DE2213083A1 - Elektroden für elektrochemische Verfahren - Google Patents
Elektroden für elektrochemische VerfahrenInfo
- Publication number
- DE2213083A1 DE2213083A1 DE19722213083 DE2213083A DE2213083A1 DE 2213083 A1 DE2213083 A1 DE 2213083A1 DE 19722213083 DE19722213083 DE 19722213083 DE 2213083 A DE2213083 A DE 2213083A DE 2213083 A1 DE2213083 A1 DE 2213083A1
- Authority
- DE
- Germany
- Prior art keywords
- metal
- film
- layer
- oxide
- platinum group
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 238000000034 method Methods 0.000 title claims description 21
- 239000002184 metal Substances 0.000 claims description 37
- 229910052751 metal Inorganic materials 0.000 claims description 36
- 238000000576 coating method Methods 0.000 claims description 24
- 239000011248 coating agent Substances 0.000 claims description 23
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 18
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 15
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical group [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 15
- 229910044991 metal oxide Inorganic materials 0.000 claims description 14
- 150000004706 metal oxides Chemical class 0.000 claims description 14
- 125000000217 alkyl group Chemical group 0.000 claims description 12
- 229910052719 titanium Inorganic materials 0.000 claims description 12
- 239000010936 titanium Substances 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 10
- 150000002739 metals Chemical class 0.000 claims description 10
- 150000001875 compounds Chemical class 0.000 claims description 9
- 239000004408 titanium dioxide Substances 0.000 claims description 9
- -1 alkyl titanate Chemical compound 0.000 claims description 8
- 150000002894 organic compounds Chemical class 0.000 claims description 8
- 230000001590 oxidative effect Effects 0.000 claims description 6
- 229910052736 halogen Inorganic materials 0.000 claims description 5
- 150000002367 halogens Chemical class 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims description 4
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims description 4
- 229910052794 bromium Inorganic materials 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 238000001704 evaporation Methods 0.000 claims description 4
- 229910052731 fluorine Inorganic materials 0.000 claims description 4
- 239000011737 fluorine Substances 0.000 claims description 4
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims description 3
- 229910001069 Ti alloy Inorganic materials 0.000 claims description 3
- 229910052801 chlorine Inorganic materials 0.000 claims description 3
- 239000000460 chlorine Substances 0.000 claims description 3
- 230000008020 evaporation Effects 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 230000010287 polarization Effects 0.000 claims description 3
- 230000001131 transforming effect Effects 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 2
- 239000003638 chemical reducing agent Substances 0.000 claims description 2
- 238000005868 electrolysis reaction Methods 0.000 claims description 2
- 229910001092 metal group alloy Inorganic materials 0.000 claims 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 2
- 150000002736 metal compounds Chemical class 0.000 claims 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims 1
- 241000130764 Tinea Species 0.000 claims 1
- 208000002474 Tinea Diseases 0.000 claims 1
- 239000004927 clay Substances 0.000 claims 1
- 238000001035 drying Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 claims 1
- 229910052709 silver Inorganic materials 0.000 claims 1
- 239000004332 silver Substances 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- 239000010410 layer Substances 0.000 description 19
- 239000003973 paint Substances 0.000 description 11
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 8
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 6
- YBCAZPLXEGKKFM-UHFFFAOYSA-K ruthenium(iii) chloride Chemical compound [Cl-].[Cl-].[Cl-].[Ru+3] YBCAZPLXEGKKFM-UHFFFAOYSA-K 0.000 description 3
- 239000011780 sodium chloride Substances 0.000 description 3
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 150000004820 halides Chemical class 0.000 description 2
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 2
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 2
- 229910052753 mercury Inorganic materials 0.000 description 2
- 235000006408 oxalic acid Nutrition 0.000 description 2
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 description 1
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 description 1
- 229910000497 Amalgam Inorganic materials 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- RRKGBEPNZRCDAP-UHFFFAOYSA-N [C].[Ag] Chemical compound [C].[Ag] RRKGBEPNZRCDAP-UHFFFAOYSA-N 0.000 description 1
- 229910001514 alkali metal chloride Inorganic materials 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 125000001246 bromo group Chemical group Br* 0.000 description 1
- FPCJKVGGYOAWIZ-UHFFFAOYSA-N butan-1-ol;titanium Chemical compound [Ti].CCCCO.CCCCO.CCCCO.CCCCO FPCJKVGGYOAWIZ-UHFFFAOYSA-N 0.000 description 1
- 125000001309 chloro group Chemical group Cl* 0.000 description 1
- YVZQFSNXOYLGMJ-UHFFFAOYSA-L chloro(2-hydroxyethyl)mercury;1-hexadecylpyridin-1-ium;bromide Chemical compound [Br-].OCC[Hg]Cl.CCCCCCCCCCCCCCCC[N+]1=CC=CC=C1 YVZQFSNXOYLGMJ-UHFFFAOYSA-L 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910052741 iridium Inorganic materials 0.000 description 1
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 description 1
- 229930007744 linalool Natural products 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- 239000010948 rhodium Substances 0.000 description 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
- 229910052707 ruthenium Inorganic materials 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
- C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
- C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
- C25B11/073—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material
- C25B11/091—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of at least one catalytic element and at least one catalytic compound; consisting of two or more catalytic elements or catalytic compounds
- C25B11/093—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of at least one catalytic element and at least one catalytic compound; consisting of two or more catalytic elements or catalytic compounds at least one noble metal or noble metal oxide and at least one non-noble metal oxide
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/50—Fuel cells
Landscapes
- Chemical & Material Sciences (AREA)
- Electrochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Electrodes For Compound Or Non-Metal Manufacture (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Electrolytic Production Of Metals (AREA)
- Inert Electrodes (AREA)
- Secondary Cells (AREA)
- Chemically Coating (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB721171 | 1971-03-18 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2213083A1 true DE2213083A1 (de) | 1972-09-21 |
Family
ID=9828761
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19722213083 Ceased DE2213083A1 (de) | 1971-03-18 | 1972-03-17 | Elektroden für elektrochemische Verfahren |
Country Status (21)
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3793164A (en) * | 1973-04-19 | 1974-02-19 | Diamond Shamrock Corp | High current density brine electrolysis |
| JPS5137877A (en) * | 1974-09-27 | 1976-03-30 | Asahi Chemical Ind | Denkaiyodenkyoku oyobi sonoseizoho |
| FR2289632A1 (fr) * | 1974-10-29 | 1976-05-28 | Marston Excelsior Ltd | Procede de realisation d'electrodes pour operations electrolytiques |
| US3969216A (en) * | 1974-12-27 | 1976-07-13 | Doreen Veronica Barrett | Flotation separation |
| US4112140A (en) * | 1977-04-14 | 1978-09-05 | The Dow Chemical Company | Electrode coating process |
| US4214971A (en) * | 1978-08-14 | 1980-07-29 | The Dow Chemical Company | Electrode coating process |
| US4331528A (en) * | 1980-10-06 | 1982-05-25 | Diamond Shamrock Corporation | Coated metal electrode with improved barrier layer |
| JPS582175A (ja) * | 1981-06-27 | 1983-01-07 | フジテック株式会社 | エレベ−タの制御装置 |
| US4871703A (en) * | 1983-05-31 | 1989-10-03 | The Dow Chemical Company | Process for preparation of an electrocatalyst |
| US4615913A (en) * | 1984-03-13 | 1986-10-07 | Kaman Sciences Corporation | Multilayered chromium oxide bonded, hardened and densified coatings and method of making same |
| IL73536A (en) * | 1984-09-13 | 1987-12-20 | Eltech Systems Corp | Composite catalytic material particularly for electrolysis electrodes,its manufacture and its use in electrolysis |
| EP0174413A1 (en) * | 1984-09-17 | 1986-03-19 | Eltech Systems Corporation | Composite catalytic material particularly for electrolysis electrodes and method of manufacture |
| US6000982A (en) * | 1995-07-31 | 1999-12-14 | Casio Computer Co., Ltd. | Method of manufacturing a cold-cathode for a discharge device |
| US5707715A (en) * | 1996-08-29 | 1998-01-13 | L. Pierre deRochemont | Metal ceramic composites with improved interfacial properties and methods to make such composites |
| US6323549B1 (en) * | 1996-08-29 | 2001-11-27 | L. Pierre deRochemont | Ceramic composite wiring structures for semiconductor devices and method of manufacture |
| US6143432A (en) * | 1998-01-09 | 2000-11-07 | L. Pierre deRochemont | Ceramic composites with improved interfacial properties and methods to make such composites |
| US7247229B2 (en) * | 1999-06-28 | 2007-07-24 | Eltech Systems Corporation | Coatings for the inhibition of undesirable oxidation in an electrochemical cell |
| KR100407710B1 (ko) * | 2001-11-08 | 2003-12-01 | (주) 테크윈 | 고온 소결에 의한 촉매성 산화물 전극의 제조방법 |
| US8022004B2 (en) * | 2008-05-24 | 2011-09-20 | Freeport-Mcmoran Corporation | Multi-coated electrode and method of making |
| CN102443818B (zh) | 2010-10-08 | 2016-01-13 | 水之星公司 | 多层混合金属氧化物电极及其制造方法 |
| ITMI20102354A1 (it) * | 2010-12-22 | 2012-06-23 | Industrie De Nora Spa | Elettrodo per cella elettrolitica |
| CN104005047B (zh) * | 2014-06-11 | 2017-02-15 | 中国船舶重工集团公司第七二五研究所 | 新型的电解低温海水防污用混合金属氧化物电极 |
| CN106099047A (zh) * | 2016-08-25 | 2016-11-09 | 深圳市贝特瑞纳米科技有限公司 | 一种电极材料的表面包覆方法及其用途 |
| US11668017B2 (en) | 2018-07-30 | 2023-06-06 | Water Star, Inc. | Current reversal tolerant multilayer material, method of making the same, use as an electrode, and use in electrochemical processes |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1195871A (en) * | 1967-02-10 | 1970-06-24 | Chemnor Ag | Improvements in or relating to the Manufacture of Electrodes. |
| GB1246447A (en) * | 1967-09-26 | 1971-09-15 | Imp Metal Ind Kynoch Ltd | Improvements in or relating to the manufacture of oxide-coated electrodes for use in electrolytic processes |
| US3616445A (en) * | 1967-12-14 | 1971-10-26 | Electronor Corp | Titanium or tantalum base electrodes with applied titanium or tantalum oxide face activated with noble metals or noble metal oxides |
| GB1206863A (en) * | 1968-04-02 | 1970-09-30 | Ici Ltd | Electrodes for electrochemical process |
| US3562008A (en) * | 1968-10-14 | 1971-02-09 | Ppg Industries Inc | Method for producing a ruthenium coated titanium electrode |
| GB1327760A (en) * | 1969-12-22 | 1973-08-22 | Imp Metal Ind Kynoch Ltd | Electrodes |
| GB1294373A (en) * | 1970-03-18 | 1972-10-25 | Ici Ltd | Electrodes for electrochemical processes |
| US3711385A (en) * | 1970-09-25 | 1973-01-16 | Chemnor Corp | Electrode having platinum metal oxide coating thereon,and method of use thereof |
| US3684543A (en) * | 1970-11-19 | 1972-08-15 | Patricia J Barbato | Recoating of electrodes |
-
1971
- 1971-03-18 GB GB721171*[A patent/GB1352872A/en not_active Expired
-
1972
- 1972-03-06 NO NO707/72A patent/NO140235C/no unknown
- 1972-03-06 ZA ZA721481A patent/ZA721481B/xx unknown
- 1972-03-10 AU AU39853/72A patent/AU463572B2/en not_active Expired
- 1972-03-12 IL IL38958A patent/IL38958A/xx unknown
- 1972-03-14 AR AR240928A patent/AR194834A1/es active
- 1972-03-15 TR TR17134A patent/TR17134A/xx unknown
- 1972-03-16 BE BE780756A patent/BE780756A/xx not_active IP Right Cessation
- 1972-03-17 CH CH396672A patent/CH578625A5/xx not_active IP Right Cessation
- 1972-03-17 BR BR1555/72A patent/BR7201555D0/pt unknown
- 1972-03-17 CA CA137,422A patent/CA976505A/en not_active Expired
- 1972-03-17 NL NL7203580A patent/NL7203580A/xx active Search and Examination
- 1972-03-17 DD DD161624A patent/DD99934A5/xx unknown
- 1972-03-17 JP JP2659972A patent/JPS559471B1/ja active Pending
- 1972-03-17 IT IT7222049A patent/IT950343B/it active
- 1972-03-17 DE DE19722213083 patent/DE2213083A1/de not_active Ceased
- 1972-03-17 FR FR7209511A patent/FR2130419B1/fr not_active Expired
- 1972-03-18 ES ES400915A patent/ES400915A1/es not_active Expired
- 1972-03-20 AT AT235172A patent/AT312633B/de not_active IP Right Cessation
-
1973
- 1973-09-04 US US394394A patent/US3869312A/en not_active Expired - Lifetime
-
1974
- 1974-12-31 MY MY1974318A patent/MY7400318A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| AT312633B (de) | 1974-01-10 |
| NO140235B (no) | 1979-04-17 |
| IT950343B (it) | 1973-06-20 |
| TR17134A (tr) | 1974-04-25 |
| ES400915A1 (es) | 1975-01-16 |
| AU3985372A (en) | 1973-09-13 |
| CA976505A (en) | 1975-10-21 |
| IL38958A0 (en) | 1972-05-30 |
| FR2130419A1 (enrdf_load_stackoverflow) | 1972-11-03 |
| NO140235C (no) | 1984-02-14 |
| CH578625A5 (enrdf_load_stackoverflow) | 1976-08-13 |
| FR2130419B1 (enrdf_load_stackoverflow) | 1974-08-02 |
| BR7201555D0 (pt) | 1973-06-14 |
| US3869312A (en) | 1975-03-04 |
| AR194834A1 (es) | 1973-08-24 |
| GB1352872A (en) | 1974-05-15 |
| JPS559471B1 (enrdf_load_stackoverflow) | 1980-03-10 |
| ZA721481B (en) | 1972-11-29 |
| DD99934A5 (enrdf_load_stackoverflow) | 1973-09-05 |
| MY7400318A (en) | 1974-12-31 |
| IL38958A (en) | 1974-12-31 |
| BE780756A (en) | 1972-09-18 |
| AU463572B2 (en) | 1975-07-14 |
| NL7203580A (enrdf_load_stackoverflow) | 1972-09-20 |
| JPS4733076A (enrdf_load_stackoverflow) | 1972-11-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| 8131 | Rejection |