DE2249893C3 - Verfahren zur Herstellung von Hydraziniumazid - Google Patents
Verfahren zur Herstellung von HydraziniumazidInfo
- Publication number
- DE2249893C3 DE2249893C3 DE19722249893 DE2249893A DE2249893C3 DE 2249893 C3 DE2249893 C3 DE 2249893C3 DE 19722249893 DE19722249893 DE 19722249893 DE 2249893 A DE2249893 A DE 2249893A DE 2249893 C3 DE2249893 C3 DE 2249893C3
- Authority
- DE
- Germany
- Prior art keywords
- hydrazoic acid
- solution
- azide
- aqueous
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- UZXHZRFWCCZBDW-UHFFFAOYSA-O aminoazanium;azide Chemical compound [NH3+]N.[N-]=[N+]=[N-] UZXHZRFWCCZBDW-UHFFFAOYSA-O 0.000 title claims description 11
- 238000000034 method Methods 0.000 title claims description 6
- JUINSXZKUKVTMD-UHFFFAOYSA-N hydrogen azide Chemical compound N=[N+]=[N-] JUINSXZKUKVTMD-UHFFFAOYSA-N 0.000 claims description 25
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 claims description 18
- 239000000243 solution Substances 0.000 claims description 17
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 12
- 239000011261 inert gas Substances 0.000 claims description 7
- 229910052757 nitrogen Inorganic materials 0.000 claims description 6
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 5
- 150000001540 azides Chemical class 0.000 claims description 5
- 239000003729 cation exchange resin Substances 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 239000007789 gas Substances 0.000 claims description 4
- 229910052751 metal Inorganic materials 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 4
- 239000001257 hydrogen Substances 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims description 3
- 239000001307 helium Substances 0.000 claims description 2
- 229910052734 helium Inorganic materials 0.000 claims description 2
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims description 2
- 229930195734 saturated hydrocarbon Natural products 0.000 claims description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 8
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 6
- 239000012535 impurity Substances 0.000 description 5
- PXIPVTKHYLBLMZ-UHFFFAOYSA-N Sodium azide Chemical compound [Na+].[N-]=[N+]=[N-] PXIPVTKHYLBLMZ-UHFFFAOYSA-N 0.000 description 4
- 239000011347 resin Substances 0.000 description 4
- 229920005989 resin Polymers 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000003421 catalytic decomposition reaction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- -1 hydrazinium azide Chemical class 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical compound C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- TZLVRPLSVNESQC-UHFFFAOYSA-N potassium azide Chemical compound [K+].[N-]=[N+]=[N-] TZLVRPLSVNESQC-UHFFFAOYSA-N 0.000 description 1
- 238000012552 review Methods 0.000 description 1
- 239000002760 rocket fuel Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- FISGLHSNQHXMGY-UHFFFAOYSA-N sodium;aminoazanide Chemical compound [Na+].[NH-]N FISGLHSNQHXMGY-UHFFFAOYSA-N 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/08—Hydrazoic acid; Azides; Halogen azides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/16—Hydrazine; Salts thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7139101A FR2158732A5 (enExample) | 1971-10-29 | 1971-10-29 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2249893A1 DE2249893A1 (de) | 1973-05-10 |
| DE2249893B2 DE2249893B2 (de) | 1979-01-04 |
| DE2249893C3 true DE2249893C3 (de) | 1979-08-30 |
Family
ID=9085141
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19722249893 Expired DE2249893C3 (de) | 1971-10-29 | 1972-10-11 | Verfahren zur Herstellung von Hydraziniumazid |
Country Status (8)
| Country | Link |
|---|---|
| JP (1) | JPS5315480B2 (enExample) |
| BE (1) | BE789426A (enExample) |
| CA (1) | CA978331A (enExample) |
| DE (1) | DE2249893C3 (enExample) |
| FR (1) | FR2158732A5 (enExample) |
| GB (1) | GB1367824A (enExample) |
| IT (1) | IT975398B (enExample) |
| NL (1) | NL7214087A (enExample) |
-
0
- BE BE789426D patent/BE789426A/xx unknown
-
1971
- 1971-10-29 FR FR7139101A patent/FR2158732A5/fr not_active Expired
-
1972
- 1972-10-11 DE DE19722249893 patent/DE2249893C3/de not_active Expired
- 1972-10-18 NL NL7214087A patent/NL7214087A/xx not_active Application Discontinuation
- 1972-10-23 CA CA154,577A patent/CA978331A/en not_active Expired
- 1972-10-27 GB GB4970172A patent/GB1367824A/en not_active Expired
- 1972-10-27 IT IT7039872A patent/IT975398B/it active
- 1972-10-28 JP JP10764172A patent/JPS5315480B2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE2249893B2 (de) | 1979-01-04 |
| NL7214087A (enExample) | 1973-05-02 |
| JPS5315480B2 (enExample) | 1978-05-25 |
| CA978331A (en) | 1975-11-25 |
| FR2158732A5 (enExample) | 1973-06-15 |
| DE2249893A1 (de) | 1973-05-10 |
| JPS4851898A (enExample) | 1973-07-20 |
| GB1367824A (en) | 1974-09-25 |
| BE789426A (fr) | 1973-01-15 |
| IT975398B (it) | 1974-07-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| EHJ | Ceased/non-payment of the annual fee |