DE122046C - - Google Patents

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Publication number

DE122046C

DE122046C DENDAT122046D DE122046DA DE122046C DE 122046 C DE122046 C DE 122046C DE NDAT122046 D DENDAT122046 D DE NDAT122046D DE 122046D A DE122046D A DE 122046DA DE 122046 C DE122046 C DE 122046C

Authority

DE

Germany

Prior art keywords

hydrochloric acid

tin

reduction

azoxybenzene

benzidine

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
• QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 5
• HPGGPRDJHPYFRM-UHFFFAOYSA-J tin(iv) chloride Chemical compound Cl[Sn](Cl)(Cl)Cl HPGGPRDJHPYFRM-UHFFFAOYSA-J 0.000 claims description 5
• ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 4
• 238000000034 method Methods 0.000 claims description 4
• HFACYLZERDEVSX-UHFFFAOYSA-N benzidine Chemical class C1=CC(N)=CC=C1C1=CC=C(N)C=C1 HFACYLZERDEVSX-UHFFFAOYSA-N 0.000 claims description 3
• 230000004048 modification Effects 0.000 claims 1
• 238000012986 modification Methods 0.000 claims 1
• GAUZCKBSTZFWCT-UHFFFAOYSA-N azoxybenzene Chemical compound C=1C=CC=CC=1[N+]([O-])=NC1=CC=CC=C1 GAUZCKBSTZFWCT-UHFFFAOYSA-N 0.000 description 6
• 239000002184 metal Substances 0.000 description 6
• 229910052751 metal Inorganic materials 0.000 description 6
• 238000006722 reduction reaction Methods 0.000 description 6
• LQNUZADURLCDLV-UHFFFAOYSA-N nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 description 4
• 150000003839 salts Chemical class 0.000 description 4
• 238000005868 electrolysis reaction Methods 0.000 description 3
• 239000000243 solution Substances 0.000 description 3
• PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
• 239000002253 acid Substances 0.000 description 2
• 238000006243 chemical reaction Methods 0.000 description 2
• 230000000694 effects Effects 0.000 description 2
• 150000002739 metals Chemical class 0.000 description 2
• 239000011135 tin Substances 0.000 description 2
• 229910052718 tin Inorganic materials 0.000 description 2
• FYRTZXXTIDKEJD-UHFFFAOYSA-N 4-(4-aminophenyl)aniline;hydron;chloride Chemical compound Cl.C1=CC(N)=CC=C1C1=CC=C(N)C=C1 FYRTZXXTIDKEJD-UHFFFAOYSA-N 0.000 description 1
• HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
• ZOXJIQNURSAHRV-UHFFFAOYSA-N [4-(4-azaniumylphenyl)phenyl]azanium;sulfate Chemical compound [O-]S([O-])(=O)=O.C1=CC([NH3+])=CC=C1C1=CC=C([NH3+])C=C1 ZOXJIQNURSAHRV-UHFFFAOYSA-N 0.000 description 1
• 239000003513 alkali Substances 0.000 description 1
• 150000001447 alkali salts Chemical class 0.000 description 1
• 239000002585 base Substances 0.000 description 1
• 239000003638 chemical reducing agent Substances 0.000 description 1
• 150000001879 copper Chemical class 0.000 description 1
• 230000008021 deposition Effects 0.000 description 1
• 230000002349 favourable effect Effects 0.000 description 1
• HKOOXMFOFWEVGF-UHFFFAOYSA-N phenylhydrazine Chemical compound NNC1=CC=CC=C1 HKOOXMFOFWEVGF-UHFFFAOYSA-N 0.000 description 1
• 230000001105 regulatory effect Effects 0.000 description 1
• 239000012266 salt solution Substances 0.000 description 1
• 229910052725 zinc Inorganic materials 0.000 description 1
• 239000011701 zinc Substances 0.000 description 1