DE1642980B1 - Verfahren zum veraschen von radioaktive stoffe enthaltenden fluorhaltigen organischen fluessigkeiten - Google Patents
Verfahren zum veraschen von radioaktive stoffe enthaltenden fluorhaltigen organischen fluessigkeitenInfo
- Publication number
- DE1642980B1 DE1642980B1 DE19671642980 DE1642980A DE1642980B1 DE 1642980 B1 DE1642980 B1 DE 1642980B1 DE 19671642980 DE19671642980 DE 19671642980 DE 1642980 A DE1642980 A DE 1642980A DE 1642980 B1 DE1642980 B1 DE 1642980B1
- Authority
- DE
- Germany
- Prior art keywords
- alkaline earth
- metal
- magnesium salt
- liquid
- hydrofluoric acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000007788 liquid Substances 0.000 title claims description 29
- 238000000034 method Methods 0.000 title claims description 21
- 239000012857 radioactive material Substances 0.000 title 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 38
- 229910052731 fluorine Inorganic materials 0.000 claims description 22
- 239000011737 fluorine Substances 0.000 claims description 22
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 21
- 238000002485 combustion reaction Methods 0.000 claims description 10
- 159000000003 magnesium salts Chemical class 0.000 claims description 10
- NDWWLJQHOLSEHX-UHFFFAOYSA-L calcium;octanoate Chemical compound [Ca+2].CCCCCCCC([O-])=O.CCCCCCCC([O-])=O NDWWLJQHOLSEHX-UHFFFAOYSA-L 0.000 claims description 9
- 239000000567 combustion gas Substances 0.000 claims description 9
- 229910052751 metal Inorganic materials 0.000 claims description 7
- 239000002184 metal Substances 0.000 claims description 7
- 238000006386 neutralization reaction Methods 0.000 claims description 7
- 239000000344 soap Substances 0.000 claims description 6
- 150000002894 organic compounds Chemical class 0.000 claims description 5
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 4
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 3
- 229930195729 fatty acid Natural products 0.000 claims description 3
- 239000000194 fatty acid Substances 0.000 claims description 3
- 150000004665 fatty acids Chemical class 0.000 claims description 3
- 239000000941 radioactive substance Substances 0.000 claims description 3
- 229910001512 metal fluoride Inorganic materials 0.000 claims description 2
- -1 organic compound Calcium phenate Chemical class 0.000 claims description 2
- 239000003960 organic solvent Substances 0.000 claims description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- 239000011777 magnesium Substances 0.000 claims 1
- 150000002989 phenols Chemical class 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 description 9
- 239000011575 calcium Substances 0.000 description 9
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 8
- 239000003921 oil Substances 0.000 description 8
- 239000007789 gas Substances 0.000 description 5
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 description 3
- 229910001634 calcium fluoride Inorganic materials 0.000 description 3
- ZMRQTIAUOLVKOX-UHFFFAOYSA-L calcium;diphenoxide Chemical compound [Ca+2].[O-]C1=CC=CC=C1.[O-]C1=CC=CC=C1 ZMRQTIAUOLVKOX-UHFFFAOYSA-L 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 238000000137 annealing Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- TXBBUSUXYMIVOS-UHFFFAOYSA-N thenoyltrifluoroacetone Chemical compound FC(F)(F)C(=O)CC(=O)C1=CC=CS1 TXBBUSUXYMIVOS-UHFFFAOYSA-N 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229910004261 CaF 2 Inorganic materials 0.000 description 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 239000003849 aromatic solvent Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000010425 asbestos Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 159000000007 calcium salts Chemical class 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- OMRRUNXAWXNVFW-UHFFFAOYSA-N fluoridochlorine Chemical compound ClF OMRRUNXAWXNVFW-UHFFFAOYSA-N 0.000 description 1
- 125000001153 fluoro group Chemical group F* 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- FHFHPENPORXWHG-UHFFFAOYSA-N magnesium;phenol Chemical class [Mg].OC1=CC=CC=C1 FHFHPENPORXWHG-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 1
- 239000011824 nuclear material Substances 0.000 description 1
- 125000005474 octanoate group Chemical group 0.000 description 1
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical class C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000002285 radioactive effect Effects 0.000 description 1
- 238000003303 reheating Methods 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
- 238000007127 saponification reaction Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 150000003871 sulfonates Chemical class 0.000 description 1
- JOHWNGGYGAVMGU-UHFFFAOYSA-N trifluorochlorine Chemical compound FCl(F)F JOHWNGGYGAVMGU-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000004056 waste incineration Methods 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21F—PROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT; TREATING RADIOACTIVELY CONTAMINATED MATERIAL; DECONTAMINATION ARRANGEMENTS THEREFOR
- G21F9/00—Treating radioactively contaminated material; Decontamination arrangements therefor
- G21F9/04—Treating liquids
- G21F9/06—Processing
- G21F9/14—Processing by incineration; by calcination, e.g. desiccation
Landscapes
- Physics & Mathematics (AREA)
- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- High Energy & Nuclear Physics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fire-Extinguishing Compositions (AREA)
- Treating Waste Gases (AREA)
- Gasification And Melting Of Waste (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR73048A FR1495622A (fr) | 1966-08-12 | 1966-08-12 | Procédé d'incinération de liquides organiques fluorés |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1642980B1 true DE1642980B1 (de) | 1971-12-30 |
Family
ID=8615383
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19671642980 Withdrawn DE1642980B1 (de) | 1966-08-12 | 1967-08-08 | Verfahren zum veraschen von radioaktive stoffe enthaltenden fluorhaltigen organischen fluessigkeiten |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3483128A (https=) |
| BE (1) | BE701716A (https=) |
| CH (1) | CH480865A (https=) |
| DE (1) | DE1642980B1 (https=) |
| ES (1) | ES344068A1 (https=) |
| FR (1) | FR1495622A (https=) |
| GB (1) | GB1181132A (https=) |
| LU (1) | LU54292A1 (https=) |
| NL (1) | NL6711025A (https=) |
| SE (1) | SE314154B (https=) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2061935A5 (en) * | 1969-10-03 | 1971-06-25 | Commissariat Energie Atomique | Liquid organic phosphorus compounds burntwit |
| US3666673A (en) * | 1969-12-24 | 1972-05-30 | Atomic Energy Commission | Method of disposing of radioactive organic waste solutions |
| US4154811A (en) * | 1977-10-06 | 1979-05-15 | The Dow Chemical Company | Method for producing hydrohalic acids in a diesel engine |
| DE2855650C2 (de) * | 1978-12-22 | 1984-10-25 | Nukem Gmbh, 6450 Hanau | Verfahren zur pyrohydrolytischen Zersetzung von Phosphor enthaltenden, mit hochangereichertem Uran kontaminierten Flüssigkeiten |
| DE3028193C2 (de) * | 1980-07-25 | 1984-11-22 | Nukem Gmbh, 6450 Hanau | Verfahren und Vorrichtung zur pyrolytischen Zersetzung von Halogene und/oder Phosphor enthaltenden organischen Substanzen |
| DE3840565A1 (de) * | 1988-08-15 | 1990-02-22 | Ruhrkohle Ag | Verfahren zur hydrierung von organochlorverbindungen und neutralisation des anfallenden chlorwasserstoffs sowie neutralisationsmittel fuer aus organochlorverbindungen anfallenden chlorwasserstoff |
| EP0371201A1 (de) * | 1988-12-01 | 1990-06-06 | Ruhrkohle Aktiengesellschaft | Verfahren zur Hydrierung von Organochlorverbindungen und Neutralisation des anfallenden Chlorwasserstoffs sowie Neutralisationsmittel für aus Organochlorverbindungen anfallenden Clorwasserstoff |
| US5276251A (en) * | 1990-01-17 | 1994-01-04 | Mitsubishi Nuclear Fuel Co. | Process for treating organic phosphoric acids |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3196619A (en) * | 1961-04-19 | 1965-07-27 | Continental Oil Co | Method for disposing of harmful organic waste materials |
| US3120493A (en) * | 1962-04-27 | 1964-02-04 | Walter E Clark | Suppression of ruthenium volatilization in evaporation and calcination of radioactive waste solutions |
| US3330088A (en) * | 1964-12-23 | 1967-07-11 | Jr John V Dunlea | Method of bulk rubbish disposal |
| US3265627A (en) * | 1965-03-04 | 1966-08-09 | Walter E Clark | Addition of lithium values in conversion of fission-product wastes to a glass-like solid for disposal |
-
1966
- 1966-08-12 FR FR73048A patent/FR1495622A/fr not_active Expired
-
1967
- 1967-07-24 BE BE701716D patent/BE701716A/xx not_active IP Right Cessation
- 1967-07-27 GB GB34678/67A patent/GB1181132A/en not_active Expired
- 1967-07-31 US US657029A patent/US3483128A/en not_active Expired - Lifetime
- 1967-08-08 DE DE19671642980 patent/DE1642980B1/de not_active Withdrawn
- 1967-08-10 NL NL6711025A patent/NL6711025A/xx unknown
- 1967-08-10 LU LU54292D patent/LU54292A1/xx unknown
- 1967-08-10 CH CH1125567A patent/CH480865A/fr not_active IP Right Cessation
- 1967-08-11 SE SE11376/67A patent/SE314154B/xx unknown
- 1967-08-12 ES ES344068A patent/ES344068A1/es not_active Expired
Non-Patent Citations (1)
| Title |
|---|
| None * |
Also Published As
| Publication number | Publication date |
|---|---|
| FR1495622A (fr) | 1967-09-22 |
| BE701716A (https=) | 1968-01-02 |
| SE314154B (https=) | 1969-09-01 |
| CH480865A (fr) | 1969-11-15 |
| NL6711025A (https=) | 1968-02-13 |
| LU54292A1 (https=) | 1967-10-10 |
| GB1181132A (en) | 1970-02-11 |
| US3483128A (en) | 1969-12-09 |
| ES344068A1 (es) | 1969-11-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| E77 | Valid patent as to the heymanns-index 1977 | ||
| 8339 | Ceased/non-payment of the annual fee |