DE2146753A1 - Verfahren zur herstellung von emulgatorhaltigen kunststoffpulvern auf der basis von polyvinylchlorid oder vinylchlorid-copolymerisat - Google Patents
Verfahren zur herstellung von emulgatorhaltigen kunststoffpulvern auf der basis von polyvinylchlorid oder vinylchlorid-copolymerisatInfo
- Publication number
- DE2146753A1 DE2146753A1 DE2146753A DE2146753A DE2146753A1 DE 2146753 A1 DE2146753 A1 DE 2146753A1 DE 2146753 A DE2146753 A DE 2146753A DE 2146753 A DE2146753 A DE 2146753A DE 2146753 A1 DE2146753 A1 DE 2146753A1
- Authority
- DE
- Germany
- Prior art keywords
- dispersion
- spray
- emulsifier
- weight
- september
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 239000000843 powder Substances 0.000 title claims description 28
- 238000000034 method Methods 0.000 title claims description 24
- 229920000915 polyvinyl chloride Polymers 0.000 title claims description 21
- 239000004800 polyvinyl chloride Substances 0.000 title claims description 21
- 229920003023 plastic Polymers 0.000 title claims description 7
- 239000004033 plastic Substances 0.000 title claims description 7
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 title claims description 5
- 238000004519 manufacturing process Methods 0.000 title description 10
- 239000006185 dispersion Substances 0.000 claims description 44
- 239000007921 spray Substances 0.000 claims description 23
- 238000001694 spray drying Methods 0.000 claims description 7
- 229920000642 polymer Polymers 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims 1
- 239000003995 emulsifying agent Substances 0.000 description 13
- 230000008719 thickening Effects 0.000 description 10
- 229920001944 Plastisol Polymers 0.000 description 7
- 239000004999 plastisol Substances 0.000 description 7
- MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 description 6
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 description 6
- 239000007787 solid Substances 0.000 description 6
- 238000000889 atomisation Methods 0.000 description 5
- 229920001577 copolymer Polymers 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000012530 fluid Substances 0.000 description 4
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 2
- 229940045714 alkyl sulfonate alkylating agent Drugs 0.000 description 2
- 125000005227 alkyl sulfonate group Chemical group 0.000 description 2
- 150000008052 alkyl sulfonates Chemical class 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- MOTZDAYCYVMXPC-UHFFFAOYSA-N dodecyl hydrogen sulfate Chemical compound CCCCCCCCCCCCOS(O)(=O)=O MOTZDAYCYVMXPC-UHFFFAOYSA-N 0.000 description 2
- 238000007720 emulsion polymerization reaction Methods 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 239000002649 leather substitute Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000012216 screening Methods 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 description 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 150000008051 alkyl sulfates Chemical class 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 238000009750 centrifugal casting Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- POULHZVOKOAJMA-UHFFFAOYSA-M dodecanoate Chemical compound CCCCCCCCCCCC([O-])=O POULHZVOKOAJMA-UHFFFAOYSA-M 0.000 description 1
- YRIUSKIDOIARQF-UHFFFAOYSA-N dodecyl benzenesulfonate Chemical compound CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 YRIUSKIDOIARQF-UHFFFAOYSA-N 0.000 description 1
- 229940071161 dodecylbenzenesulfonate Drugs 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229940070765 laurate Drugs 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000010327 methods by industry Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000001175 rotational moulding Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
- C08J3/122—Pulverisation by spraying
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2327/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers
- C08J2327/02—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment
- C08J2327/04—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment containing chlorine atoms
- C08J2327/06—Homopolymers or copolymers of vinyl chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Glanulating (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2146753A DE2146753A1 (de) | 1971-09-18 | 1971-09-18 | Verfahren zur herstellung von emulgatorhaltigen kunststoffpulvern auf der basis von polyvinylchlorid oder vinylchlorid-copolymerisat |
| FR7231433A FR2153919A5 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1971-09-18 | 1972-09-05 | |
| US288972A US3883494A (en) | 1971-09-18 | 1972-09-14 | Process for the preparation of emulsifier-containing polyvinyl chloride or vinyl chloride copolymer powders |
| JP47091827A JPS4867341A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1971-09-18 | 1972-09-14 | |
| IT52756/72A IT965359B (it) | 1971-09-18 | 1972-09-15 | Procedimento per la produzione di polveri di materie plastiche viniliche ed ugello per realizzarlo |
| BR006416/72A BR7206416D0 (pt) | 1971-09-18 | 1972-09-15 | Processo para a fabricacao de materiais sinteticos em pocontendo emulsionantes a base de cloreto de polivinila ou copolimero de cloreto de polivinila ou copolimero de cloreto de vinila e bocal de dupla entrada para a execucao do processo |
| US00307946A US3805869A (en) | 1971-09-18 | 1972-11-20 | Apparatus for the preparation of emulsifier-containing polyvinyl chloride or vinyl chloride copolymer powders |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2146753A DE2146753A1 (de) | 1971-09-18 | 1971-09-18 | Verfahren zur herstellung von emulgatorhaltigen kunststoffpulvern auf der basis von polyvinylchlorid oder vinylchlorid-copolymerisat |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2146753A1 true DE2146753A1 (de) | 1973-03-29 |
| DE2146753B2 DE2146753B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1974-05-22 |
Family
ID=5819979
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2146753A Ceased DE2146753A1 (de) | 1971-09-18 | 1971-09-18 | Verfahren zur herstellung von emulgatorhaltigen kunststoffpulvern auf der basis von polyvinylchlorid oder vinylchlorid-copolymerisat |
Country Status (6)
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS49126749A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1973-04-06 | 1974-12-04 | ||
| US4229249A (en) * | 1976-05-12 | 1980-10-21 | A/S Niro Atomizer | Production of a powder of polyvinylchloride or a vinylchloride copolymerizate suitable for producing plastisols |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3993857A (en) * | 1973-09-27 | 1976-11-23 | Chemische Werke Huls Aktiengesellschaft | Method for preparing synthetic powders based on polyvinyl chloride or vinyl chloride copolymers |
| JPS5947685B2 (ja) * | 1974-03-05 | 1984-11-21 | 鐘淵化学工業株式会社 | 塩化ビニル共重合体の製造方法 |
| DE2531780C3 (de) * | 1975-07-16 | 1980-02-07 | Chemische Werke Huels Ag, 4370 Marl | Verfahren zur Herstellung von verpastbaren Polymeren des Vinylchlorids |
| DE2541013C3 (de) * | 1975-09-13 | 1980-12-18 | Chemische Werke Huels Ag, 4370 Marl | Verfahren zur Nachbehandlung von verpastbaren Polymerisaten des Vinylchlorids |
| DE2543823C2 (de) * | 1975-10-01 | 1982-10-21 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur Herstellung von Polymeren des Vinylchlorids |
| JPS5290565A (en) * | 1976-01-26 | 1977-07-29 | Dainippon Toryo Kk | Process for producing resin powder |
| DE2650331C3 (de) * | 1976-11-03 | 1981-05-07 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur Herstellung von zur Plastisolbereitung geeigneten Pulvern auf der Grundlage von Polyvinylchlorid |
| JPS53132057A (en) * | 1977-04-22 | 1978-11-17 | Dainippon Toryo Co Ltd | Manufacture of powdered resin |
| DE2736645C2 (de) * | 1977-08-13 | 1982-06-09 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur Herstellung von zur Extruder- oder Kalanderverarbeitung geeigneten Pulvern auf der Grundlage von Polyvinylchlorid |
| DE3009148A1 (de) * | 1980-03-10 | 1981-10-08 | Wacker-Chemie GmbH, 8000 München | Carboxylgruppenmodifiziertes vinylchlorid-emulsionspolymerisat, verfahren zu seiner herstellung und seine verwendung |
| EP0596426B1 (en) * | 1992-11-04 | 1997-03-12 | Mitsubishi Chemical Corporation | Method for producing a vinyl chloride resin |
| EP0635544B1 (en) * | 1993-07-23 | 1997-09-24 | Mitsubishi Chemical Corporation | Granular vinyl chloride resin composition and process for its production |
| EP1059312B1 (en) * | 1998-01-27 | 2006-10-04 | Shin Dai-Ichi Vinyl Corporation | Process for producing granules of a polyvinylchloride resin for the preparation of paste |
| WO2007052911A1 (en) * | 2005-10-31 | 2007-05-10 | Lg Chem, Ltd. | Method of preparing vinylchloride-based resin capable of producing plastisol with low viscosity, vinylchloride-based resin prepared using the method, method of preparing vinylchloride-based plastisol, and vinylchloride-based plastisol prepared using the method |
| JP6043278B2 (ja) | 2010-04-09 | 2016-12-14 | パシラ ファーマシューティカルズ インコーポレーテッド | 多小胞リポソームを作製するための方法、大直径合成膜小胞を調製するための方法、および蒸発装置 |
| JP5850544B2 (ja) * | 2011-02-28 | 2016-02-03 | イェア プロセス エンジニアリング アグシャセルスガーッブＧＥＡ Ｐｒｏｃｅｓｓ Ｅｎｇｉｎｅｅｒｉｎｇ Ａ／Ｓ | スプレー乾燥装置 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2187877A (en) * | 1936-06-19 | 1940-01-23 | Carbide & Carbon Chem Corp | Process for spray drying thermoplastic resins |
| US2556260A (en) * | 1946-08-12 | 1951-06-12 | Celanese Corp | Process for coagulating polymer emulsions and recovering spherical particles |
| US2721859A (en) * | 1954-08-16 | 1955-10-25 | Us Rubber Co | Spray-drying process for making plastisol grade vinyl chloride polymers |
| BE590645A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1959-05-09 | |||
| US3198773A (en) * | 1962-09-13 | 1965-08-03 | Allied Chemicals Corp | Large size vinyl chloride polymer particles from emulsion latex |
-
1971
- 1971-09-18 DE DE2146753A patent/DE2146753A1/de not_active Ceased
-
1972
- 1972-09-05 FR FR7231433A patent/FR2153919A5/fr not_active Expired
- 1972-09-14 JP JP47091827A patent/JPS4867341A/ja active Pending
- 1972-09-14 US US288972A patent/US3883494A/en not_active Expired - Lifetime
- 1972-09-15 BR BR006416/72A patent/BR7206416D0/pt unknown
- 1972-09-15 IT IT52756/72A patent/IT965359B/it active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS49126749A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1973-04-06 | 1974-12-04 | ||
| US4229249A (en) * | 1976-05-12 | 1980-10-21 | A/S Niro Atomizer | Production of a powder of polyvinylchloride or a vinylchloride copolymerizate suitable for producing plastisols |
Also Published As
| Publication number | Publication date |
|---|---|
| BR7206416D0 (pt) | 1973-08-30 |
| FR2153919A5 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1973-05-04 |
| US3883494A (en) | 1975-05-13 |
| DE2146753B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1974-05-22 |
| IT965359B (it) | 1974-01-31 |
| JPS4867341A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1973-09-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8235 | Patent refused |