions of cellulose, modified cellulose or cellulose derivatives
- C08L1/08—Cellulose derivatives
- C08L1/32—Cellulose ether-esters
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Ceramic Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Wood Science & Technology (AREA)
- Biochemistry (AREA)
- Structural Engineering (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Priority Applications (9)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863620991 DE3620991A1 (de) | 1986-06-23 | 1986-06-23 | Wasserloesliche alkenyl- oder alkylbernsteinsaeureester enthaltende celluloseether |
| ES198787108595T ES2036546T3 (es) | 1986-06-23 | 1987-06-15 | Eteres de celulosa hidrosolubles que contienen esteres del acido alquenil- o alquilsuccinico. |
| AT87108595T ATE75755T1 (de) | 1986-06-23 | 1987-06-15 | Alkenyl- oder alkylbernsteinsaeureester enthaltende wasserloesliche celluloseether. |
| EP87108595A EP0254025B1 (de) | 1986-06-23 | 1987-06-15 | Alkenyl- oder Alkylbernsteinsäureester enthaltende Wasserlösliche Celluloseether |
| DE8787108595T DE3778775D1 (de) | 1986-06-23 | 1987-06-15 | Alkenyl- oder alkylbernsteinsaeureester enthaltende wasserloesliche celluloseether. |
| JP62153587A JPS633001A (ja) | 1986-06-23 | 1987-06-22 | アルケニル又はアルキルコハク酸エステルを含む水溶性セルロ−スエ−テル |
| CA000540384A CA1287628C (en) | 1986-06-23 | 1987-06-23 | Water-soluble ethers substituted with alkenyl or alkyl succinic acidesters |
| US07/307,211 US4906744A (en) | 1986-06-23 | 1989-02-03 | Water-soluble ethers substituted with alkenyl or alkyl succinic acid esters |
| GR920401595T GR3005266T3 (enExample) | 1986-06-23 | 1992-07-24 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863620991 DE3620991A1 (de) | 1986-06-23 | 1986-06-23 | Wasserloesliche alkenyl- oder alkylbernsteinsaeureester enthaltende celluloseether |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3620991A1 true DE3620991A1 (de) | 1988-01-14 |
Family
ID=6303513
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19863620991 Withdrawn DE3620991A1 (de) | 1986-06-23 | 1986-06-23 | Wasserloesliche alkenyl- oder alkylbernsteinsaeureester enthaltende celluloseether |
| DE8787108595T Expired - Fee Related DE3778775D1 (de) | 1986-06-23 | 1987-06-15 | Alkenyl- oder alkylbernsteinsaeureester enthaltende wasserloesliche celluloseether. |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE8787108595T Expired - Fee Related DE3778775D1 (de) | 1986-06-23 | 1987-06-15 | Alkenyl- oder alkylbernsteinsaeureester enthaltende wasserloesliche celluloseether. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4906744A (enExample) |
| EP (1) | EP0254025B1 (enExample) |
| JP (1) | JPS633001A (enExample) |
| AT (1) | ATE75755T1 (enExample) |
| CA (1) | CA1287628C (enExample) |
| DE (2) | DE3620991A1 (enExample) |
| ES (1) | ES2036546T3 (enExample) |
| GR (1) | GR3005266T3 (enExample) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3887114D1 (de) * | 1987-12-11 | 1994-02-24 | Akzo Nv | Biocompatible Dialysemembran aus Cellulose mit erhöhter Beta-2-Microglobulinadsorption. |
| DE4317231A1 (de) * | 1993-05-24 | 1994-12-01 | Wolff Walsrode Ag | Thermoplastische Celluloseetherester-Mischpfropfpolymerisate und Verfahren zu ihrer Herstellung |
| EP0703243B1 (en) * | 1994-09-26 | 2000-12-13 | Unilever N.V. | Process for the preparation of a liquid detergent composition. |
| US5763381A (en) * | 1995-09-13 | 1998-06-09 | National Starch And Chemical Investment Holding Corporation | Starched-based adjuncts for detergents |
| DE19708531A1 (de) * | 1997-03-03 | 1998-09-10 | Clariant Gmbh | 2-Propenylgruppen enthaltende Celluloseether und deren Verwendung als Schutzkolloide bei Polymerisationen |
| US11173106B2 (en) * | 2009-10-07 | 2021-11-16 | Johnson & Johnson Consumer Inc. | Compositions comprising a superhydrophilic amphiphilic copolymer and a micellar thickener |
| US8399590B2 (en) * | 2009-10-07 | 2013-03-19 | Akzo Nobel Chemicals International B.V. | Superhydrophilic amphiphilic copolymers and processes for making the same |
| US8258250B2 (en) | 2009-10-07 | 2012-09-04 | Johnson & Johnson Consumer Companies, Inc. | Compositions comprising superhydrophilic amphiphilic copolymers and methods of use thereof |
| JP6306691B2 (ja) * | 2013-05-14 | 2018-04-04 | ダウ グローバル テクノロジーズ エルエルシー | ジカルボン酸を用いたエステル化セルロースエーテル |
| JP6543086B2 (ja) * | 2015-05-20 | 2019-07-10 | 住友ゴム工業株式会社 | ゴム組成物、タイヤ用ゴム組成物及び空気入りタイヤ |
| JP6378130B2 (ja) * | 2015-05-20 | 2018-08-22 | 住友ゴム工業株式会社 | 空気入りタイヤ |
| JP6378132B2 (ja) * | 2015-05-20 | 2018-08-22 | 住友ゴム工業株式会社 | 空気入りタイヤ |
| JP6378131B2 (ja) * | 2015-05-20 | 2018-08-22 | 住友ゴム工業株式会社 | 空気入りタイヤ |
| JP6423311B2 (ja) * | 2015-05-20 | 2018-11-14 | 住友ゴム工業株式会社 | 空気入りタイヤ |
| JP6378134B2 (ja) * | 2015-05-20 | 2018-08-22 | 住友ゴム工業株式会社 | 空気入りタイヤ |
| JP6378133B2 (ja) * | 2015-05-20 | 2018-08-22 | 住友ゴム工業株式会社 | ランフラットタイヤ |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2661349A (en) * | 1949-02-18 | 1953-12-01 | Nat Starch Products Inc | Polysaccharide derivatives of substituted dicarboxylic acids |
| GB2063880B (en) * | 1979-09-24 | 1983-08-03 | Secr Defence | Internally plasticised cellulose ether-esters |
-
1986
- 1986-06-23 DE DE19863620991 patent/DE3620991A1/de not_active Withdrawn
-
1987
- 1987-06-15 EP EP87108595A patent/EP0254025B1/de not_active Expired - Lifetime
- 1987-06-15 AT AT87108595T patent/ATE75755T1/de not_active IP Right Cessation
- 1987-06-15 ES ES198787108595T patent/ES2036546T3/es not_active Expired - Lifetime
- 1987-06-15 DE DE8787108595T patent/DE3778775D1/de not_active Expired - Fee Related
- 1987-06-22 JP JP62153587A patent/JPS633001A/ja active Pending
- 1987-06-23 CA CA000540384A patent/CA1287628C/en not_active Expired - Fee Related
-
1989
- 1989-02-03 US US07/307,211 patent/US4906744A/en not_active Expired - Lifetime
-
1992
- 1992-07-24 GR GR920401595T patent/GR3005266T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP0254025B1 (de) | 1992-05-06 |
| JPS633001A (ja) | 1988-01-08 |
| GR3005266T3 (enExample) | 1993-05-24 |
| US4906744A (en) | 1990-03-06 |
| CA1287628C (en) | 1991-08-13 |
| ES2036546T3 (es) | 1993-06-01 |
| EP0254025A2 (de) | 1988-01-27 |
| ATE75755T1 (de) | 1992-05-15 |
| DE3778775D1 (de) | 1992-06-11 |
| EP0254025A3 (en) | 1988-04-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8141 | Disposal/no request for examination |