DE149748C - - Google Patents
Info
- Publication number
- DE149748C DE149748C DENDAT149748D DE149748DA DE149748C DE 149748 C DE149748 C DE 149748C DE NDAT149748 D DENDAT149748 D DE NDAT149748D DE 149748D A DE149748D A DE 149748DA DE 149748 C DE149748 C DE 149748C
- Authority
- DE
- Germany
- Prior art keywords
- melts
- found
- ferric chloride
- amino
- nitrobenzaldehyde
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims description 3
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 5
- 239000000155 melt Substances 0.000 description 4
- BMYNFMYTOJXKLE-UHFFFAOYSA-N 3-azaniumyl-2-hydroxypropanoate Chemical compound NCC(O)C(O)=O BMYNFMYTOJXKLE-UHFFFAOYSA-N 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- GSXUXSXBEUJRAJ-UHFFFAOYSA-N 4-bromo-2-nitrobenzaldehyde Chemical compound [O-][N+](=O)C1=CC(Br)=CC=C1C=O GSXUXSXBEUJRAJ-UHFFFAOYSA-N 0.000 description 1
- MZPNQUMLOFWSEK-UHFFFAOYSA-N 4-chloro-2-nitrobenzaldehyde Chemical compound [O-][N+](=O)C1=CC(Cl)=CC=C1C=O MZPNQUMLOFWSEK-UHFFFAOYSA-N 0.000 description 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- UDOQAMWYTUYIHP-UHFFFAOYSA-N [N+](=O)([O-])NC1=C(C=NO)C=CC=C1 Chemical compound [N+](=O)([O-])NC1=C(C=NO)C=CC=C1 UDOQAMWYTUYIHP-UHFFFAOYSA-N 0.000 description 1
- OTIKYRVPXSEIPV-UHFFFAOYSA-N acetic acid;phenylhydrazine Chemical compound CC(O)=O.NNC1=CC=CC=C1 OTIKYRVPXSEIPV-UHFFFAOYSA-N 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- GEXSYMYVUXRCKI-UHFFFAOYSA-N n-[(4-amino-2-nitrophenyl)methylidene]hydroxylamine Chemical compound NC1=CC=C(C=NO)C([N+]([O-])=O)=C1 GEXSYMYVUXRCKI-UHFFFAOYSA-N 0.000 description 1
- 125000003544 oxime group Chemical group 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 150000007659 semicarbazones Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE149748C true DE149748C (en, 2012) |
Family
ID=416734
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT149748D Active DE149748C (en, 2012) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE149748C (en, 2012) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2517150A1 (de) * | 1974-04-18 | 1975-10-30 | Mitsubishi Chem Ind | Photoempfindliche masse fuer die elektrophotographie |
-
0
- DE DENDAT149748D patent/DE149748C/de active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2517150A1 (de) * | 1974-04-18 | 1975-10-30 | Mitsubishi Chem Ind | Photoempfindliche masse fuer die elektrophotographie |
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