DE192530C - - Google Patents

Info

Publication number

DE192530C

DE192530C DE1906192530D DE192530DA DE192530C DE 192530 C DE192530 C DE 192530C DE 1906192530 D DE1906192530 D DE 1906192530D DE 192530D A DE192530D A DE 192530DA DE 192530 C DE192530 C DE 192530C

Authority

DE

Germany

Prior art keywords

aryl

dye

blue

dyes

sulfur

Prior art date

1906-10-03

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired - Lifetime

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• 239000002253 acid Substances 0.000 claims description 5
• 238000000034 method Methods 0.000 claims description 3
• 229920001021 polysulfide Polymers 0.000 claims description 3
• 239000000988 sulfur dye Substances 0.000 claims description 3
• DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
• 150000007513 acids Chemical class 0.000 claims description 2
• 125000003118 aryl group Chemical group 0.000 claims description 2
• -1 aryl sulfoderivatives of aminooxydiphenylamine Chemical class 0.000 claims description 2
• 239000011734 sodium Substances 0.000 claims description 2
• 229910052708 sodium Inorganic materials 0.000 claims description 2
• 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 claims description 2
• 229910052500 inorganic mineral Inorganic materials 0.000 claims 1
• 239000011707 mineral Substances 0.000 claims 1
• 239000000975 dye Substances 0.000 description 10
• 239000000047 product Substances 0.000 description 5
• 239000000243 solution Substances 0.000 description 5
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
• 229920000742 Cotton Polymers 0.000 description 4
• QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
• 150000001875 compounds Chemical class 0.000 description 3
• GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 3
• NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
• 230000001476 alcoholic effect Effects 0.000 description 2
• CTYRPMDGLDAWRQ-UHFFFAOYSA-N phenyl hydrogen sulfate Chemical compound OS(=O)(=O)OC1=CC=CC=C1 CTYRPMDGLDAWRQ-UHFFFAOYSA-N 0.000 description 2
• 239000002244 precipitate Substances 0.000 description 2
• 238000002360 preparation method Methods 0.000 description 2
• 239000011593 sulfur Substances 0.000 description 2
• 229910052717 sulfur Inorganic materials 0.000 description 2
• RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
• 241000189705 Dunedin group Species 0.000 description 1
• CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
• BNOODXBBXFZASF-UHFFFAOYSA-N [Na].[S] Chemical compound [Na].[S] BNOODXBBXFZASF-UHFFFAOYSA-N 0.000 description 1
• 230000002378 acidificating effect Effects 0.000 description 1
• 239000003513 alkali Substances 0.000 description 1
• 239000007864 aqueous solution Substances 0.000 description 1
• 238000004040 coloring Methods 0.000 description 1
• 230000006378 damage Effects 0.000 description 1
• 238000001035 drying Methods 0.000 description 1
• 238000004043 dyeing Methods 0.000 description 1
• 238000001914 filtration Methods 0.000 description 1
• 239000013067 intermediate product Substances 0.000 description 1
• 239000012452 mother liquor Substances 0.000 description 1
• 239000005077 polysulfide Substances 0.000 description 1
• 150000008117 polysulfides Polymers 0.000 description 1
• 238000010992 reflux Methods 0.000 description 1
• 238000007086 side reaction Methods 0.000 description 1
• ORFSSYGWXNGVFB-UHFFFAOYSA-N sodium 4-amino-6-[[4-[4-[(8-amino-1-hydroxy-5,7-disulfonaphthalen-2-yl)diazenyl]-3-methoxyphenyl]-2-methoxyphenyl]diazenyl]-5-hydroxynaphthalene-1,3-disulfonic acid Chemical compound COC1=C(C=CC(=C1)C2=CC(=C(C=C2)N=NC3=C(C4=C(C=C3)C(=CC(=C4N)S(=O)(=O)O)S(=O)(=O)O)O)OC)N=NC5=C(C6=C(C=C5)C(=CC(=C6N)S(=O)(=O)O)S(=O)(=O)O)O.[Na+] ORFSSYGWXNGVFB-UHFFFAOYSA-N 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• 238000005406 washing Methods 0.000 description 1