DE2356153A1 - Verfahren zur herstellung von schwermetallaziden und -styphnaten - Google Patents
Verfahren zur herstellung von schwermetallaziden und -styphnatenInfo
- Publication number
- DE2356153A1 DE2356153A1 DE2356153A DE2356153A DE2356153A1 DE 2356153 A1 DE2356153 A1 DE 2356153A1 DE 2356153 A DE2356153 A DE 2356153A DE 2356153 A DE2356153 A DE 2356153A DE 2356153 A1 DE2356153 A1 DE 2356153A1
- Authority
- DE
- Germany
- Prior art keywords
- reaction vessel
- heavy metal
- chambers
- crystals
- continuously
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 25
- 229910001385 heavy metal Inorganic materials 0.000 title claims description 16
- 238000004519 manufacturing process Methods 0.000 title description 13
- 238000006243 chemical reaction Methods 0.000 claims description 59
- 239000000243 solution Substances 0.000 claims description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- 150000001540 azides Chemical class 0.000 claims description 13
- 239000011521 glass Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 8
- 230000003746 surface roughness Effects 0.000 claims description 7
- 239000005388 borosilicate glass Substances 0.000 claims description 5
- 239000012266 salt solution Substances 0.000 claims description 4
- 229920006395 saturated elastomer Polymers 0.000 claims description 4
- 239000000126 substance Substances 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 claims description 2
- 239000013078 crystal Substances 0.000 description 42
- -1 alkali metal azide Chemical class 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- RLJMLMKIBZAXJO-UHFFFAOYSA-N lead nitrate Chemical compound [O-][N+](=O)O[Pb]O[N+]([O-])=O RLJMLMKIBZAXJO-UHFFFAOYSA-N 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- 238000009826 distribution Methods 0.000 description 4
- 238000004880 explosion Methods 0.000 description 4
- WETZJIOEDGMBMA-UHFFFAOYSA-L lead styphnate Chemical compound [Pb+2].[O-]C1=C([N+]([O-])=O)C=C([N+]([O-])=O)C([O-])=C1[N+]([O-])=O WETZJIOEDGMBMA-UHFFFAOYSA-L 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 3
- 238000013019 agitation Methods 0.000 description 3
- 238000010923 batch production Methods 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 230000008021 deposition Effects 0.000 description 3
- 229910052749 magnesium Inorganic materials 0.000 description 3
- 239000011777 magnesium Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 239000004698 Polyethylene Substances 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229920000573 polyethylene Polymers 0.000 description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- XFTQEBKVHOSOJT-UHFFFAOYSA-N [Mg+2].O[N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O Chemical compound [Mg+2].O[N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O XFTQEBKVHOSOJT-UHFFFAOYSA-N 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- SLGWESQGEUXWJQ-UHFFFAOYSA-N formaldehyde;phenol Chemical compound O=C.OC1=CC=CC=C1 SLGWESQGEUXWJQ-UHFFFAOYSA-N 0.000 description 1
- 239000012213 gelatinous substance Substances 0.000 description 1
- 231100001261 hazardous Toxicity 0.000 description 1
- 230000002706 hydrostatic effect Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 1
- 239000004926 polymethyl methacrylate Substances 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 239000005297 pyrex Substances 0.000 description 1
- 230000002393 scratching effect Effects 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 210000003462 vein Anatomy 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/08—Hydrazoic acid; Azides; Halogen azides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C247/00—Compounds containing azido groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Manufacture Of Alloys Or Alloy Compounds (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB5168072A GB1427338A (en) | 1972-11-09 | 1972-11-09 | Methods of manufacturing heavy metal azides and styphnates |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2356153A1 true DE2356153A1 (de) | 1974-06-12 |
Family
ID=10460980
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2356153A Pending DE2356153A1 (de) | 1972-11-09 | 1973-11-09 | Verfahren zur herstellung von schwermetallaziden und -styphnaten |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US3928405A (OSRAM) |
| JP (1) | JPS49133356A (OSRAM) |
| AR (1) | AR205698A1 (OSRAM) |
| AT (1) | AT335325B (OSRAM) |
| AU (1) | AU475639B2 (OSRAM) |
| BE (1) | BE806935A (OSRAM) |
| BR (1) | BR7308738D0 (OSRAM) |
| CH (1) | CH585670A5 (OSRAM) |
| DD (1) | DD109361A5 (OSRAM) |
| DE (1) | DE2356153A1 (OSRAM) |
| ES (1) | ES420405A1 (OSRAM) |
| FR (1) | FR2206271A1 (OSRAM) |
| GB (1) | GB1427338A (OSRAM) |
| HU (1) | HU167001B (OSRAM) |
| IE (1) | IE38410B1 (OSRAM) |
| IT (1) | IT999238B (OSRAM) |
| NL (1) | NL7315058A (OSRAM) |
| PH (1) | PH10929A (OSRAM) |
| RO (1) | RO65952A (OSRAM) |
| TR (1) | TR18165A (OSRAM) |
| ZA (1) | ZA738344B (OSRAM) |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1999728A (en) * | 1927-11-08 | 1935-04-30 | Remington Arms Co Inc | Manufacture of lead styphnate |
| US1942274A (en) * | 1931-10-19 | 1934-01-02 | Remington Arms Co Inc | Priming mixture |
| BE430296A (OSRAM) * | 1937-09-22 | |||
| US3770721A (en) * | 1956-02-09 | 1973-11-06 | Us Army | Direct production of beta hmx |
| US2927845A (en) * | 1956-05-15 | 1960-03-08 | Hercules Powder Co Ltd | Apparatus for manufacture of nitrocellulose |
| DE1593045A1 (de) * | 1966-07-02 | 1970-04-09 | Meissner Fa Josef | Verfahren und Vorrichtung zum zeitweiligen Abschalten der Produktion von Trinitrotoluol |
-
1972
- 1972-11-09 GB GB5168072A patent/GB1427338A/en not_active Expired
-
1973
- 1973-01-01 AR AR250869A patent/AR205698A1/es active
- 1973-10-09 ES ES420405A patent/ES420405A1/es not_active Expired
- 1973-10-24 IE IE1905/73A patent/IE38410B1/xx unknown
- 1973-10-26 US US410092A patent/US3928405A/en not_active Expired - Lifetime
- 1973-10-29 ZA ZA738344*A patent/ZA738344B/xx unknown
- 1973-10-30 AU AU61978/73A patent/AU475639B2/en not_active Expired
- 1973-11-02 NL NL7315058A patent/NL7315058A/xx unknown
- 1973-11-05 BE BE137426A patent/BE806935A/xx unknown
- 1973-11-06 IT IT30977/73A patent/IT999238B/it active
- 1973-11-06 HU HUIE595A patent/HU167001B/hu unknown
- 1973-11-08 DD DD174620A patent/DD109361A5/xx unknown
- 1973-11-08 TR TR18165A patent/TR18165A/xx unknown
- 1973-11-08 FR FR7339682A patent/FR2206271A1/fr not_active Withdrawn
- 1973-11-08 BR BR8738/73A patent/BR7308738D0/pt unknown
- 1973-11-09 AT AT947773A patent/AT335325B/de not_active IP Right Cessation
- 1973-11-09 DE DE2356153A patent/DE2356153A1/de active Pending
- 1973-11-09 RO RO7376590A patent/RO65952A/ro unknown
- 1973-11-09 PH PH15208A patent/PH10929A/en unknown
- 1973-11-09 JP JP48125574A patent/JPS49133356A/ja active Pending
- 1973-11-09 CH CH1575573A patent/CH585670A5/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| BE806935A (fr) | 1974-05-06 |
| AR205698A1 (es) | 1976-05-31 |
| FR2206271A1 (OSRAM) | 1974-06-07 |
| BR7308738D0 (pt) | 1974-08-22 |
| CH585670A5 (OSRAM) | 1977-03-15 |
| JPS49133356A (OSRAM) | 1974-12-21 |
| RO65952A (ro) | 1980-07-15 |
| PH10929A (en) | 1977-10-05 |
| ES420405A1 (es) | 1976-07-01 |
| ZA738344B (en) | 1974-10-30 |
| AT335325B (de) | 1977-03-10 |
| GB1427338A (en) | 1976-03-10 |
| NL7315058A (OSRAM) | 1974-05-13 |
| TR18165A (tr) | 1976-10-11 |
| IE38410B1 (en) | 1978-03-01 |
| ATA947773A (de) | 1976-06-15 |
| IE38410L (en) | 1974-05-09 |
| US3928405A (en) | 1975-12-23 |
| DD109361A5 (OSRAM) | 1974-11-05 |
| IT999238B (it) | 1976-02-20 |
| AU475639B2 (en) | 1976-08-26 |
| HU167001B (OSRAM) | 1975-07-28 |
| AU6197873A (en) | 1975-05-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHJ | Non-payment of the annual fee |