DE2508708C2 - Elektrolytlösungen auf Cr (VI)-Basis zur galvanischen Abscheidung von Chromschichten - Google Patents
Elektrolytlösungen auf Cr (VI)-Basis zur galvanischen Abscheidung von ChromschichtenInfo
- Publication number
- DE2508708C2 DE2508708C2 DE2508708A DE2508708A DE2508708C2 DE 2508708 C2 DE2508708 C2 DE 2508708C2 DE 2508708 A DE2508708 A DE 2508708A DE 2508708 A DE2508708 A DE 2508708A DE 2508708 C2 DE2508708 C2 DE 2508708C2
- Authority
- DE
- Germany
- Prior art keywords
- chromium
- electrolyte solutions
- galvanic deposition
- solutions based
- chromium layers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical group [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 title claims description 28
- 239000011651 chromium Substances 0.000 title claims description 13
- 229910052804 chromium Inorganic materials 0.000 title claims description 9
- 239000008151 electrolyte solution Substances 0.000 title claims description 7
- 229940021013 electrolyte solution Drugs 0.000 title claims description 7
- 230000008021 deposition Effects 0.000 title claims description 6
- 239000004094 surface-active agent Substances 0.000 claims description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 3
- JOPOVCBBYLSVDA-UHFFFAOYSA-N chromium(6+) Chemical compound [Cr+6] JOPOVCBBYLSVDA-UHFFFAOYSA-N 0.000 claims description 3
- 150000003871 sulfonates Chemical class 0.000 claims description 2
- KRVSOGSZCMJSLX-UHFFFAOYSA-L chromic acid Substances O[Cr](O)(=O)=O KRVSOGSZCMJSLX-UHFFFAOYSA-L 0.000 description 9
- 239000003792 electrolyte Substances 0.000 description 9
- AWJWCTOOIBYHON-UHFFFAOYSA-N furo[3,4-b]pyrazine-5,7-dione Chemical compound C1=CN=C2C(=O)OC(=O)C2=N1 AWJWCTOOIBYHON-UHFFFAOYSA-N 0.000 description 9
- -1 oxygen - chromic acid Chemical compound 0.000 description 9
- 238000007747 plating Methods 0.000 description 9
- 239000006260 foam Substances 0.000 description 7
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 6
- 229910052731 fluorine Inorganic materials 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 239000000080 wetting agent Substances 0.000 description 6
- 125000004432 carbon atom Chemical group C* 0.000 description 5
- 239000003595 mist Substances 0.000 description 5
- 239000007921 spray Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 4
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 4
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 4
- 238000000151 deposition Methods 0.000 description 4
- 239000011737 fluorine Substances 0.000 description 4
- 150000002500 ions Chemical class 0.000 description 4
- JHDXAQHGAJXNBY-UHFFFAOYSA-M 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonate;tetraethylazanium Chemical compound CC[N+](CC)(CC)CC.[O-]S(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F JHDXAQHGAJXNBY-UHFFFAOYSA-M 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- HNDRMMRAACCQKO-UHFFFAOYSA-M 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonate;tetramethylazanium Chemical compound C[N+](C)(C)C.[O-]S(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F HNDRMMRAACCQKO-UHFFFAOYSA-M 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- KMUONIBRACKNSN-UHFFFAOYSA-N potassium dichromate Chemical compound [K+].[K+].[O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O KMUONIBRACKNSN-UHFFFAOYSA-N 0.000 description 2
- NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 description 2
- 125000001453 quaternary ammonium group Chemical group 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 235000017557 sodium bicarbonate Nutrition 0.000 description 2
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- QZHDEAJFRJCDMF-UHFFFAOYSA-M 1,1,2,2,3,3,4,4,5,5,6,6,6-tridecafluorohexane-1-sulfonate Chemical compound [O-]S(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F QZHDEAJFRJCDMF-UHFFFAOYSA-M 0.000 description 1
- YFSUTJLHUFNCNZ-UHFFFAOYSA-M 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonate Chemical compound [O-]S(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F YFSUTJLHUFNCNZ-UHFFFAOYSA-M 0.000 description 1
- HYWZIAVPBSTISZ-UHFFFAOYSA-M 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-henicosafluorodecane-1-sulfonate Chemical compound [O-]S(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F HYWZIAVPBSTISZ-UHFFFAOYSA-M 0.000 description 1
- QLOKJRIVRGCVIM-UHFFFAOYSA-N 1-[(4-methylsulfanylphenyl)methyl]piperazine Chemical compound C1=CC(SC)=CC=C1CN1CCNCC1 QLOKJRIVRGCVIM-UHFFFAOYSA-N 0.000 description 1
- JHWIEAWILPSRMU-UHFFFAOYSA-N 2-methyl-3-pyrimidin-4-ylpropanoic acid Chemical compound OC(=O)C(C)CC1=CC=NC=N1 JHWIEAWILPSRMU-UHFFFAOYSA-N 0.000 description 1
- PQBAWAQIRZIWIV-UHFFFAOYSA-N N-methylpyridinium Chemical compound C[N+]1=CC=CC=C1 PQBAWAQIRZIWIV-UHFFFAOYSA-N 0.000 description 1
- VDRSDNINOSAWIV-UHFFFAOYSA-N [F].[Si] Chemical class [F].[Si] VDRSDNINOSAWIV-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- LXMQZGGLHVSEBA-UHFFFAOYSA-N chromium;trihydrate Chemical compound O.O.O.[Cr] LXMQZGGLHVSEBA-UHFFFAOYSA-N 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000004070 electrodeposition Methods 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 238000009713 electroplating Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000003682 fluorination reaction Methods 0.000 description 1
- 150000002222 fluorine compounds Chemical class 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 229910001506 inorganic fluoride Inorganic materials 0.000 description 1
- 230000002452 interceptive effect Effects 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- YNAVUWVOSKDBBP-UHFFFAOYSA-O morpholinium Chemical compound [H+].C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-O 0.000 description 1
- HTKPDYSCAPSXIR-UHFFFAOYSA-N octyltrimethylammonium ion Chemical compound CCCCCCCC[N+](C)(C)C HTKPDYSCAPSXIR-UHFFFAOYSA-N 0.000 description 1
- 150000002897 organic nitrogen compounds Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- YFSUTJLHUFNCNZ-UHFFFAOYSA-N perfluorooctane-1-sulfonic acid Chemical compound OS(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F YFSUTJLHUFNCNZ-UHFFFAOYSA-N 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- 235000003270 potassium fluoride Nutrition 0.000 description 1
- 239000011698 potassium fluoride Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical class O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- PXLIDIMHPNPGMH-UHFFFAOYSA-N sodium chromate Chemical compound [Na+].[Na+].[O-][Cr]([O-])(=O)=O PXLIDIMHPNPGMH-UHFFFAOYSA-N 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
- CBXCPBUEXACCNR-UHFFFAOYSA-N tetraethylammonium Chemical compound CC[N+](CC)(CC)CC CBXCPBUEXACCNR-UHFFFAOYSA-N 0.000 description 1
- TXEYQDLBPFQVAA-UHFFFAOYSA-N tetrafluoromethane Chemical group FC(F)(F)F TXEYQDLBPFQVAA-UHFFFAOYSA-N 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 231100000563 toxic property Toxicity 0.000 description 1
- BHOCBLDBJFCBQS-UHFFFAOYSA-N trifluoro(methyl)silane Chemical compound C[Si](F)(F)F BHOCBLDBJFCBQS-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/04—Electroplating: Baths therefor from solutions of chromium
- C25D3/10—Electroplating: Baths therefor from solutions of chromium characterised by the organic bath constituents used
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Electroplating Methods And Accessories (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2508708A DE2508708C2 (de) | 1975-02-28 | 1975-02-28 | Elektrolytlösungen auf Cr (VI)-Basis zur galvanischen Abscheidung von Chromschichten |
| US05/657,014 US4006064A (en) | 1975-02-28 | 1976-02-10 | Process for the electrodeposition of chrome plate using fluorine-containing wetting agents |
| GB7614/76A GB1529104A (en) | 1975-02-28 | 1976-02-26 | Process for the electrodeposition of chrome plate |
| JP1948676A JPS5543512B2 (index.php) | 1975-02-28 | 1976-02-26 | |
| IT48290/76A IT1056193B (it) | 1975-02-28 | 1976-02-26 | Procedimento per la cromatura galvanica con l impiego di agenti bagnanti contenenti fluoro |
| NLAANVRAGE7602066,A NL183200C (nl) | 1975-02-28 | 1976-02-27 | Werkwijze voor het vormen van een chroombekleding door elektrolytische afzetting, alsmede gevormd voortbrengsel voorzien van een elektrolytisch afgezette chroombekleding verkregen volgens deze werkwijze. |
| BE2054849A BE838991A (fr) | 1975-02-28 | 1976-02-27 | Procede pour le depot electrolytique d'un revetement de chrome en utilisant des agents mouillants fluores |
| FR7605671A FR2302354A1 (fr) | 1975-02-28 | 1976-02-27 | Proce |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2508708A DE2508708C2 (de) | 1975-02-28 | 1975-02-28 | Elektrolytlösungen auf Cr (VI)-Basis zur galvanischen Abscheidung von Chromschichten |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2508708A1 DE2508708A1 (de) | 1976-09-09 |
| DE2508708C2 true DE2508708C2 (de) | 1982-07-01 |
Family
ID=5940061
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2508708A Expired DE2508708C2 (de) | 1975-02-28 | 1975-02-28 | Elektrolytlösungen auf Cr (VI)-Basis zur galvanischen Abscheidung von Chromschichten |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4006064A (index.php) |
| JP (1) | JPS5543512B2 (index.php) |
| BE (1) | BE838991A (index.php) |
| DE (1) | DE2508708C2 (index.php) |
| FR (1) | FR2302354A1 (index.php) |
| GB (1) | GB1529104A (index.php) |
| IT (1) | IT1056193B (index.php) |
| NL (1) | NL183200C (index.php) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3723198A1 (de) * | 1987-07-14 | 1989-02-16 | Bayer Ag | Schaumhemmender zusatz in sauren beizen und galvanischen baedern |
| US4873020A (en) * | 1988-10-04 | 1989-10-10 | Minnesota Mining And Manufacturing Company | Fluorochemical surfactants and process for preparing same |
| US5478486A (en) * | 1993-11-18 | 1995-12-26 | Henkel Corporation | Composition and method for treating substrates to reduce electrostatic charge and resultant article |
| US5534192A (en) * | 1993-11-18 | 1996-07-09 | Henkel Corporation | Composition and method for treating substrates to reduce electrostatic charge and resultant article |
| EP1215304A1 (en) * | 2000-12-06 | 2002-06-19 | Lido Frediani | Two-layer chrome-plating process |
| WO2002059397A1 (de) * | 2001-01-23 | 2002-08-01 | Bolta-Werke Gmbh | Verfahren zur kontinuierlichen abscheidung eines nickelhaltigen belages auf einer metallfolie |
| DE102006025847A1 (de) * | 2006-06-02 | 2007-12-06 | Merck Patent Gmbh | Verwendung von Phosphinsäure in der Galvanotechnik |
| DE102011102052A1 (de) | 2011-05-19 | 2012-11-22 | Anke Gmbh & Co. Kg | Netzmittel für elektrolytische Anwendung und dessen Verwendung |
| ES2766775T3 (es) * | 2013-09-05 | 2020-06-15 | Macdermid Enthone Inc | Composición acuosa de electrolito que tiene una emisión aérea reducida |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2750334A (en) * | 1953-01-29 | 1956-06-12 | Udylite Res Corp | Electrodeposition of chromium |
| US2750335A (en) * | 1953-07-17 | 1956-06-12 | Udylite Res Corp | Chromium electrodeposition |
| US2846380A (en) * | 1956-05-07 | 1958-08-05 | Udylite Res Corp | Chromium electroplating |
| US3476753A (en) * | 1965-05-03 | 1969-11-04 | Minnesota Mining & Mfg | Tertiaryamino perfluoro alkylene sulfonic acid fluorides |
| US3432408A (en) * | 1966-08-03 | 1969-03-11 | Udylite Corp | Chromium plating electrolyte and method for preventing mist therein |
-
1975
- 1975-02-28 DE DE2508708A patent/DE2508708C2/de not_active Expired
-
1976
- 1976-02-10 US US05/657,014 patent/US4006064A/en not_active Expired - Lifetime
- 1976-02-26 IT IT48290/76A patent/IT1056193B/it active
- 1976-02-26 JP JP1948676A patent/JPS5543512B2/ja not_active Expired
- 1976-02-26 GB GB7614/76A patent/GB1529104A/en not_active Expired
- 1976-02-27 BE BE2054849A patent/BE838991A/xx not_active IP Right Cessation
- 1976-02-27 NL NLAANVRAGE7602066,A patent/NL183200C/xx not_active IP Right Cessation
- 1976-02-27 FR FR7605671A patent/FR2302354A1/fr active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| FR2302354B1 (index.php) | 1980-02-29 |
| DE2508708A1 (de) | 1976-09-09 |
| NL7602066A (nl) | 1976-08-31 |
| FR2302354A1 (fr) | 1976-09-24 |
| NL183200B (nl) | 1988-03-16 |
| US4006064A (en) | 1977-02-01 |
| GB1529104A (en) | 1978-10-18 |
| IT1056193B (it) | 1982-01-30 |
| BE838991A (fr) | 1976-08-27 |
| JPS5543512B2 (index.php) | 1980-11-06 |
| NL183200C (nl) | 1988-08-16 |
| JPS51110441A (index.php) | 1976-09-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| D2 | Grant after examination |