DE2410612A1 - Verfahren zur reinigung und kohlenwasserstoffen - Google Patents
Verfahren zur reinigung und kohlenwasserstoffenInfo
- Publication number
- DE2410612A1 DE2410612A1 DE19742410612 DE2410612A DE2410612A1 DE 2410612 A1 DE2410612 A1 DE 2410612A1 DE 19742410612 DE19742410612 DE 19742410612 DE 2410612 A DE2410612 A DE 2410612A DE 2410612 A1 DE2410612 A1 DE 2410612A1
- Authority
- DE
- Germany
- Prior art keywords
- acid
- extraction
- hydrocarbons
- phosphoric acid
- ammonia
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 32
- 229930195733 hydrocarbon Natural products 0.000 title claims description 18
- 150000002430 hydrocarbons Chemical class 0.000 title claims description 18
- 238000004140 cleaning Methods 0.000 title claims description 8
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 28
- 238000000605 extraction Methods 0.000 claims description 17
- 239000002253 acid Substances 0.000 claims description 16
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 16
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 14
- 230000000813 microbial effect Effects 0.000 claims description 9
- 239000004215 Carbon black (E152) Substances 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 238000007670 refining Methods 0.000 claims description 8
- 229910021529 ammonia Inorganic materials 0.000 claims description 7
- 230000002255 enzymatic effect Effects 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 230000002378 acidificating effect Effects 0.000 claims description 6
- 239000004615 ingredient Substances 0.000 claims description 5
- 239000002904 solvent Substances 0.000 claims description 5
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 4
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 3
- 239000000194 fatty acid Substances 0.000 claims description 3
- 229930195729 fatty acid Natural products 0.000 claims description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- 150000004665 fatty acids Chemical class 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 238000000622 liquid--liquid extraction Methods 0.000 claims description 2
- 229910052757 nitrogen Inorganic materials 0.000 claims description 2
- 238000004064 recycling Methods 0.000 claims description 2
- 238000000638 solvent extraction Methods 0.000 claims description 2
- -1 fatty acids ammonium salts Chemical class 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 7
- 239000007795 chemical reaction product Substances 0.000 description 7
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 6
- 150000007513 acids Chemical class 0.000 description 6
- 239000013543 active substance Substances 0.000 description 6
- 229910052698 phosphorus Inorganic materials 0.000 description 6
- 239000011574 phosphorus Substances 0.000 description 6
- 239000003208 petroleum Substances 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 230000002503 metabolic effect Effects 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 229910019142 PO4 Inorganic materials 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 235000021317 phosphate Nutrition 0.000 description 3
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 238000005352 clarification Methods 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 238000000855 fermentation Methods 0.000 description 2
- 230000004151 fermentation Effects 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 230000004060 metabolic process Effects 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 230000007483 microbial process Effects 0.000 description 2
- 230000002906 microbiologic effect Effects 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 230000002411 adverse Effects 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 239000002283 diesel fuel Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 150000002902 organometallic compounds Chemical class 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 150000003018 phosphorus compounds Chemical class 0.000 description 1
- 230000010349 pulsation Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G32/00—Refining of hydrocarbon oils by electric or magnetic means, by irradiation, or by using microorganisms
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G21/00—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
- C10G21/06—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents characterised by the solvent used
- C10G21/12—Organic compounds only
- C10G21/24—Phosphorus-containing compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Microbiology (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DD17120273A DD103921A1 (enrdf_load_stackoverflow) | 1973-05-30 | 1973-05-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2410612A1 true DE2410612A1 (de) | 1975-01-09 |
Family
ID=5491438
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19742410612 Pending DE2410612A1 (de) | 1973-05-30 | 1974-03-06 | Verfahren zur reinigung und kohlenwasserstoffen |
Country Status (9)
| Country | Link |
|---|---|
| JP (1) | JPS5052281A (enrdf_load_stackoverflow) |
| BG (1) | BG23039A1 (enrdf_load_stackoverflow) |
| CS (1) | CS184891B1 (enrdf_load_stackoverflow) |
| DD (1) | DD103921A1 (enrdf_load_stackoverflow) |
| DE (1) | DE2410612A1 (enrdf_load_stackoverflow) |
| FR (1) | FR2231734B1 (enrdf_load_stackoverflow) |
| GB (1) | GB1453235A (enrdf_load_stackoverflow) |
| HU (1) | HU174687B (enrdf_load_stackoverflow) |
| RO (1) | RO63985A (enrdf_load_stackoverflow) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5829598U (ja) * | 1981-08-24 | 1983-02-25 | 石川島播磨重工業株式会社 | 水中超音波装置のトランスデユ−サ取付装置 |
-
1973
- 1973-05-30 DD DD17120273A patent/DD103921A1/xx unknown
-
1974
- 1974-03-06 DE DE19742410612 patent/DE2410612A1/de active Pending
- 1974-04-08 GB GB1540274A patent/GB1453235A/en not_active Expired
- 1974-04-16 JP JP4184674A patent/JPS5052281A/ja active Pending
- 1974-04-30 BG BG2657274A patent/BG23039A1/xx unknown
- 1974-05-01 RO RO7863474A patent/RO63985A/ro unknown
- 1974-05-21 CS CS363374A patent/CS184891B1/cs unknown
- 1974-05-30 HU HU74CE1002A patent/HU174687B/hu unknown
- 1974-05-30 FR FR7418833A patent/FR2231734B1/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DD103921A1 (enrdf_load_stackoverflow) | 1974-02-12 |
| CS184891B1 (en) | 1978-09-15 |
| JPS5052281A (enrdf_load_stackoverflow) | 1975-05-09 |
| RO63985A (fr) | 1978-08-15 |
| GB1453235A (en) | 1976-10-20 |
| BG23039A1 (enrdf_load_stackoverflow) | 1977-07-12 |
| FR2231734B1 (enrdf_load_stackoverflow) | 1978-01-13 |
| FR2231734A1 (enrdf_load_stackoverflow) | 1974-12-27 |
| HU174687B (hu) | 1980-03-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP0658183B1 (de) | Verfahren zur herstellung von fettsäureestern kurzkettiger einwertiger alkohole | |
| DE1767442C3 (de) | Kontinuierliches Verfahren zum Reinigen einer Rohphosphorsäureaufschlußlösung | |
| DE2138428C3 (de) | Verfahren zur gegebenenfalls gleichzeitigen Gewinnung von reinen n-Paraffinen und Mineralölen mit tiefem Stockpunkt | |
| DE2329480A1 (de) | Verfahren zur wiedergewinnung von saeuren aus waessrigen loesungen | |
| DE865140C (de) | Verfahren zum Fraktionieren von Gemischen organischer Verbindungen | |
| DE2637553C3 (de) | Verfahren zum Trennen von Öl-Wasser-Emulsionen | |
| EP0111801B1 (de) | Verfahren zur Reinigung von Nassverfahrensphosphorsäure | |
| DE2410612A1 (de) | Verfahren zur reinigung und kohlenwasserstoffen | |
| EP1576078B1 (de) | Verfahren zur kontinuierlichen herstellung von biomethanoldiesel | |
| DE2645777C2 (enrdf_load_stackoverflow) | ||
| DE2822303A1 (de) | Verfahren zur herstellung einer praktisch fluorfreien konzentrierten phosphorsaeureloesung | |
| DE2321882B2 (de) | Verfahren zum Reinigen einer rohen Phosphorsäurelösung | |
| DE2926943C2 (enrdf_load_stackoverflow) | ||
| DE2365883A1 (de) | Verfahren zur reinigung von durch nassaufschluss gewonnener phosphorsaeure | |
| DE3209183A1 (de) | Verfahren zur abtrennung von schwermetallverbindungen aus zwischenprodukten der fabrikation von phosphorduengemitteln | |
| DD103921B1 (de) | Verfahren zur Reinigung von Kohlenwasserstoffen | |
| DE1592085A1 (de) | Verfahren zum Reinigen von Magnesiumchloridsolen | |
| EP0184690A2 (de) | Verfahren zur Entarsenierung von phosphorsauren Lösungen | |
| DE2837694A1 (de) | Verfahren und extraktionsmittel zur herstellung von reiner phosphorsaeure | |
| DE579032C (de) | Verfahren zum Raffinieren von Erdoelprodukten | |
| DE4321023C1 (de) | Verfahren zur Gewinnung von Fettstoffen mit verbesserter Reinheit aus wäßrigen Emulsionen bzw. Dispersionen | |
| DE1811813B2 (de) | Kontinuierliches verfahren zum reinigen einer rohphosphorsaeureaufschlussloesung | |
| DE503201C (de) | Wiedergewinnung von Salpetersaeure aus diese enthaltenden Abwaessern | |
| DE2755248C2 (de) | Verfahren zur Herstellung eines Heizöls aus Kohlehydrierölen | |
| AT264545B (de) | Verfahren zur Herstellung von Äthan-1-hydroxy-1,1-diphosphonsäure und Salzen derselben |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHN | Withdrawal |