DE2628746C3 - Vorrichtung zur Herstellung von Aluminiumalkylverbindungen - Google Patents
Vorrichtung zur Herstellung von AluminiumalkylverbindungenInfo
- Publication number
- DE2628746C3 DE2628746C3 DE2628746A DE2628746A DE2628746C3 DE 2628746 C3 DE2628746 C3 DE 2628746C3 DE 2628746 A DE2628746 A DE 2628746A DE 2628746 A DE2628746 A DE 2628746A DE 2628746 C3 DE2628746 C3 DE 2628746C3
- Authority
- DE
- Germany
- Prior art keywords
- aluminum
- reactor
- reaction
- gas
- liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052782 aluminium Inorganic materials 0.000 title claims description 45
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 39
- 239000007789 gas Substances 0.000 claims description 37
- 238000006243 chemical reaction Methods 0.000 claims description 23
- 239000007788 liquid Substances 0.000 claims description 21
- 239000001257 hydrogen Substances 0.000 claims description 13
- 229910052739 hydrogen Inorganic materials 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 13
- 239000012429 reaction media Substances 0.000 claims description 12
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 9
- 239000000376 reactant Substances 0.000 claims description 9
- 239000007787 solid Substances 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 7
- 239000011261 inert gas Substances 0.000 claims description 6
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical compound [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims description 5
- 150000002431 hydrogen Chemical class 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 2
- 239000007795 chemical reaction product Substances 0.000 claims 2
- 239000012071 phase Substances 0.000 description 19
- 239000002245 particle Substances 0.000 description 8
- 229910000096 monohydride Inorganic materials 0.000 description 6
- 229930195733 hydrocarbon Natural products 0.000 description 5
- 239000007791 liquid phase Substances 0.000 description 5
- 238000000926 separation method Methods 0.000 description 5
- VXNZUUAINFGPBY-UHFFFAOYSA-N 1-Butene Chemical compound CCC=C VXNZUUAINFGPBY-UHFFFAOYSA-N 0.000 description 4
- 239000004215 Carbon black (E152) Substances 0.000 description 4
- VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical compound CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 description 4
- IAQRGUVFOMOMEM-UHFFFAOYSA-N but-2-ene Chemical compound CC=CC IAQRGUVFOMOMEM-UHFFFAOYSA-N 0.000 description 4
- 239000012295 chemical reaction liquid Substances 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 238000007872 degassing Methods 0.000 description 3
- VTZJFPSWNQFPCQ-UHFFFAOYSA-N dibutylaluminum Chemical compound CCCC[Al]CCCC VTZJFPSWNQFPCQ-UHFFFAOYSA-N 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 2
- 239000001273 butane Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- XNMQEEKYCVKGBD-UHFFFAOYSA-N dimethylacetylene Natural products CC#CC XNMQEEKYCVKGBD-UHFFFAOYSA-N 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000001282 iso-butane Substances 0.000 description 2
- AWJUIBRHMBBTKR-UHFFFAOYSA-N isoquinoline Chemical compound C1=NC=CC2=CC=CC=C21 AWJUIBRHMBBTKR-UHFFFAOYSA-N 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 2
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
- 239000007790 solid phase Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 101100378709 Arabidopsis thaliana AIR3 gene Proteins 0.000 description 1
- 125000000217 alkyl group Chemical class 0.000 description 1
- 230000029936 alkylation Effects 0.000 description 1
- 238000005804 alkylation reaction Methods 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 230000009172 bursting Effects 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 230000009918 complex formation Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000010908 decantation Methods 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 231100001261 hazardous Toxicity 0.000 description 1
- 150000004678 hydrides Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 239000002923 metal particle Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 239000012495 reaction gas Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 125000002914 sec-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/04—Pressure vessels, e.g. autoclaves
- B01J3/044—Pressure vessels, e.g. autoclaves in the form of a loop
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/06—Aluminium compounds
- C07F5/061—Aluminium compounds with C-aluminium linkage
- C07F5/065—Aluminium compounds with C-aluminium linkage compounds with an Al-H linkage
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7520254A FR2315506A1 (fr) | 1975-06-27 | 1975-06-27 | Procede et dispositif de fabrication d'alkylaluminiums |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2628746A1 DE2628746A1 (de) | 1977-04-21 |
| DE2628746B2 DE2628746B2 (de) | 1978-01-26 |
| DE2628746C3 true DE2628746C3 (de) | 1978-09-21 |
Family
ID=9157184
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2628746A Expired DE2628746C3 (de) | 1975-06-27 | 1976-06-25 | Vorrichtung zur Herstellung von Aluminiumalkylverbindungen |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US4111662A (OSRAM) |
| JP (1) | JPS5217426A (OSRAM) |
| AT (1) | AT352752B (OSRAM) |
| BE (1) | BE843405A (OSRAM) |
| BR (1) | BR7604174A (OSRAM) |
| CA (1) | CA1085866A (OSRAM) |
| CH (1) | CH614635A5 (OSRAM) |
| DE (1) | DE2628746C3 (OSRAM) |
| ES (1) | ES449213A1 (OSRAM) |
| FR (1) | FR2315506A1 (OSRAM) |
| GB (1) | GB1515812A (OSRAM) |
| IT (1) | IT1065645B (OSRAM) |
| LU (1) | LU75247A1 (OSRAM) |
| NL (1) | NL7606973A (OSRAM) |
| RO (1) | RO69044A (OSRAM) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5597937A (en) * | 1995-05-11 | 1997-01-28 | Albemarle Corporation | Conversion of deep internal olefins into primary alkylaluminum compounds by isomerization-displacement |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2576769A (en) * | 1950-10-23 | 1951-11-27 | Souren Z Avedikian | Method of making hyposulfites by means of amalgam |
| US3373179A (en) * | 1962-09-14 | 1968-03-12 | Continental Oil Co | Method for the manufacture of dialkyl aluminum hydride compounds |
| US3388142A (en) * | 1963-07-12 | 1968-06-11 | Continental Oil Co | Method for producing dialkylaluminum hydride compounds |
| BE759284A (fr) * | 1969-11-24 | 1971-05-24 | Shell Int Research | Procede et appareil pour la mise en contact d'un liquide avec des particules solides |
-
1975
- 1975-06-27 FR FR7520254A patent/FR2315506A1/fr active Granted
-
1976
- 1976-06-24 US US05/699,338 patent/US4111662A/en not_active Expired - Lifetime
- 1976-06-25 ES ES449213A patent/ES449213A1/es not_active Expired
- 1976-06-25 BR BR7604174A patent/BR7604174A/pt unknown
- 1976-06-25 GB GB26641/76A patent/GB1515812A/en not_active Expired
- 1976-06-25 IT IT50134/76A patent/IT1065645B/it active
- 1976-06-25 DE DE2628746A patent/DE2628746C3/de not_active Expired
- 1976-06-25 AT AT469776A patent/AT352752B/de not_active IP Right Cessation
- 1976-06-25 JP JP51075380A patent/JPS5217426A/ja active Granted
- 1976-06-25 NL NL7606973A patent/NL7606973A/xx not_active Application Discontinuation
- 1976-06-25 BE BE168307A patent/BE843405A/xx not_active IP Right Cessation
- 1976-06-25 CA CA255,770A patent/CA1085866A/en not_active Expired
- 1976-06-25 LU LU75247A patent/LU75247A1/xx unknown
- 1976-06-25 CH CH820076A patent/CH614635A5/xx not_active IP Right Cessation
- 1976-08-28 RO RO7686596A patent/RO69044A/ro unknown
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5217426A (en) | 1977-02-09 |
| AT352752B (de) | 1979-10-10 |
| DE2628746A1 (de) | 1977-04-21 |
| US4111662A (en) | 1978-09-05 |
| CH614635A5 (OSRAM) | 1979-12-14 |
| ATA469776A (de) | 1979-03-15 |
| IT1065645B (it) | 1985-03-04 |
| BE843405A (fr) | 1976-12-27 |
| CA1085866A (en) | 1980-09-16 |
| FR2315506A1 (fr) | 1977-01-21 |
| GB1515812A (en) | 1978-06-28 |
| LU75247A1 (OSRAM) | 1977-03-16 |
| NL7606973A (nl) | 1976-12-29 |
| ES449213A1 (es) | 1977-07-16 |
| JPS5442963B2 (OSRAM) | 1979-12-17 |
| FR2315506B1 (OSRAM) | 1977-12-02 |
| DE2628746B2 (de) | 1978-01-26 |
| BR7604174A (pt) | 1977-07-26 |
| RO69044A (ro) | 1980-05-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |