DE2343026A1 - Verfahren zur herstellung waessriger alkalipolysilikatloesungen - Google Patents
Verfahren zur herstellung waessriger alkalipolysilikatloesungenInfo
- Publication number
- DE2343026A1 DE2343026A1 DE19732343026 DE2343026A DE2343026A1 DE 2343026 A1 DE2343026 A1 DE 2343026A1 DE 19732343026 DE19732343026 DE 19732343026 DE 2343026 A DE2343026 A DE 2343026A DE 2343026 A1 DE2343026 A1 DE 2343026A1
- Authority
- DE
- Germany
- Prior art keywords
- solution
- water
- added
- content
- alcohol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 28
- 238000002360 preparation method Methods 0.000 title claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 34
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims description 24
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 19
- 229910052744 lithium Inorganic materials 0.000 claims description 19
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 14
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 14
- 239000007787 solid Substances 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 12
- 239000003513 alkali Substances 0.000 claims description 10
- 229910001854 alkali hydroxide Inorganic materials 0.000 claims description 9
- 238000004821 distillation Methods 0.000 claims description 7
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 claims description 7
- 229910052708 sodium Inorganic materials 0.000 claims description 6
- 229910052700 potassium Inorganic materials 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 3
- 239000003973 paint Substances 0.000 claims description 3
- 239000011541 reaction mixture Substances 0.000 claims description 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 2
- 239000011230 binding agent Substances 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 238000000576 coating method Methods 0.000 claims description 2
- 229910052725 zinc Inorganic materials 0.000 claims 1
- 239000011701 zinc Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 description 58
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 18
- 229910004298 SiO 2 Inorganic materials 0.000 description 16
- 238000006243 chemical reaction Methods 0.000 description 12
- 229910018068 Li 2 O Inorganic materials 0.000 description 7
- 150000002500 ions Chemical class 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- 239000011734 sodium Substances 0.000 description 7
- 239000000203 mixture Substances 0.000 description 6
- 239000007788 liquid Substances 0.000 description 4
- 239000000725 suspension Substances 0.000 description 4
- 239000007966 viscous suspension Substances 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- -1 lithium silicates Chemical class 0.000 description 2
- 239000011591 potassium Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 150000004760 silicates Chemical class 0.000 description 2
- 239000002023 wood Substances 0.000 description 2
- 241000261585 Hadrobregmus pertinax Species 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
- 239000006004 Quartz sand Substances 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 1
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000011083 clear filtration Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 150000002641 lithium Chemical class 0.000 description 1
- HPGPEWYJWRWDTP-UHFFFAOYSA-N lithium peroxide Chemical compound [Li+].[Li+].[O-][O-] HPGPEWYJWRWDTP-UHFFFAOYSA-N 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 150000004702 methyl esters Chemical class 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- 229910001414 potassium ion Inorganic materials 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
- C09D1/02—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/32—Alkali metal silicates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/02—Polysilicates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/02—Polysilicates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Polymers & Plastics (AREA)
- Medicinal Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Silicon Compounds (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Priority Applications (18)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19732343026 DE2343026A1 (de) | 1973-08-25 | 1973-08-25 | Verfahren zur herstellung waessriger alkalipolysilikatloesungen |
| SE7407623A SE7407623L (https=) | 1973-08-25 | 1974-06-10 | |
| AU70555/74A AU487697B2 (en) | 1973-08-25 | 1974-06-27 | Alkali metal polysilicate solutions and process for their production |
| DD180338A DD113737A5 (https=) | 1973-08-25 | 1974-08-05 | |
| NO742824A NO742824L (https=) | 1973-08-25 | 1974-08-05 | |
| ZA00745152A ZA745152B (en) | 1973-08-25 | 1974-08-12 | A process for the production of aqueous alkali poysilicate solutions |
| US05/496,778 US3984526A (en) | 1973-08-25 | 1974-08-12 | Method of manufacturing aqueous solutions of alkali polysilicates |
| YU02275/74A YU227574A (en) | 1973-08-25 | 1974-08-20 | Process for preparing aqueous solutions of alkali polysilicates |
| BE147777A BE819040A (fr) | 1973-08-25 | 1974-08-21 | Procede de fabrication de solutions aqueuses de polysilicates alcalins |
| JP49096036A JPS5051100A (https=) | 1973-08-25 | 1974-08-21 | |
| FR7428843A FR2241494B1 (https=) | 1973-08-25 | 1974-08-22 | |
| FI2474/74A FI247474A7 (https=) | 1973-08-25 | 1974-08-22 | |
| GB3724074A GB1468565A (en) | 1973-08-25 | 1974-08-23 | Aqueous solutions of alkali metal polysilicates |
| NL7411261A NL7411261A (nl) | 1973-08-25 | 1974-08-23 | Werkwijze voor het bereiden van waterige alkali- polysilicaatoplossingen. |
| IT52720/74A IT1019095B (it) | 1973-08-25 | 1974-08-23 | Procedimento per la produzionedi soluzioni acquose di polisilicati alcalini |
| DK451774A DK451774A (https=) | 1973-08-25 | 1974-08-23 | |
| ES429514A ES429514A1 (es) | 1973-08-25 | 1974-08-24 | Procedimiento para la preparacion de soluciones acuosas de polisilicatos de metales alcalinos. |
| US05/748,603 US4120938A (en) | 1973-08-25 | 1976-07-08 | Aqueous solutions of alkali polysilicates |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19732343026 DE2343026A1 (de) | 1973-08-25 | 1973-08-25 | Verfahren zur herstellung waessriger alkalipolysilikatloesungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2343026A1 true DE2343026A1 (de) | 1975-03-06 |
Family
ID=5890737
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19732343026 Pending DE2343026A1 (de) | 1973-08-25 | 1973-08-25 | Verfahren zur herstellung waessriger alkalipolysilikatloesungen |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US3984526A (https=) |
| JP (1) | JPS5051100A (https=) |
| BE (1) | BE819040A (https=) |
| DD (1) | DD113737A5 (https=) |
| DE (1) | DE2343026A1 (https=) |
| DK (1) | DK451774A (https=) |
| ES (1) | ES429514A1 (https=) |
| FI (1) | FI247474A7 (https=) |
| FR (1) | FR2241494B1 (https=) |
| GB (1) | GB1468565A (https=) |
| IT (1) | IT1019095B (https=) |
| NL (1) | NL7411261A (https=) |
| NO (1) | NO742824L (https=) |
| SE (1) | SE7407623L (https=) |
| YU (1) | YU227574A (https=) |
| ZA (1) | ZA745152B (https=) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4120938A (en) * | 1973-08-25 | 1978-10-17 | Dynamit Nobel Aktiengesellschaft | Aqueous solutions of alkali polysilicates |
| US4297163A (en) * | 1980-01-07 | 1981-10-27 | Pq Corporation | Drying of potassium silicate |
| CA2009035A1 (en) * | 1989-01-31 | 1990-07-31 | Rudolf Novotny | Process for hydrothermal production of sodium silicate solutions |
| GB9424711D0 (en) * | 1994-12-07 | 1995-02-01 | Alcan Int Ltd | Composition for surface treatment |
| RU2170213C1 (ru) * | 2000-11-09 | 2001-07-10 | Шабанова Надежда Антоновна | Способ получения полисиликатов калия |
| KR101450346B1 (ko) * | 2006-03-15 | 2014-10-14 | 알이에스씨 인베스트먼츠 엘엘씨 | 태양 전지 및 다른 용도를 위한 규소 제조 방법 |
| EP2216371A1 (de) * | 2009-02-07 | 2010-08-11 | Cognis IP Management GmbH | Lösemittelfreie wasserlösliche Silan modifizierte Silikate |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2047614A (en) * | 1932-07-09 | 1936-07-14 | Cavezzale Candido | Production of alkali metal silicates |
| US3180747A (en) * | 1961-08-03 | 1965-04-27 | Exxon Research Engineering Co | Protective coating |
| US3459500A (en) * | 1964-11-27 | 1969-08-05 | Exxon Research Engineering Co | Novel lithium silicate compositions and process for producing same |
| US3392039A (en) * | 1964-12-17 | 1968-07-09 | Philadelphia Quartz Company Of | Lithium silicate composition |
| DE1567585C3 (de) * | 1966-11-30 | 1975-12-18 | Henkel & Cie Gmbh, 4000 Duesseldorf | Verfahren zur Herstellung von Lithiumsilikatlösungen |
-
1973
- 1973-08-25 DE DE19732343026 patent/DE2343026A1/de active Pending
-
1974
- 1974-06-10 SE SE7407623A patent/SE7407623L/xx unknown
- 1974-08-05 NO NO742824A patent/NO742824L/no unknown
- 1974-08-05 DD DD180338A patent/DD113737A5/xx unknown
- 1974-08-12 US US05/496,778 patent/US3984526A/en not_active Expired - Lifetime
- 1974-08-12 ZA ZA00745152A patent/ZA745152B/xx unknown
- 1974-08-20 YU YU02275/74A patent/YU227574A/xx unknown
- 1974-08-21 JP JP49096036A patent/JPS5051100A/ja active Pending
- 1974-08-21 BE BE147777A patent/BE819040A/xx unknown
- 1974-08-22 FR FR7428843A patent/FR2241494B1/fr not_active Expired
- 1974-08-22 FI FI2474/74A patent/FI247474A7/fi unknown
- 1974-08-23 GB GB3724074A patent/GB1468565A/en not_active Expired
- 1974-08-23 NL NL7411261A patent/NL7411261A/xx not_active Application Discontinuation
- 1974-08-23 IT IT52720/74A patent/IT1019095B/it active
- 1974-08-23 DK DK451774A patent/DK451774A/da unknown
- 1974-08-24 ES ES429514A patent/ES429514A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DK451774A (https=) | 1975-04-28 |
| ES429514A1 (es) | 1976-09-01 |
| US3984526A (en) | 1976-10-05 |
| FR2241494B1 (https=) | 1978-06-09 |
| NL7411261A (nl) | 1975-02-27 |
| BE819040A (fr) | 1974-12-16 |
| FI247474A7 (https=) | 1975-02-26 |
| ZA745152B (en) | 1975-08-27 |
| IT1019095B (it) | 1977-11-10 |
| FR2241494A1 (https=) | 1975-03-21 |
| NO742824L (https=) | 1975-03-24 |
| DD113737A5 (https=) | 1975-06-20 |
| SE7407623L (https=) | 1975-02-26 |
| GB1468565A (en) | 1977-03-30 |
| JPS5051100A (https=) | 1975-05-07 |
| AU7055574A (en) | 1976-01-08 |
| YU227574A (en) | 1982-05-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHJ | Non-payment of the annual fee |