DE2419453A1 - Kontinuierliche herstellung basischer aluminiumnitratloesungen - Google Patents
Kontinuierliche herstellung basischer aluminiumnitratloesungenInfo
- Publication number
- DE2419453A1 DE2419453A1 DE2419453A DE2419453A DE2419453A1 DE 2419453 A1 DE2419453 A1 DE 2419453A1 DE 2419453 A DE2419453 A DE 2419453A DE 2419453 A DE2419453 A DE 2419453A DE 2419453 A1 DE2419453 A1 DE 2419453A1
- Authority
- DE
- Germany
- Prior art keywords
- aluminum
- aluminum nitrate
- reaction
- basic aluminum
- nitric acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical compound [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 title claims description 55
- 238000010924 continuous production Methods 0.000 title description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 60
- 238000006243 chemical reaction Methods 0.000 claims description 41
- 229910052782 aluminium Inorganic materials 0.000 claims description 37
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 31
- 229910017604 nitric acid Inorganic materials 0.000 claims description 31
- 238000000034 method Methods 0.000 claims description 24
- 239000000203 mixture Substances 0.000 claims description 21
- 238000004519 manufacturing process Methods 0.000 claims description 13
- 239000008187 granular material Substances 0.000 claims description 10
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 8
- 238000009835 boiling Methods 0.000 claims description 4
- 229910052742 iron Inorganic materials 0.000 claims description 4
- 229910052738 indium Inorganic materials 0.000 claims description 2
- 239000000243 solution Substances 0.000 description 54
- 239000007789 gas Substances 0.000 description 25
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 18
- 239000001257 hydrogen Substances 0.000 description 18
- 229910052739 hydrogen Inorganic materials 0.000 description 18
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 14
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical class Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 14
- 239000002253 acid Substances 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 230000015572 biosynthetic process Effects 0.000 description 7
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- 239000012495 reaction gas Substances 0.000 description 6
- 239000011521 glass Substances 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 229910002651 NO3 Inorganic materials 0.000 description 4
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 230000003247 decreasing effect Effects 0.000 description 4
- NHNBFGGVMKEFGY-UHFFFAOYSA-N nitrate group Chemical group [N+](=O)([O-])[O-] NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 230000029087 digestion Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000002360 explosive Substances 0.000 description 3
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 3
- 229920000642 polymer Polymers 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- -1 carboxylic acid aluminum hydroxide Chemical class 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000005189 flocculation Methods 0.000 description 2
- 230000016615 flocculation Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000002923 metal particle Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000004062 sedimentation Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000002912 waste gas Substances 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 150000007933 aliphatic carboxylic acids Chemical class 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000012267 brine Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- GPRLSGONYQIRFK-UHFFFAOYSA-N hydron Chemical compound [H+] GPRLSGONYQIRFK-UHFFFAOYSA-N 0.000 description 1
- 230000002706 hydrostatic effect Effects 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000001023 inorganic pigment Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- GQPLMRYTRLFLPF-UHFFFAOYSA-N nitrous oxide Inorganic materials [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/66—Nitrates, with or without other cations besides aluminium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Catalysts (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2419453A DE2419453A1 (de) | 1974-04-23 | 1974-04-23 | Kontinuierliche herstellung basischer aluminiumnitratloesungen |
| US05/563,761 US3983221A (en) | 1974-04-23 | 1975-03-31 | Production of basic aluminium nitrate solution |
| JP50047616A JPS50154197A (https=) | 1974-04-23 | 1975-04-21 | |
| BE155589A BE828160A (fr) | 1974-04-23 | 1975-04-21 | Production d'une solution de nitrate d'aluminium basique |
| IT49204/75A IT1035389B (it) | 1974-04-23 | 1975-04-21 | Procedimento ed apparecchiatura per produrre soluzioni di nitra to di allumino basico |
| GB16342/75A GB1498252A (en) | 1974-04-23 | 1975-04-21 | Production of basic aluminium nitrate solution |
| NL7504819A NL7504819A (nl) | 1974-04-23 | 1975-04-23 | Werkwijze voor het bereiden van basische aluminiumnitraatoplossingen. |
| FR7512683A FR2268751B1 (https=) | 1974-04-23 | 1975-04-23 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2419453A DE2419453A1 (de) | 1974-04-23 | 1974-04-23 | Kontinuierliche herstellung basischer aluminiumnitratloesungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2419453A1 true DE2419453A1 (de) | 1975-11-06 |
Family
ID=5913650
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2419453A Withdrawn DE2419453A1 (de) | 1974-04-23 | 1974-04-23 | Kontinuierliche herstellung basischer aluminiumnitratloesungen |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3983221A (https=) |
| JP (1) | JPS50154197A (https=) |
| BE (1) | BE828160A (https=) |
| DE (1) | DE2419453A1 (https=) |
| FR (1) | FR2268751B1 (https=) |
| GB (1) | GB1498252A (https=) |
| IT (1) | IT1035389B (https=) |
| NL (1) | NL7504819A (https=) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI241277B (en) * | 2001-03-29 | 2005-10-11 | Daicel Chem | Method for the production of the basic metal nitrate |
| TW200909354A (en) * | 2007-07-17 | 2009-03-01 | Grace W R & Co | Basic aluminum nitrate |
| CN112694108A (zh) * | 2019-10-23 | 2021-04-23 | 中国石油化工股份有限公司 | 连续制备铝溶胶的方法及其制备的铝溶胶 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2931706A (en) * | 1954-06-21 | 1960-04-05 | Alan T Gresky | Preparation of dibasic aluminum nitrate |
| US3340205A (en) * | 1965-05-25 | 1967-09-05 | Universal Oil Prod Co | Manufacture of high purity alumina sol from relatively low grade aluminum |
| US3535268A (en) * | 1968-06-10 | 1970-10-20 | Universal Oil Prod Co | Continuous process for manufacture of sols |
-
1974
- 1974-04-23 DE DE2419453A patent/DE2419453A1/de not_active Withdrawn
-
1975
- 1975-03-31 US US05/563,761 patent/US3983221A/en not_active Expired - Lifetime
- 1975-04-21 JP JP50047616A patent/JPS50154197A/ja active Pending
- 1975-04-21 IT IT49204/75A patent/IT1035389B/it active
- 1975-04-21 BE BE155589A patent/BE828160A/xx unknown
- 1975-04-21 GB GB16342/75A patent/GB1498252A/en not_active Expired
- 1975-04-23 FR FR7512683A patent/FR2268751B1/fr not_active Expired
- 1975-04-23 NL NL7504819A patent/NL7504819A/xx not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| JPS50154197A (https=) | 1975-12-11 |
| IT1035389B (it) | 1979-10-20 |
| NL7504819A (nl) | 1975-10-27 |
| FR2268751A1 (https=) | 1975-11-21 |
| US3983221A (en) | 1976-09-28 |
| GB1498252A (en) | 1978-01-18 |
| FR2268751B1 (https=) | 1981-08-07 |
| BE828160A (fr) | 1975-10-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| 8130 | Withdrawal |