DE2013216A1 - Verfahren zur Herstellung von Phosphorpentafluorid - Google Patents
Verfahren zur Herstellung von PhosphorpentafluoridInfo
- Publication number
- DE2013216A1 DE2013216A1 DE19702013216 DE2013216A DE2013216A1 DE 2013216 A1 DE2013216 A1 DE 2013216A1 DE 19702013216 DE19702013216 DE 19702013216 DE 2013216 A DE2013216 A DE 2013216A DE 2013216 A1 DE2013216 A1 DE 2013216A1
- Authority
- DE
- Germany
- Prior art keywords
- fluoride
- phosphorus pentafluoride
- sulfur trioxide
- phosphorus
- phosphoryl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- OBCUTHMOOONNBS-UHFFFAOYSA-N phosphorus pentafluoride Chemical compound FP(F)(F)(F)F OBCUTHMOOONNBS-UHFFFAOYSA-N 0.000 title claims description 22
- 238000000034 method Methods 0.000 title claims description 18
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 claims description 29
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 11
- 229910000040 hydrogen fluoride Inorganic materials 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 11
- FFUQCRZBKUBHQT-UHFFFAOYSA-N phosphoryl fluoride Chemical compound FP(F)(F)=O FFUQCRZBKUBHQT-UHFFFAOYSA-N 0.000 claims description 10
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 239000007795 chemical reaction product Substances 0.000 claims description 5
- FYGKVENAJHIGPN-UHFFFAOYSA-N S(=O)(=O)=O.P(=O)(F)(F)F Chemical compound S(=O)(=O)=O.P(=O)(F)(F)F FYGKVENAJHIGPN-UHFFFAOYSA-N 0.000 claims description 3
- VVRKSAMWBNJDTH-UHFFFAOYSA-N difluorophosphane Chemical compound FPF VVRKSAMWBNJDTH-UHFFFAOYSA-N 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 claims 1
- 239000000835 fiber Substances 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 150000004820 halides Chemical class 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- CQXADFVORZEARL-UHFFFAOYSA-N Rilmenidine Chemical compound C1CC1C(C1CC1)NC1=NCCO1 CQXADFVORZEARL-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000010494 dissociation reaction Methods 0.000 description 1
- 230000005593 dissociations Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- UQSQSQZYBQSBJZ-UHFFFAOYSA-N fluorosulfonic acid Chemical compound OS(F)(=O)=O UQSQSQZYBQSBJZ-UHFFFAOYSA-N 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 125000005843 halogen group Chemical group 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- WKFBZNUBXWCCHG-UHFFFAOYSA-N phosphorus trifluoride Chemical compound FP(F)F WKFBZNUBXWCCHG-UHFFFAOYSA-N 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003797 solvolysis reaction Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/10—Halides or oxyhalides of phosphorus
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB01527/70A GB1287202A (en) | 1970-03-10 | 1970-03-10 | Process for the manufacture of phosphorous pentafluoride |
| FR7009645A FR2082501A5 (enExample) | 1970-03-10 | 1970-03-18 | |
| DE19702013216 DE2013216A1 (de) | 1970-03-10 | 1970-03-19 | Verfahren zur Herstellung von Phosphorpentafluorid |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB01527/70A GB1287202A (en) | 1970-03-10 | 1970-03-10 | Process for the manufacture of phosphorous pentafluoride |
| FR7009645A FR2082501A5 (enExample) | 1970-03-10 | 1970-03-18 | |
| DE19702013216 DE2013216A1 (de) | 1970-03-10 | 1970-03-19 | Verfahren zur Herstellung von Phosphorpentafluorid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2013216A1 true DE2013216A1 (de) | 1971-10-07 |
Family
ID=27182481
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19702013216 Pending DE2013216A1 (de) | 1970-03-10 | 1970-03-19 | Verfahren zur Herstellung von Phosphorpentafluorid |
Country Status (3)
| Country | Link |
|---|---|
| DE (1) | DE2013216A1 (enExample) |
| FR (1) | FR2082501A5 (enExample) |
| GB (1) | GB1287202A (enExample) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN120057872B (zh) * | 2025-04-29 | 2025-07-15 | 池州天赐高新材料有限公司 | 一种以二氟磷酸为原料合成五氟化磷的方法 |
-
1970
- 1970-03-10 GB GB01527/70A patent/GB1287202A/en not_active Expired
- 1970-03-18 FR FR7009645A patent/FR2082501A5/fr not_active Expired
- 1970-03-19 DE DE19702013216 patent/DE2013216A1/de active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| FR2082501A5 (enExample) | 1971-12-10 |
| GB1287202A (en) | 1972-08-31 |
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