DE296867C - - Google Patents
Info
- Publication number
- DE296867C DE296867C DENDAT296867D DE296867DA DE296867C DE 296867 C DE296867 C DE 296867C DE NDAT296867 D DENDAT296867 D DE NDAT296867D DE 296867D A DE296867D A DE 296867DA DE 296867 C DE296867 C DE 296867C
- Authority
- DE
- Germany
- Prior art keywords
- mercury
- arc
- metal
- reduction
- nozzle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims description 33
- 229910052751 metal Inorganic materials 0.000 claims description 30
- 239000002184 metal Substances 0.000 claims description 30
- 229910052753 mercury Inorganic materials 0.000 claims description 29
- 238000000034 method Methods 0.000 claims description 22
- 230000001603 reducing Effects 0.000 claims description 20
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 18
- 229910052796 boron Inorganic materials 0.000 claims description 18
- 238000006722 reduction reaction Methods 0.000 claims description 16
- 238000006243 chemical reaction Methods 0.000 claims description 11
- 150000001875 compounds Chemical class 0.000 claims description 9
- 229910000497 Amalgam Inorganic materials 0.000 claims description 6
- 150000004820 halides Chemical class 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 5
- RTAQQCXQSZGOHL-UHFFFAOYSA-N titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 5
- 229910052719 titanium Inorganic materials 0.000 claims description 5
- 239000010936 titanium Substances 0.000 claims description 5
- QCWXUUIWCKQGHC-UHFFFAOYSA-N zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 4
- 229910052726 zirconium Inorganic materials 0.000 claims description 4
- 150000002739 metals Chemical class 0.000 claims description 3
- 150000003568 thioethers Chemical class 0.000 claims description 3
- 229910052720 vanadium Inorganic materials 0.000 claims description 3
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium(0) Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims description 3
- 229910052776 Thorium Inorganic materials 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- 238000004821 distillation Methods 0.000 claims description 2
- 230000000087 stabilizing Effects 0.000 claims description 2
- ZSLUVFAKFWKJRC-UHFFFAOYSA-N thorium Chemical compound [Th] ZSLUVFAKFWKJRC-UHFFFAOYSA-N 0.000 claims description 2
- 239000000463 material Substances 0.000 description 14
- 238000010438 heat treatment Methods 0.000 description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- FAQYAMRNWDIXMY-UHFFFAOYSA-N trichloroborane Chemical compound ClB(Cl)Cl FAQYAMRNWDIXMY-UHFFFAOYSA-N 0.000 description 6
- 239000007858 starting material Substances 0.000 description 5
- 150000001805 chlorine compounds Chemical class 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 239000001257 hydrogen Substances 0.000 description 4
- 229910052739 hydrogen Inorganic materials 0.000 description 4
- -1 B. of calcium Chemical class 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 3
- 229910052721 tungsten Inorganic materials 0.000 description 3
- 239000010937 tungsten Substances 0.000 description 3
- GFQYVLUOOAAOGM-UHFFFAOYSA-N Zirconium(IV) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- 239000003517 fume Substances 0.000 description 2
- 150000002731 mercury compounds Chemical class 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 229910052709 silver Inorganic materials 0.000 description 2
- 239000004332 silver Substances 0.000 description 2
- KEAYESYHFKHZAL-UHFFFAOYSA-N sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 238000000859 sublimation Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910052845 zircon Inorganic materials 0.000 description 2
- 229910052846 zircon Inorganic materials 0.000 description 2
- 241000094396 Bolitoglossa carri Species 0.000 description 1
- 229910052684 Cerium Inorganic materials 0.000 description 1
- 210000000078 Claw Anatomy 0.000 description 1
- 241001148662 Phragmites australis Species 0.000 description 1
- XJDNKRIXUMDJCW-UHFFFAOYSA-J Titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 1
- 229910052770 Uranium Inorganic materials 0.000 description 1
- DUNKXUFBGCUVQW-UHFFFAOYSA-J Zirconium(IV) chloride Chemical compound Cl[Zr](Cl)(Cl)Cl DUNKXUFBGCUVQW-UHFFFAOYSA-J 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 230000002349 favourable Effects 0.000 description 1
- 238000005755 formation reaction Methods 0.000 description 1
- 150000002366 halogen compounds Chemical class 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 230000000977 initiatory Effects 0.000 description 1
- 229940100892 mercury compounds Drugs 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N oxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- FZTWZIMSKAGPSB-UHFFFAOYSA-N phosphide(3-) Chemical compound [P-3] FZTWZIMSKAGPSB-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 229910052904 quartz Inorganic materials 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
- 150000003755 zirconium compounds Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B35/00—Boron; Compounds thereof
- C01B35/02—Boron; Borides
- C01B35/023—Boron
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE296867C true DE296867C (es) |
Family
ID=551215
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT296867D Active DE296867C (es) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE296867C (es) |
Cited By (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2676882A (en) * | 1950-05-31 | 1954-04-27 | Kennecott Copper Corp | Method for recovering refractory metals |
| US2703752A (en) * | 1951-01-20 | 1955-03-08 | Kennecott Copper Corp | Method for production of refractory metals |
| US2708158A (en) * | 1950-09-27 | 1955-05-10 | Eugene M Smith | Production of titanium |
| US2758921A (en) * | 1952-06-24 | 1956-08-14 | Reynolds Metals Co | Reducing metal compounds with amalgam |
| US2764480A (en) * | 1952-08-19 | 1956-09-25 | Fulmer Res Inst Ltd | Production and purification of titanium |
| US2772875A (en) * | 1953-02-18 | 1956-12-04 | Levy Joseph Peppo | Production of pure titanium and zirconium |
| US2773759A (en) * | 1952-02-19 | 1956-12-11 | Monsanto Chemicals | Production of refractory metals |
| US2805151A (en) * | 1953-09-29 | 1957-09-03 | Du Pont | Method of minimizing product buildup in the production of metal including titanium and zirconium |
| US2813787A (en) * | 1952-07-03 | 1957-11-19 | Reynolds Metals Co | Method of reducing metal compounds with amalgam |
| US2814561A (en) * | 1953-02-26 | 1957-11-26 | Union Carbide Corp | Process and apparatus for reducing metal chlorides employing calcium carbide |
| US2816828A (en) * | 1956-06-20 | 1957-12-17 | Nat Res Corp | Method of producing refractory metals |
| US2827371A (en) * | 1951-11-01 | 1958-03-18 | Ici Ltd | Method of producing titanium in an agitated solids bed |
| US2828199A (en) * | 1950-12-13 | 1958-03-25 | Nat Res Corp | Method for producing metals |
| US2830893A (en) * | 1954-04-06 | 1958-04-15 | Chicago Dev Corp | Processes for making titanium |
| US2839384A (en) * | 1954-10-26 | 1958-06-17 | Du Pont | Method for producing fourth group metals |
| US2854392A (en) * | 1955-09-22 | 1958-09-30 | Tokumoto Shin-Ichi | Arc discharge production of low valency halides of titanium |
| US2870007A (en) * | 1952-07-17 | 1959-01-20 | Degussa | Process for the production of metals by reduction of their compounds in the vapor phase |
| US2890953A (en) * | 1954-11-16 | 1959-06-16 | Peter Spence & Sons Ltd | Continuous process for the manufacture of titanium metal |
| US2902360A (en) * | 1957-05-14 | 1959-09-01 | Ionics | Production of titanium and zirconium by reduction of their sulfides |
| US2956872A (en) * | 1956-01-23 | 1960-10-18 | Ethyl Corp | Preparation of refractory metals |
| US2978316A (en) * | 1953-09-14 | 1961-04-04 | Weir Horace Mccolloch | Production of elements and compounds by continuous vapor plating of particles |
| US3058820A (en) * | 1958-07-25 | 1962-10-16 | Bert W Whitehurst | Method of producing titanium metal |
| US3123464A (en) * | 1964-03-03 | Method of producing titanium |
-
0
- DE DENDAT296867D patent/DE296867C/de active Active
Cited By (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3123464A (en) * | 1964-03-03 | Method of producing titanium | ||
| US2676882A (en) * | 1950-05-31 | 1954-04-27 | Kennecott Copper Corp | Method for recovering refractory metals |
| US2708158A (en) * | 1950-09-27 | 1955-05-10 | Eugene M Smith | Production of titanium |
| US2828199A (en) * | 1950-12-13 | 1958-03-25 | Nat Res Corp | Method for producing metals |
| US2703752A (en) * | 1951-01-20 | 1955-03-08 | Kennecott Copper Corp | Method for production of refractory metals |
| US2827371A (en) * | 1951-11-01 | 1958-03-18 | Ici Ltd | Method of producing titanium in an agitated solids bed |
| US2773759A (en) * | 1952-02-19 | 1956-12-11 | Monsanto Chemicals | Production of refractory metals |
| US2758921A (en) * | 1952-06-24 | 1956-08-14 | Reynolds Metals Co | Reducing metal compounds with amalgam |
| US2813787A (en) * | 1952-07-03 | 1957-11-19 | Reynolds Metals Co | Method of reducing metal compounds with amalgam |
| US2870007A (en) * | 1952-07-17 | 1959-01-20 | Degussa | Process for the production of metals by reduction of their compounds in the vapor phase |
| US2764480A (en) * | 1952-08-19 | 1956-09-25 | Fulmer Res Inst Ltd | Production and purification of titanium |
| US2772875A (en) * | 1953-02-18 | 1956-12-04 | Levy Joseph Peppo | Production of pure titanium and zirconium |
| US2814561A (en) * | 1953-02-26 | 1957-11-26 | Union Carbide Corp | Process and apparatus for reducing metal chlorides employing calcium carbide |
| US2978316A (en) * | 1953-09-14 | 1961-04-04 | Weir Horace Mccolloch | Production of elements and compounds by continuous vapor plating of particles |
| US2805151A (en) * | 1953-09-29 | 1957-09-03 | Du Pont | Method of minimizing product buildup in the production of metal including titanium and zirconium |
| US2830893A (en) * | 1954-04-06 | 1958-04-15 | Chicago Dev Corp | Processes for making titanium |
| US2839384A (en) * | 1954-10-26 | 1958-06-17 | Du Pont | Method for producing fourth group metals |
| US2890953A (en) * | 1954-11-16 | 1959-06-16 | Peter Spence & Sons Ltd | Continuous process for the manufacture of titanium metal |
| US2854392A (en) * | 1955-09-22 | 1958-09-30 | Tokumoto Shin-Ichi | Arc discharge production of low valency halides of titanium |
| US2956872A (en) * | 1956-01-23 | 1960-10-18 | Ethyl Corp | Preparation of refractory metals |
| US2816828A (en) * | 1956-06-20 | 1957-12-17 | Nat Res Corp | Method of producing refractory metals |
| US2902360A (en) * | 1957-05-14 | 1959-09-01 | Ionics | Production of titanium and zirconium by reduction of their sulfides |
| US3058820A (en) * | 1958-07-25 | 1962-10-16 | Bert W Whitehurst | Method of producing titanium metal |
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