DE149603C - - Google Patents
Info
- Publication number
- DE149603C DE149603C DENDAT149603D DE149603DA DE149603C DE 149603 C DE149603 C DE 149603C DE NDAT149603 D DENDAT149603 D DE NDAT149603D DE 149603D A DE149603D A DE 149603DA DE 149603 C DE149603 C DE 149603C
- Authority
- DE
- Germany
- Prior art keywords
- oil
- farnesol
- alcohol
- saponification
- fractional distillation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 235000019198 oils Nutrition 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 11
- 150000002148 esters Chemical class 0.000 claims description 6
- 238000004508 fractional distillation Methods 0.000 claims description 6
- 238000007127 saponification reaction Methods 0.000 claims description 6
- 229930004725 sesquiterpene Natural products 0.000 claims description 5
- 150000004354 sesquiterpene derivatives Chemical class 0.000 claims description 5
- 150000008065 acid anhydrides Chemical class 0.000 claims description 4
- 239000007858 starting material Substances 0.000 claims description 4
- 241000402754 Erythranthe moschata Species 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- 240000007472 Leucaena leucocephala Species 0.000 claims description 2
- 235000010643 Leucaena leucocephala Nutrition 0.000 claims description 2
- 240000007313 Tilia cordata Species 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 2
- 235000005135 Micromeria juliana Nutrition 0.000 claims 1
- 240000002114 Satureja hortensis Species 0.000 claims 1
- 235000007315 Satureja hortensis Nutrition 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- CRDAMVZIKSXKFV-FBXUGWQNSA-N (2-cis,6-cis)-farnesol Chemical compound CC(C)=CCC\C(C)=C/CC\C(C)=C/CO CRDAMVZIKSXKFV-FBXUGWQNSA-N 0.000 description 11
- 239000000260 (2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-ol Substances 0.000 description 11
- 229930002886 farnesol Natural products 0.000 description 11
- 229940043259 farnesol Drugs 0.000 description 11
- CRDAMVZIKSXKFV-UHFFFAOYSA-N trans-Farnesol Natural products CC(C)=CCCC(C)=CCCC(C)=CCO CRDAMVZIKSXKFV-UHFFFAOYSA-N 0.000 description 11
- 239000003921 oil Substances 0.000 description 10
- 239000003205 fragrance Substances 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000002085 persistent effect Effects 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 239000001306 (7E,9E,11E,13E)-pentadeca-7,9,11,13-tetraen-1-ol Substances 0.000 description 1
- NOGFHTGYPKWWRX-UHFFFAOYSA-N 2,2,6,6-tetramethyloxan-4-one Chemical compound CC1(C)CC(=O)CC(C)(C)O1 NOGFHTGYPKWWRX-UHFFFAOYSA-N 0.000 description 1
- VFZDNKRDYPTSTP-UHFFFAOYSA-N 5,8,8-trimethyl-3-oxabicyclo[3.2.1]octane-2,4-dione Chemical compound O=C1OC(=O)C2(C)CCC1C2(C)C VFZDNKRDYPTSTP-UHFFFAOYSA-N 0.000 description 1
- 235000003074 Acacia farnesiana Nutrition 0.000 description 1
- 244000215068 Acacia senegal Species 0.000 description 1
- 241001493421 Robinia <trematode> Species 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000012230 colorless oil Substances 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 235000011118 potassium hydroxide Nutrition 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 150000003333 secondary alcohols Chemical class 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C33/00—Unsaturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C33/02—Acyclic alcohols with carbon-to-carbon double bonds
- C07C33/025—Acyclic alcohols with carbon-to-carbon double bonds with only one double bond
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE149603C true DE149603C (enrdf_load_stackoverflow) |
Family
ID=416598
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT149603D Active DE149603C (enrdf_load_stackoverflow) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE149603C (enrdf_load_stackoverflow) |
-
0
- DE DENDAT149603D patent/DE149603C/de active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE1692002B2 (de) | Riechstoffkomposition | |
| DE2317583C3 (de) | Verfahren zur Reinigung von a- Bisabolol | |
| DE2652452C2 (de) | Cyclohexenester, Verfahren zu ihrer Herstellung und ihre Verwendung als Riechstoffe | |
| DE149603C (enrdf_load_stackoverflow) | ||
| DE1218643B (de) | Riechstoffkomposition | |
| DE1617025B1 (de) | Verfahren zur Verlängerung der Durftwirkung parfümierter Materialien | |
| DE2726559C2 (de) | Parfum | |
| DE958837C (de) | Verfahren zur Herstellung von ambraartig riechendem 4,8,8-Trimethyl-9-methylenbicyclo-(1,3,3,)-nonanol-(4), dessen AEthern und Stereoisomeren | |
| DE2242913B2 (de) | Nordehydropatschulol, seine Gewinnung und dieses enthaltende Geruchskompositionen | |
| DE2418166C3 (de) | Verfahren zur Gewinnung von reinem «Bisabolol | |
| DE2461605C3 (de) | S-Acetyl-U.e-trimethyltricyclo [53 AO2·7!-dodeca-5-en, Verfahren zu seiner Herstellung und seine Verwendung als Riechstoff | |
| DE860214C (de) | Verfahren zur Herstellung von 2, 5, 5, 9-Tetramethyloktahydronaphthalinderivaten | |
| DE3128790C2 (de) | C-8-substituierte 1,5-Dimethyl-bicyclo[3.2.1]octan-8-ole, Verfahren zu ihrer Herstellung und ihre Verwendung | |
| EP0026323B1 (de) | 4(5)-Acetyl-9,9-dimethyltricyclo-(4.4.0.1(8,10))-undec-1-en, dessen Herstellung und Verwendung als Riechstoff, sowie dieses enthaltende Riechstoffkompositionen | |
| DE2209923A1 (de) | Verfahren zur Herstellung von synthetischem Limetteöl | |
| DE1966337C3 (de) | Dialkyl resorcinsäure-Este r | |
| DE428548C (de) | Verfahren zur Herstellung von Riechstoffen | |
| DE142416C (enrdf_load_stackoverflow) | ||
| DE80007C (enrdf_load_stackoverflow) | ||
| EP0051240B1 (de) | Acetylcycloundecan und Acetylcycloundecene, deren Verwendung und diese enthaltende Riechstoffkompositionen | |
| DE801988C (de) | Verfahren zur Reinigung und Trennung von durch Hydrierung von Kohlenoxyd erhaltenen,der Isobutylreihe angehoerenden Alkoholen | |
| DE254858C (enrdf_load_stackoverflow) | ||
| DE928949C (de) | Verfahren zur Aufarbeitung von Rohphenolen aus Schwelwaessern | |
| DE907110C (de) | Verfahren zur Herstellung geruchfreier Seifen | |
| DE1966337B2 (de) | Dialkylresorcinsaeure-ester |